JPH0225388B2

JPH0225388B2 -

Info

Publication number: JPH0225388B2
Authority: JP; Japan
Prior art keywords: water; dispersed; coating composition; weight; acid
Prior art date: 1981-11-18
Legal status : Expired

Application number

JP57200491A

Other languages

English (en)

Japanese (ja)

Other versions

JPS5889665A (ja

Inventor

Edoin Kuin Robaato

Current Assignee

Lubrizol Corp

Original Assignee

Lubrizol Corp

Priority date

1981-11-18

Filing date

1982-11-17

Publication date

1990-06-01

1982-11-17 Application filed by Lubrizol Corp filed Critical Lubrizol Corp

1983-05-28 Publication of JPS5889665A publication Critical patent/JPS5889665A/ja

1990-06-01 Publication of JPH0225388B2 publication Critical patent/JPH0225388B2/ja

Status Granted legal-status Critical Current

Links

229910052751 metal Inorganic materials 0.000 claims description 128
239000002184 metal Substances 0.000 claims description 128
-1 alkaline earth metal salts Chemical class 0.000 claims description 104
239000008199 coating composition Substances 0.000 claims description 93
239000000203 mixture Substances 0.000 claims description 77
239000002245 particle Substances 0.000 claims description 72
239000006185 dispersion Substances 0.000 claims description 64
238000001246 colloidal dispersion Methods 0.000 claims description 49
239000003795 chemical substances by application Substances 0.000 claims description 42
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 39
239000002612 dispersion medium Substances 0.000 claims description 29
LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 28
239000002585 base Substances 0.000 claims description 27
239000000178 monomer Substances 0.000 claims description 27
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 26
239000007787 solid Substances 0.000 claims description 25
125000001424 substituent group Chemical group 0.000 claims description 25
229910052784 alkaline earth metal Inorganic materials 0.000 claims description 23
JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 22
239000007788 liquid Substances 0.000 claims description 22
239000003208 petroleum Substances 0.000 claims description 22
239000004014 plasticizer Substances 0.000 claims description 22
150000003839 salts Chemical class 0.000 claims description 22
LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims description 21
125000001183 hydrocarbyl group Chemical class 0.000 claims description 21
125000004432 carbon atom Chemical group C* 0.000 claims description 20
150000007524 organic acids Chemical class 0.000 claims description 19
239000003973 paint Substances 0.000 claims description 19
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 18
CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 18
229920000620 organic polymer Polymers 0.000 claims description 18
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 17
230000002209 hydrophobic effect Effects 0.000 claims description 17
239000002480 mineral oil Substances 0.000 claims description 17
235000010446 mineral oil Nutrition 0.000 claims description 16
150000002894 organic compounds Chemical class 0.000 claims description 16
MTHSVFCYNBDYFN-UHFFFAOYSA-N anhydrous diethylene glycol Natural products OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 15
229910052791 calcium Inorganic materials 0.000 claims description 15
239000011575 calcium Substances 0.000 claims description 15
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 14
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical group [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 14
229920000642 polymer Polymers 0.000 claims description 14
229920002554 vinyl polymer Polymers 0.000 claims description 13
150000001412 amines Chemical class 0.000 claims description 12
235000005985 organic acids Nutrition 0.000 claims description 12
150000001408 amides Chemical class 0.000 claims description 11
150000002148 esters Chemical class 0.000 claims description 11
239000003112 inhibitor Substances 0.000 claims description 10
229910052783 alkali metal Inorganic materials 0.000 claims description 9
125000005907 alkyl ester group Chemical group 0.000 claims description 9
WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 9
238000006386 neutralization reaction Methods 0.000 claims description 9
