JPH0413338B2 - - Google Patents
Info
- Publication number
- JPH0413338B2 JPH0413338B2 JP62317289A JP31728987A JPH0413338B2 JP H0413338 B2 JPH0413338 B2 JP H0413338B2 JP 62317289 A JP62317289 A JP 62317289A JP 31728987 A JP31728987 A JP 31728987A JP H0413338 B2 JPH0413338 B2 JP H0413338B2
- Authority
- JP
- Japan
- Prior art keywords
- ethyl chloroformate
- water
- ethanol
- ethoxythiocarbonyl
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- RIFGWPKJUGCATF-UHFFFAOYSA-N ethyl chloroformate Chemical compound CCOC(Cl)=O RIFGWPKJUGCATF-UHFFFAOYSA-N 0.000 claims abstract description 13
- RZFBEFUNINJXRQ-UHFFFAOYSA-M sodium ethyl xanthate Chemical compound [Na+].CCOC([S-])=S RZFBEFUNINJXRQ-UHFFFAOYSA-M 0.000 claims abstract description 13
- ALGQDBJUFSYDLA-UHFFFAOYSA-N o-ethyl ethoxycarbothioylsulfanylmethanethioate Chemical compound CCOC(=S)SC(=S)OCC ALGQDBJUFSYDLA-UHFFFAOYSA-N 0.000 claims abstract description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 16
- 239000002253 acid Substances 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 5
- 238000001308 synthesis method Methods 0.000 claims description 5
- 238000003786 synthesis reaction Methods 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract 1
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- 239000011541 reaction mixture Substances 0.000 description 4
- 239000006227 byproduct Substances 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 230000002194 synthesizing effect Effects 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 235000019502 Orange oil Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- MYXNWWDJRWCURH-UHFFFAOYSA-N ethoxymethanethioic s-acid Chemical compound CCOC(S)=O MYXNWWDJRWCURH-UHFFFAOYSA-N 0.000 description 1
- -1 ethoxythiocarbonyl Chemical class 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000010502 orange oil Substances 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 238000010647 peptide synthesis reaction Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- 239000013076 target substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C329/00—Thiocarbonic acids; Halides, esters or anhydrides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Paper (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US94353686A | 1986-12-18 | 1986-12-18 | |
| US943536 | 1986-12-18 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS63179854A JPS63179854A (ja) | 1988-07-23 |
| JPH0413338B2 true JPH0413338B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1992-03-09 |
Family
ID=25479827
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP62317289A Granted JPS63179854A (ja) | 1986-12-18 | 1987-12-15 | 硫化ビス（エトキシチオカルボニル）の合成法 |
Country Status (12)
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11490898B2 (en) | 2019-10-18 | 2022-11-08 | Depuy Synthes Products, Inc | Surgical saw blade |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4354980A (en) * | 1981-06-04 | 1982-10-19 | Crozier Ronald D G | Process for producing alkyl xanthogen alkylformates |
-
1987
- 1987-02-17 ZA ZA879455A patent/ZA879455B/xx unknown
- 1987-12-15 EP EP87311015A patent/EP0274876B1/en not_active Expired - Lifetime
