JPH04135495A - 難消化性多糖類の製造法 - Google Patents
難消化性多糖類の製造法Info
- Publication number
- JPH04135495A JPH04135495A JP2185851A JP18585190A JPH04135495A JP H04135495 A JPH04135495 A JP H04135495A JP 2185851 A JP2185851 A JP 2185851A JP 18585190 A JP18585190 A JP 18585190A JP H04135495 A JPH04135495 A JP H04135495A
- Authority
- JP
- Japan
- Prior art keywords
- inorganic acid
- starch
- polysaccharide
- indigestible
- aqueous solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000004676 glycans Chemical class 0.000 title claims abstract description 33
- 229920001282 polysaccharide Polymers 0.000 title claims abstract description 32
- 239000005017 polysaccharide Substances 0.000 title claims abstract description 32
- 238000004519 manufacturing process Methods 0.000 title claims description 9
- 229920002472 Starch Polymers 0.000 claims abstract description 22
- 235000019698 starch Nutrition 0.000 claims abstract description 22
- 239000008107 starch Substances 0.000 claims abstract description 20
- 229920001353 Dextrin Polymers 0.000 claims abstract description 19
- 239000004375 Dextrin Substances 0.000 claims abstract description 19
- 235000019425 dextrin Nutrition 0.000 claims abstract description 19
- 239000007864 aqueous solution Substances 0.000 claims abstract description 15
- 150000007522 mineralic acids Chemical class 0.000 claims abstract description 15
- 239000004382 Amylase Substances 0.000 claims abstract description 12
- 102000013142 Amylases Human genes 0.000 claims abstract description 12
- 108010065511 Amylases Proteins 0.000 claims abstract description 12
- 235000019418 amylase Nutrition 0.000 claims abstract description 12
- 235000000346 sugar Nutrition 0.000 claims abstract description 11
- 150000007524 organic acids Chemical class 0.000 claims abstract description 6
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000003456 ion exchange resin Substances 0.000 claims abstract description 3
- 229920003303 ion-exchange polymer Polymers 0.000 claims abstract description 3
- 239000000243 solution Substances 0.000 claims description 12
- 150000001720 carbohydrates Chemical class 0.000 claims description 8
- 238000005194 fractionation Methods 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 abstract description 16
- 239000008103 glucose Substances 0.000 abstract description 16
- 239000007788 liquid Substances 0.000 abstract description 8
- 238000000354 decomposition reaction Methods 0.000 abstract description 7
- 108010073178 Glucan 1,4-alpha-Glucosidase Proteins 0.000 abstract description 6
- 102100022624 Glucoamylase Human genes 0.000 abstract description 6
- 238000000034 method Methods 0.000 abstract description 6
- 238000010438 heat treatment Methods 0.000 abstract description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract description 4
- 240000003183 Manihot esculenta Species 0.000 abstract description 3
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 abstract description 3
- 230000003472 neutralizing effect Effects 0.000 abstract description 2
- -1 HCl Chemical class 0.000 abstract 1
- 239000000706 filtrate Substances 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 235000015097 nutrients Nutrition 0.000 abstract 1
- 150000004804 polysaccharides Polymers 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 16
- 239000000203 mixture Substances 0.000 description 9
- 238000006243 chemical reaction Methods 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 235000013305 food Nutrition 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 239000002253 acid Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 description 3
- 229920002261 Corn starch Polymers 0.000 description 3
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 239000008120 corn starch Substances 0.000 description 3