XYLMUPLGERFSHI-UHFFFAOYSA-N alpha-Methylstyrene Chemical compound CC(=C)C1=CC=CC=C1 XYLMUPLGERFSHI-UHFFFAOYSA-N 0.000 claims description 8
229910019142 PO4 Inorganic materials 0.000 claims description 7
150000001340 alkali metals Chemical class 0.000 claims description 7
229910000019 calcium carbonate Inorganic materials 0.000 claims description 7
150000001735 carboxylic acids Chemical class 0.000 claims description 7
235000021317 phosphate Nutrition 0.000 claims description 7
229910052788 barium Inorganic materials 0.000 claims description 6
WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical class OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 claims description 5
150000001342 alkaline earth metals Chemical class 0.000 claims description 5
DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims description 5
150000007942 carboxylates Chemical class 0.000 claims description 4
150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 4
125000005498 phthalate group Chemical class 0.000 claims description 4
229920000058 polyacrylate Polymers 0.000 claims description 4
229920000728 polyester Polymers 0.000 claims description 4
CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical class OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 claims description 4
229920000178 Acrylic resin Polymers 0.000 claims description 2
239000004925 Acrylic resin Substances 0.000 claims description 2
150000004649 carbonic acid derivatives Chemical group 0.000 claims description 2
239000002270 dispersing agent Substances 0.000 claims description 2
239000000839 emulsion Substances 0.000 claims description 2
229920006243 acrylic copolymer Polymers 0.000 claims 5
AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Chemical compound [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 claims 4
125000003011 styrenyl group Chemical group [H]\C(*)=C(/[H])C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 claims 2
150000003871 sulfonates Chemical class 0.000 claims 2
125000004178 (C1-C4) alkyl group Chemical group 0.000 claims 1
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 1
WNLRTRBMVRJNCN-UHFFFAOYSA-L adipate(2-) Chemical compound [O-]C(=O)CCCCC([O-])=O WNLRTRBMVRJNCN-UHFFFAOYSA-L 0.000 claims 1
239000012752 auxiliary agent Substances 0.000 claims 1
AYJRCSIUFZENHW-DEQYMQKBSA-L barium(2+);oxomethanediolate Chemical compound [Ba+2].[O-][14C]([O-])=O AYJRCSIUFZENHW-DEQYMQKBSA-L 0.000 claims 1
QHIWVLPBUQWDMQ-UHFFFAOYSA-N butyl prop-2-enoate;methyl 2-methylprop-2-enoate;prop-2-enoic acid Chemical compound OC(=O)C=C.COC(=O)C(C)=C.CCCCOC(=O)C=C QHIWVLPBUQWDMQ-UHFFFAOYSA-N 0.000 claims 1
230000004927 fusion Effects 0.000 claims 1
229910052749 magnesium Inorganic materials 0.000 claims 1
239000011777 magnesium Substances 0.000 claims 1
229920001225 polyester resin Polymers 0.000 claims 1
239000004645 polyester resin Substances 0.000 claims 1
229920005672 polyolefin resin Polymers 0.000 claims 1
239000004814 polyurethane Substances 0.000 claims 1
229920002635 polyurethane Polymers 0.000 claims 1
229910052712 strontium Inorganic materials 0.000 claims 1
CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 claims 1
239000000463 material Substances 0.000 description 73
239000000126 substance Substances 0.000 description 56
239000002253 acid Substances 0.000 description 49
238000006243 chemical reaction Methods 0.000 description 33
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 27
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 25
230000002378 acidificating effect Effects 0.000 description 23
239000000047 product Substances 0.000 description 23
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 22
238000000034 method Methods 0.000 description 21
150000007513 acids Chemical class 0.000 description 20
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 18
238000005260 corrosion Methods 0.000 description 18
238000000576 coating method Methods 0.000 description 17
230000007797 corrosion Effects 0.000 description 17
DNIAPMSPPWPWGF-UHFFFAOYSA-N monopropylene glycol Natural products CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 14
125000000217 alkyl group Chemical group 0.000 description 13
238000003756 stirring Methods 0.000 description 13
150000003460 sulfonic acids Chemical class 0.000 description 13
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 12