- 1987-12-15 JP JP62317289A patent/JPS63179854A/ja active Granted
- 1987-12-15 AT AT87311015T patent/ATE60577T1/de not_active IP Right Cessation
- 1987-12-15 DE DE8787311015T patent/DE3767865D1/de not_active Expired - Lifetime
- 1987-12-15 ES ES87311015T patent/ES2019948B3/es not_active Expired - Lifetime
- 1987-12-16 CA CA000554442A patent/CA1297888C/en not_active Expired - Lifetime
- 1987-12-17 AU AU82656/87A patent/AU593414B2/en not_active Ceased
- 1987-12-17 MX MX981487A patent/MX168553B/es unknown
- 1987-12-17 DK DK664987A patent/DK169405B1/da not_active IP Right Cessation
- 1987-12-17 IE IE343187A patent/IE60136B1/en not_active IP Right Cessation
-
1991
- 1991-01-31 GR GR91400098T patent/GR3001414T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| IE873431L (en) | 1988-06-18 |
| ATE60577T1 (de) | 1991-02-15 |
| AU593414B2 (en) | 1990-02-08 |
| ES2019948B3 (es) | 1991-07-16 |
| JPS63179854A (ja) | 1988-07-23 |
| DK664987A (da) | 1988-06-19 |
| EP0274876A1 (en) | 1988-07-20 |
| CA1297888C (en) | 1992-03-24 |
| EP0274876B1 (en) | 1991-01-30 |
| ZA879455B (en) | 1989-07-26 |
| GR3001414T3 (en) | 1992-09-25 |
| DK664987D0 (da) | 1987-12-17 |
| DK169405B1 (da) | 1994-10-24 |
| DE3767865D1 (de) | 1991-03-07 |
| MX168553B (es) | 1993-05-31 |
| IE60136B1 (en) | 1994-06-01 |
| AU8265687A (en) | 1988-06-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| SU1508959A3 (ru) | Способ получени производных карбапенема | |
| US5498711A (en) | Synthesis of 4,10-dinitro-2,6,8,12-tetraoxa-4,10-diazatetracyclo[5.5.0.05,903,11]dodecane | |
| US4222970A (en) | Process for producing phosphonomycin | |
| JPH0413338B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| JPH07116126B2 (ja) | ２，３‐ジアミノアクリロニトリル誘導体 | |
| JPS6210510B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| KR950001026B1 (ko) | 페니실란산 유도체의 개선된 제조방법 | |
| JPH0737440B2 (ja) | スルホニウム化合物の製造方法 | |
| EP0105664B1 (en) | Process for the preparation of 3-carboxy-1-methylpyrrol-2-acetic-acid and alkali metal salts thereof | |
| KR100502390B1 (ko) | 세팔로스포린산 유도체의 제조방법 | |
| US4515958A (en) | Process for preparing 1-alkyl-5-mercaptotetrazoles | |
| US3308132A (en) | 6, 8-dithiooctanoyl amides and intermediates | |
| JPS61218555A (ja) | トリフルオロジクロロエチル基により置換された酸類の製法および亜鉛化合物類 | |
| KR890001851B1 (ko) | 아미노알칸올에스테르의 신규 제조방법 | |
| KR100229175B1 (ko) | 세펨 유도체의 제조방법 | |
| JPH06256286A (ja) | １−アミノ−１−シアナミド−２，２−ジシアノエチレン ナトリウム塩の製造方法 | |
| HUT59687A (en) | Process for producing 7-amino-3-methoxy-methyl-ceph-3-eme-4-carboxylic acid | |
| KR100245015B1 (ko) | ο-(카르보알콕시)페닐메탄술포닐 클로라이드 유도체의 제조방법 | |
| KR0164947B1 (ko) | 7-아미노-3-메톡시메틸-3-세펨-4-카르복실산의 신규 제조방법 | |
| JP2553859B2 (ja) | ピラゾ−ル誘導体の製造方法 | |
| HU190428B (en) | Process for the production of n-/phosphono-methyl/-glycine | |
| KR960005518B1 (ko) | 1-아미노-4-[[2-(치환된아미노)메틸-4-메틸-6-술포페닐]아미노]-9,10-디히드로-9, 10-디옥소-2-안트라센술폰산의 제조방법 | |
| JPH10218868A (ja) | ５ーメチルテトラゾールの製造方法 | |
| SU482453A1 (ru) | Способ получени 2-фенацилхиноксалонов-3 | |
| JPS61140554A (ja) | アルキルｎ‐マレイルフエニルアラネートの用途およびその製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| LAPS | Cancellation because of no payment of annual fees |