JPS63179854A - 硫化ビス（エトキシチオカルボニル）の合成法 - Google Patents
硫化ビス（エトキシチオカルボニル）の合成法Info
- Publication number
- JPS63179854A JPS63179854A JP62317289A JP31728987A JPS63179854A JP S63179854 A JPS63179854 A JP S63179854A JP 62317289 A JP62317289 A JP 62317289A JP 31728987 A JP31728987 A JP 31728987A JP S63179854 A JPS63179854 A JP S63179854A
- Authority
- JP
- Japan
- Prior art keywords
- water
- synthesis method
- ethoxythiocarbonyl
- bis
- sulfide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- ALGQDBJUFSYDLA-UHFFFAOYSA-N o-ethyl ethoxycarbothioylsulfanylmethanethioate Chemical compound CCOC(=S)SC(=S)OCC ALGQDBJUFSYDLA-UHFFFAOYSA-N 0.000 title claims description 6
- 238000001308 synthesis method Methods 0.000 title claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- RIFGWPKJUGCATF-UHFFFAOYSA-N ethyl chloroformate Chemical compound CCOC(Cl)=O RIFGWPKJUGCATF-UHFFFAOYSA-N 0.000 claims description 12
- RZFBEFUNINJXRQ-UHFFFAOYSA-M sodium ethyl xanthate Chemical compound [Na+].CCOC([S-])=S RZFBEFUNINJXRQ-UHFFFAOYSA-M 0.000 claims description 12
- 239000002253 acid Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 238000006243 chemical reaction Methods 0.000 claims description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 description 8
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- 239000011541 reaction mixture Substances 0.000 description 4
- 230000002194 synthesizing effect Effects 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 235000019502 Orange oil Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- MYXNWWDJRWCURH-UHFFFAOYSA-N ethoxymethanethioic s-acid Chemical compound CCOC(S)=O MYXNWWDJRWCURH-UHFFFAOYSA-N 0.000 description 1
- -1 ethoxythiocarbonyl Chemical class 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 239000010502 orange oil Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- 239000013076 target substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C329/00—Thiocarbonic acids; Halides, esters or anhydrides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Paper (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US94353686A | 1986-12-18 | 1986-12-18 | |
| US943536 | 1986-12-18 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS63179854A true JPS63179854A (ja) | 1988-07-23 |
| JPH0413338B2 JPH0413338B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1992-03-09 |
Family
ID=25479827
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP62317289A Granted JPS63179854A (ja) | 1986-12-18 | 1987-12-15 | 硫化ビス（エトキシチオカルボニル）の合成法 |
Country Status (12)
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11490898B2 (en) | 2019-10-18 | 2022-11-08 | Depuy Synthes Products, Inc | Surgical saw blade |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4354980A (en) * | 1981-06-04 | 1982-10-19 | Crozier Ronald D G | Process for producing alkyl xanthogen alkylformates |
-
1987
- 1987-02-17 ZA ZA879455A patent/ZA879455B/xx unknown
- 1987-12-15 EP EP87311015A patent/EP0274876B1/en not_active Expired - Lifetime
- 1987-12-15 ES ES87311015T patent/ES2019948B3/es not_active Expired - Lifetime
- 1987-12-15 AT AT87311015T patent/ATE60577T1/de not_active IP Right Cessation
- 1987-12-15 DE DE8787311015T patent/DE3767865D1/de not_active Expired - Lifetime
- 1987-12-15 JP JP62317289A patent/JPS63179854A/ja active Granted
- 1987-12-16 CA CA000554442A patent/CA1297888C/en not_active Expired - Lifetime
- 1987-12-17 DK DK664987A patent/DK169405B1/da not_active IP Right Cessation
- 1987-12-17 IE IE343187A patent/IE60136B1/en not_active IP Right Cessation
- 1987-12-17 AU AU82656/87A patent/AU593414B2/en not_active Ceased
- 1987-12-17 MX MX981487A patent/MX168553B/es unknown
-
1991
- 1991-01-31 GR GR91400098T patent/GR3001414T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| AU593414B2 (en) | 1990-02-08 |
| AU8265687A (en) | 1988-06-23 |
| EP0274876B1 (en) | 1991-01-30 |
| ES2019948B3 (es) | 1991-07-16 |
| IE873431L (en) | 1988-06-18 |
| CA1297888C (en) | 1992-03-24 |
| DK664987D0 (da) | 1987-12-17 |
| ATE60577T1 (de) | 1991-02-15 |
| MX168553B (es) | 1993-05-31 |
| DK169405B1 (da) | 1994-10-24 |
| IE60136B1 (en) | 1994-06-01 |
| GR3001414T3 (en) | 1992-09-25 |
| DE3767865D1 (de) | 1991-03-07 |
| ZA879455B (en) | 1989-07-26 |
| EP0274876A1 (en) | 1988-07-20 |
| JPH0413338B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1992-03-09 |
| DK664987A (da) | 1988-06-19 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| LAPS | Cancellation because of no payment of annual fees |