- 229940099112 cornstarch Drugs 0.000 description 3
- 239000005909 Kieselgur Substances 0.000 description 2
- DLRVVLDZNNYCBX-UHFFFAOYSA-N Polydextrose Polymers OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(O)O1 DLRVVLDZNNYCBX-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 2
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 description 2
- 235000013361 beverage Nutrition 0.000 description 2
- 235000014633 carbohydrates Nutrition 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 238000011033 desalting Methods 0.000 description 2
- 235000005911 diet Nutrition 0.000 description 2
- 230000000378 dietary effect Effects 0.000 description 2
- 235000015110 jellies Nutrition 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000011550 stock solution Substances 0.000 description 2
- 150000008163 sugars Chemical class 0.000 description 2
- 238000002560 therapeutic procedure Methods 0.000 description 2
- VZSRBBMJRBPUNF-UHFFFAOYSA-N 2-(2,3-dihydro-1H-inden-2-ylamino)-N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]pyrimidine-5-carboxamide Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C(=O)NCCC(N1CC2=C(CC1)NN=N2)=O VZSRBBMJRBPUNF-UHFFFAOYSA-N 0.000 description 1
- AYRXSINWFIIFAE-UHFFFAOYSA-N O6-alpha-D-Galactopyranosyl-D-galactose Natural products OCC1OC(OCC(O)C(O)C(O)C(O)C=O)C(O)C(O)C1O AYRXSINWFIIFAE-UHFFFAOYSA-N 0.000 description 1
- 229920001100 Polydextrose Polymers 0.000 description 1
- 239000003377 acid catalyst Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 235000019577 caloric intake Nutrition 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000003729 cation exchange resin Substances 0.000 description 1
- 239000007809 chemical reaction catalyst Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 235000019621 digestibility Nutrition 0.000 description 1
- 235000012041 food component Nutrition 0.000 description 1
- 239000005417 food ingredient Substances 0.000 description 1
- 238000002523 gelfiltration Methods 0.000 description 1
- DLRVVLDZNNYCBX-CQUJWQHSSA-N gentiobiose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC[C@@H]1[C@@H](O)[C@H](O)[C@@H](O)C(O)O1 DLRVVLDZNNYCBX-CQUJWQHSSA-N 0.000 description 1
- 230000009229 glucose formation Effects 0.000 description 1
- 125000002791 glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 1
- 229920006158 high molecular weight polymer Polymers 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 125000003071 maltose group Chemical group 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 235000013856 polydextrose Nutrition 0.000 description 1
- 239000001259 polydextrose Substances 0.000 description 1
- 229940035035 polydextrose Drugs 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 229920001592 potato starch Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 150000004043 trisaccharides Chemical class 0.000 description 1
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2185851A JPH04135495A (ja) | 1990-07-13 | 1990-07-13 | 難消化性多糖類の製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2185851A JPH04135495A (ja) | 1990-07-13 | 1990-07-13 | 難消化性多糖類の製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH04135495A true JPH04135495A (ja) | 1992-05-08 |
| JPH0587237B2 JPH0587237B2 (enrdf_load_stackoverflow) | 1993-12-15 |
Family
ID=16177992
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2185851A Granted JPH04135495A (ja) | 1990-07-13 | 1990-07-13 | 難消化性多糖類の製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH04135495A (enrdf_load_stackoverflow) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0591473A4 (en) * | 1992-03-24 | 1995-03-01 | American Maize Prod Co | STARCH-BASED JELLY SWEETS. |
