JPH0521601B2 - - Google Patents
Info
- Publication number
- JPH0521601B2 JPH0521601B2 JP57170620A JP17062082A JPH0521601B2 JP H0521601 B2 JPH0521601 B2 JP H0521601B2 JP 57170620 A JP57170620 A JP 57170620A JP 17062082 A JP17062082 A JP 17062082A JP H0521601 B2 JPH0521601 B2 JP H0521601B2
- Authority
- JP
- Japan
- Prior art keywords
- rectification
- column
- boiling components
- packed
- height
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000009835 boiling Methods 0.000 claims description 42
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 24
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 23
- 239000002994 raw material Substances 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 15
- BGJSXRVXTHVRSN-UHFFFAOYSA-N 1,3,5-trioxane Chemical compound C1OCOCO1 BGJSXRVXTHVRSN-UHFFFAOYSA-N 0.000 claims description 10
- 238000004821 distillation Methods 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 2
- 239000007789 gas Substances 0.000 description 16
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- 239000007788 liquid Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 4
- 238000001944 continuous distillation Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- FQERLIOIVXPZKH-UHFFFAOYSA-N 1,2,4-trioxane Chemical compound C1COOCO1 FQERLIOIVXPZKH-UHFFFAOYSA-N 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- BLRVCKQECOAMHS-UHFFFAOYSA-N N[H].C=O.[H]CO Chemical compound N[H].C=O.[H]CO BLRVCKQECOAMHS-UHFFFAOYSA-N 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- -1 trioxane-benzene-formaldehyde Chemical compound 0.000 description 1
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP17062082A JPS5959202A (ja) | 1982-09-29 | 1982-09-29 | 精留方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP17062082A JPS5959202A (ja) | 1982-09-29 | 1982-09-29 | 精留方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5959202A JPS5959202A (ja) | 1984-04-05 |
JPH0521601B2 true JPH0521601B2 (zh) | 1993-03-25 |
Family
ID=15908242
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP17062082A Granted JPS5959202A (ja) | 1982-09-29 | 1982-09-29 | 精留方法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5959202A (zh) |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS56155601A (en) * | 1980-05-07 | 1981-12-01 | Hitachi Ltd | Distilling column |
-
1982
- 1982-09-29 JP JP17062082A patent/JPS5959202A/ja active Granted
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS56155601A (en) * | 1980-05-07 | 1981-12-01 | Hitachi Ltd | Distilling column |
Also Published As
Publication number | Publication date |
---|---|
JPS5959202A (ja) | 1984-04-05 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN100522916C (zh) | 从甲醇羰基化工艺流中去除还原高锰酸盐的化合物 | |
JP4658945B2 (ja) | エチレンアミン類を含有している混合物の蒸留による分離方法 | |
US4008131A (en) | Purification of acetic acid | |
KR101546464B1 (ko) | (메트)아크릴산의 연속 회수 방법 및 회수 장치 | |
KR20160105370A (ko) | 메틸 메타크릴레이트의 제조 방법 | |
JP3202150B2 (ja) | 酢酸の精製方法 | |
CN107709279A (zh) | 乙酸的制造方法 | |
EP0693957A4 (en) | MULTI-STOREY SUSPENDED REACTIVE EXTRACTION APPARATUS AND METHOD | |
JP2018517558A (ja) | 蒸留装置 | |
CN114105937A (zh) | 一种三聚甲醛的反应方法及其生产方法 | |
US3691021A (en) | Process for purification of vinyl acetate by extractive distillation | |
US5821384A (en) | Process for generating vinyl carboxylate esters | |
EP3362432B1 (en) | Process for purification of methyl methacrylate | |
US6921830B2 (en) | Method for purifying an organic solvent for the purposes of absorption of maleic acid anhydride | |
KR101616553B1 (ko) | (메트)아크릴산의 연속 회수 방법 및 장치 | |
JPH0521601B2 (zh) | ||
US3591463A (en) | Separation of chloroform and/or ethyl acetate and/or methylethyl ketone from vinyl acetate by extractive distillation | |
US5705039A (en) | Process for purifying a 2,6-dialkylphenol | |
JP2506021B2 (ja) | カプロラクタムの精製法 | |
JP2004323526A (ja) | 高純度トリエチレンジアミン(teda)を蒸留により精製する方法 | |
JPS63205101A (ja) | 炭酸ジメチルの分離方法 | |
US9914684B2 (en) | Feed sources for allyl alcohol production processes | |
JPS6236022B2 (zh) | ||
CN217472733U (zh) | 一种三聚甲醛的反应设备及其生产系统 | |
KR101628287B1 (ko) | (메트)아크릴산의 연속 회수 방법 및 장치 |