JPH0331646B2 - - Google Patents
Info
- Publication number
- JPH0331646B2 JPH0331646B2 JP62205255A JP20525587A JPH0331646B2 JP H0331646 B2 JPH0331646 B2 JP H0331646B2 JP 62205255 A JP62205255 A JP 62205255A JP 20525587 A JP20525587 A JP 20525587A JP H0331646 B2 JPH0331646 B2 JP H0331646B2
- Authority
- JP
- Japan
- Prior art keywords
- aqueous solution
- temperature
- stannous
- stannous oxide
- produced
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- QHGNHLZPVBIIPX-UHFFFAOYSA-N tin(II) oxide Inorganic materials [Sn]=O QHGNHLZPVBIIPX-UHFFFAOYSA-N 0.000 claims description 68
- 239000007864 aqueous solution Substances 0.000 claims description 29
- 230000002378 acidificating effect Effects 0.000 claims description 20
- 150000001805 chlorine compounds Chemical class 0.000 claims description 15
- 150000003839 salts Chemical class 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 230000032683 aging Effects 0.000 claims description 3
- CJGYQECZUAUFSN-UHFFFAOYSA-N oxygen(2-);tin(2+) Chemical compound [O-2].[Sn+2] CJGYQECZUAUFSN-UHFFFAOYSA-N 0.000 claims 7
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 16
- 235000002639 sodium chloride Nutrition 0.000 description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 10
- 238000000034 method Methods 0.000 description 10
- 235000019270 ammonium chloride Nutrition 0.000 description 8
- 238000007747 plating Methods 0.000 description 8
- 239000007788 liquid Substances 0.000 description 7
- 239000000243 solution Substances 0.000 description 7
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 5
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- 238000004090 dissolution Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 235000011121 sodium hydroxide Nutrition 0.000 description 4
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 4
- CVNKFOIOZXAFBO-UHFFFAOYSA-J tin(4+);tetrahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[Sn+4] CVNKFOIOZXAFBO-UHFFFAOYSA-J 0.000 description 4
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000006356 dehydrogenation reaction Methods 0.000 description 3
- 229910001432 tin ion Inorganic materials 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000007865 diluting Methods 0.000 description 2
- 229960002050 hydrofluoric acid Drugs 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- -1 tin hydrogen compounds Chemical class 0.000 description 2
- 229910001887 tin oxide Inorganic materials 0.000 description 2
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 238000002835 absorbance Methods 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 229910000679 solder Inorganic materials 0.000 description 1
- 238000005476 soldering Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003606 tin compounds Chemical class 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 235000005074 zinc chloride Nutrition 0.000 description 1
- 239000011592 zinc chloride Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP20525587A JPS6451330A (en) | 1987-08-20 | 1987-08-20 | Production of stannous oxide having high purity |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP20525587A JPS6451330A (en) | 1987-08-20 | 1987-08-20 | Production of stannous oxide having high purity |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6451330A JPS6451330A (en) | 1989-02-27 |
| JPH0331646B2 true JPH0331646B2 (fi) | 1991-05-08 |
Family
ID=16503958
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP20525587A Granted JPS6451330A (en) | 1987-08-20 | 1987-08-20 | Production of stannous oxide having high purity |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6451330A (fi) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103030172A (zh) * | 2011-09-30 | 2013-04-10 | 陶氏环球技术有限公司 | 制备SnO的方法 |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4975367B2 (ja) * | 2006-05-10 | 2012-07-11 | Ｊｘ日鉱日石金属株式会社 | 高純度酸化第一錫、同粉末及び高純度酸化第一錫の製造方法 |
| JP6121090B2 (ja) * | 2011-05-10 | 2017-04-26 | 三菱マテリアル株式会社 | Ｓｎ合金めっき液へのＳｎ成分補給用酸化第一錫粉末の製造方法及び該方法により製造された酸化第一錫粉末 |
| EP2578536B1 (en) * | 2011-09-30 | 2014-04-09 | Dow Global Technologies LLC | Plurality of SNO flakes |
| JP6157825B2 (ja) | 2011-10-31 | 2017-07-05 | ダウ グローバル テクノロジーズ エルエルシー | ＳｎＯを製造する方法 |
| CN103833069B (zh) * | 2013-12-20 | 2016-04-20 | 柳州百韧特先进材料有限公司 | 一种利用甲基磺酸亚锡含锡废液制备氧化亚锡的方法 |
| JP2015133306A (ja) * | 2014-01-16 | 2015-07-23 | 株式会社オートネットワーク技術研究所 | コネクタ用電気接点材料及びその製造方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61122123A (ja) * | 1984-11-17 | 1986-06-10 | Fuji Photo Film Co Ltd | 導電性酸化スズ微粉末の製造方法 |
-
1987
- 1987-08-20 JP JP20525587A patent/JPS6451330A/ja active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61122123A (ja) * | 1984-11-17 | 1986-06-10 | Fuji Photo Film Co Ltd | 導電性酸化スズ微粉末の製造方法 |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103030172A (zh) * | 2011-09-30 | 2013-04-10 | 陶氏环球技术有限公司 | 制备SnO的方法 |
| CN103030172B (zh) * | 2011-09-30 | 2015-04-22 | 陶氏环球技术有限公司 | 制备SnO的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6451330A (en) | 1989-02-27 |
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