| US5698437A (en) * | 1993-12-20 | 1997-12-16 | Matsutani Chemical Industry Co., Ltd. | Agent for promoting the proliferation of bifidobacterium |
| JPH11209403A (ja) * | 1991-10-29 | 1999-08-03 | Matsutani Chem Ind Ltd | 難消化性デキストリンを含有する酒類 |
| JP2009524439A (ja) * | 2006-01-25 | 2009-07-02 | テイト アンド ライル イングレディエンツ アメリカス インコーポレイテッド | 遅消化性または消化抵抗性炭水化物組成物を含んでなる食物製品 |
| FR2987360A1 (fr) * | 2012-02-28 | 2013-08-30 | Roquette Freres | Maltodextrines hyperbranchees hypo-glycemiantes |
| US8993039B2 (en) | 2006-01-25 | 2015-03-31 | Tate & Lyle Ingredients Americas Llc | Fiber-containing carbohydrate composition |
| US11540549B2 (en) | 2019-11-28 | 2023-01-03 | Tate & Lyle Solutions Usa Llc | High-fiber, low-sugar soluble dietary fibers, products including them and methods for using them |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3974032A (en) * | 1973-03-05 | 1976-08-10 | Cpc International Inc. | Low D.E. starch hydrolysates of improved stability prepared by enzymatic hydrolysis of dextrins |
| JPH02154664A (ja) * | 1988-12-05 | 1990-06-14 | Matsutani Kagaku Kogyo Kk | 食物繊維高含有デキストリンの製造法 |
-
1990
- 1990-07-13 JP JP2185851A patent/JPH04135495A/ja active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3974032A (en) * | 1973-03-05 | 1976-08-10 | Cpc International Inc. | Low D.E. starch hydrolysates of improved stability prepared by enzymatic hydrolysis of dextrins |
| JPH02154664A (ja) * | 1988-12-05 | 1990-06-14 | Matsutani Kagaku Kogyo Kk | 食物繊維高含有デキストリンの製造法 |
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11209403A (ja) * | 1991-10-29 | 1999-08-03 | Matsutani Chem Ind Ltd | 難消化性デキストリンを含有する酒類 |
| EP0591473A4 (en) * | 1992-03-24 | 1995-03-01 | American Maize Prod Co | STARCH-BASED JELLY SWEETS. |
| US5698437A (en) * | 1993-12-20 | 1997-12-16 | Matsutani Chemical Industry Co., Ltd. | Agent for promoting the proliferation of bifidobacterium |
| EP0659769B1 (en) * | 1993-12-20 | 1998-07-15 | Matsutani Chemical Industry Co., Ltd. | Agent for promoting the proliferation of Bifidobacterium |
| US9957537B2 (en) | 2006-01-25 | 2018-05-01 | Tate & Lyle Ingredients Americas Llc | Fiber-containing carbohydrate composition |
| JP2013066476A (ja) * | 2006-01-25 | 2013-04-18 | Tate & Lyle Ingredients Americas Llc | 遅消化性または消化抵抗性炭水化物組成物を含んでなる食物製品 |
| US8993039B2 (en) | 2006-01-25 | 2015-03-31 | Tate & Lyle Ingredients Americas Llc | Fiber-containing carbohydrate composition |
| US9868969B2 (en) | 2006-01-25 | 2018-01-16 | Tate & Lyle Ingredients Americas Llc | Fiber-containing carbohydrate composition |
| JP2009524439A (ja) * | 2006-01-25 | 2009-07-02 | テイト アンド ライル イングレディエンツ アメリカス インコーポレイテッド | 遅消化性または消化抵抗性炭水化物組成物を含んでなる食物製品 |
| US9963726B2 (en) | 2006-01-25 | 2018-05-08 | Tate & Lyle Ingredients Americas Llc | Fiber-containing carbohydrate composition |
| US10344308B2 (en) | 2006-01-25 | 2019-07-09 | Tate & Lyle Ingredients Americas Llc | Fiber-containing carbohydrate composition |
| FR2987360A1 (fr) * | 2012-02-28 | 2013-08-30 | Roquette Freres | Maltodextrines hyperbranchees hypo-glycemiantes |
| WO2013128121A1 (fr) * | 2012-02-28 | 2013-09-06 | Roquette Freres | Maltodextrines hyperbranchees hypo-glycemiantes |
| KR20140141580A (ko) * | 2012-02-28 | 2014-12-10 | 로께뜨프레르 | 혈당강하 고분지형 말토덱스트린 |
| JP2015510014A (ja) * | 2012-02-28 | 2015-04-02 | ロケット・フルーレ | 血糖降下性多分岐マルトデキストリン |
| US11540549B2 (en) | 2019-11-28 | 2023-01-03 | Tate & Lyle Solutions Usa Llc | High-fiber, low-sugar soluble dietary fibers, products including them and methods for using them |
| US12161142B2 (en) | 2019-11-28 | 2024-12-10 | Tate & Lyle Solutions Usa Llc | Methods for using high-fiber, low-sugar soluble dietary fibers |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0587237B2 (enrdf_load_stackoverflow) | 1993-12-15 |
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