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 12
239000011248 coating agent Substances 0.000 description 12
239000000243 solution Substances 0.000 description 12
BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 12
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 11
239000001569 carbon dioxide Substances 0.000 description 11
229910002092 carbon dioxide Inorganic materials 0.000 description 11
AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 10
229920001577 copolymer Polymers 0.000 description 10
239000012429 reaction media Substances 0.000 description 10
125000001931 aliphatic group Chemical group 0.000 description 9
239000000920 calcium hydroxide Substances 0.000 description 9
229910001861 calcium hydroxide Inorganic materials 0.000 description 9
239000000543 intermediate Substances 0.000 description 9
238000002360 preparation method Methods 0.000 description 9
239000000376 reactant Substances 0.000 description 9
239000011541 reaction mixture Substances 0.000 description 9
150000001298 alcohols Chemical class 0.000 description 8
150000001875 compounds Chemical class 0.000 description 8
229930195733 hydrocarbon Natural products 0.000 description 8
150000002739 metals Chemical class 0.000 description 8
239000011368 organic material Substances 0.000 description 8
230000008569 process Effects 0.000 description 8
239000007858 starting material Substances 0.000 description 8
UEEJHVSXFDXPFK-UHFFFAOYSA-N N-dimethylaminoethanol Chemical compound CN(C)CCO UEEJHVSXFDXPFK-UHFFFAOYSA-N 0.000 description 7
229960002887 deanol Drugs 0.000 description 7
239000012972 dimethylethanolamine Substances 0.000 description 7
239000002609 medium Substances 0.000 description 7
239000003921 oil Substances 0.000 description 7
239000000049 pigment Substances 0.000 description 7
239000002904 solvent Substances 0.000 description 7
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 6
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
241000158728 Meliaceae Species 0.000 description 6
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 6
235000011054 acetic acid Nutrition 0.000 description 6
239000000356 contaminant Substances 0.000 description 6
238000010438 heat treatment Methods 0.000 description 6
BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 6
150000002989 phenols Chemical class 0.000 description 6
229910052698 phosphorus Inorganic materials 0.000 description 6
239000011574 phosphorus Substances 0.000 description 6
229920002367 Polyisobutene Polymers 0.000 description 5
125000003118 aryl group Chemical group 0.000 description 5
230000015572 biosynthetic process Effects 0.000 description 5
239000000084 colloidal system Substances 0.000 description 5
239000011521 glass Substances 0.000 description 5
125000002887 hydroxy group Chemical group [H]O* 0.000 description 5
239000012071 phase Substances 0.000 description 5
238000010008 shearing Methods 0.000 description 5
KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 4
HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 4
POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 description 4
BFSVOASYOCHEOV-UHFFFAOYSA-N 2-diethylaminoethanol Chemical compound CCN(CC)CCO BFSVOASYOCHEOV-UHFFFAOYSA-N 0.000 description 4
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical group N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 4
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 4
229910000831 Steel Inorganic materials 0.000 description 4
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 description 4
125000005620 boronic acid group Chemical class 0.000 description 4
150000001732 carboxylic acid derivatives Chemical class 0.000 description 4
150000001924 cycloalkanes Chemical class 0.000 description 4
XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 4
POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 4
239000000945 filler Substances 0.000 description 4
150000004820 halides Chemical class 0.000 description 4
IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 4
238000000265 homogenisation Methods 0.000 description 4
230000002401 inhibitory effect Effects 0.000 description 4
ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 4
239000004816 latex Substances 0.000 description 4
229920000126 latex Polymers 0.000 description 4
239000001301 oxygen Substances 0.000 description 4
229910052760 oxygen Inorganic materials 0.000 description 4
IWDCLRJOBJJRNH-UHFFFAOYSA-N p-cresol Chemical compound CC1=CC=C(O)C=C1 IWDCLRJOBJJRNH-UHFFFAOYSA-N 0.000 description 4
FDPIMTJIUBPUKL-UHFFFAOYSA-N pentan-3-one Chemical compound CCC(=O)CC FDPIMTJIUBPUKL-UHFFFAOYSA-N 0.000 description 4
229920000098 polyolefin Polymers 0.000 description 4
229920005989 resin Polymers 0.000 description 4
239000011347 resin Substances 0.000 description 4
239000010959 steel Substances 0.000 description 4
238000012360 testing method Methods 0.000 description 4
DAFHKNAQFPVRKR-UHFFFAOYSA-N (3-hydroxy-2,2,4-trimethylpentyl) 2-methylpropanoate Chemical compound CC(C)C(O)C(C)(C)COC(=O)C(C)C DAFHKNAQFPVRKR-UHFFFAOYSA-N 0.000 description 3
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
SZIFAVKTNFCBPC-UHFFFAOYSA-N 2-chloroethanol Chemical compound OCCCl SZIFAVKTNFCBPC-UHFFFAOYSA-N 0.000 description 3
ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical compound CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 description 3
OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 3
QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 3
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 3
CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 3
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 3
239000004952 Polyamide Substances 0.000 description 3
239000004698 Polyethylene Substances 0.000 description 3
239000004743 Polypropylene Substances 0.000 description 3
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 3
238000013019 agitation Methods 0.000 description 3
125000003158 alcohol group Chemical group 0.000 description 3
150000008064 anhydrides Chemical class 0.000 description 3
150000001555 benzenes Chemical class 0.000 description 3
BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 description 3
ZFMQKOWCDKKBIF-UHFFFAOYSA-N bis(3,5-difluorophenyl)phosphane Chemical compound FC1=CC(F)=CC(PC=2C=C(F)C=C(F)C=2)=C1 ZFMQKOWCDKKBIF-UHFFFAOYSA-N 0.000 description 3
238000009835 boiling Methods 0.000 description 3
239000001110 calcium chloride Substances 0.000 description 3
229910001628 calcium chloride Inorganic materials 0.000 description 3
ZMRQTIAUOLVKOX-UHFFFAOYSA-L calcium;diphenoxide Chemical compound [Ca+2].[O-]C1=CC=CC=C1.[O-]C1=CC=CC=C1 ZMRQTIAUOLVKOX-UHFFFAOYSA-L 0.000 description 3
239000001913 cellulose Substances 0.000 description 3
229920002678 cellulose Polymers 0.000 description 3
235000014113 dietary fatty acids Nutrition 0.000 description 3
USIUVYZYUHIAEV-UHFFFAOYSA-N diphenyl ether Natural products C=1C=CC=CC=1OC1=CC=CC=C1 USIUVYZYUHIAEV-UHFFFAOYSA-N 0.000 description 3
238000001035 drying Methods 0.000 description 3
239000000194 fatty acid Substances 0.000 description 3
229930195729 fatty acid Natural products 0.000 description 3
235000019253 formic acid Nutrition 0.000 description 3
239000001257 hydrogen Substances 0.000 description 3
229910052739 hydrogen Inorganic materials 0.000 description 3
238000011065 in-situ storage Methods 0.000 description 3
150000002576 ketones Chemical class 0.000 description 3
150000002736 metal compounds Chemical class 0.000 description 3
238000002156 mixing Methods 0.000 description 3
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 description 3
239000000025 natural resin Substances 0.000 description 3
239000012188 paraffin wax Substances 0.000 description 3
235000019271 petrolatum Nutrition 0.000 description 3
229920002647 polyamide Polymers 0.000 description 3
229920000768 polyamine Polymers 0.000 description 3
229920000573 polyethylene Polymers 0.000 description 3
229920001223 polyethylene glycol Polymers 0.000 description 3
229920001155 polypropylene Polymers 0.000 description 3
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 3
AOHJOMMDDJHIJH-UHFFFAOYSA-N propylenediamine Chemical compound CC(N)CN AOHJOMMDDJHIJH-UHFFFAOYSA-N 0.000 description 3
238000010992 reflux Methods 0.000 description 3
239000008117 stearic acid Substances 0.000 description 3
229920003002 synthetic resin Polymers 0.000 description 3
230000009974 thixotropic effect Effects 0.000 description 3
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 3
239000001993 wax Substances 0.000 description 3
239000008096 xylene Substances 0.000 description 3
239000011701 zinc Substances 0.000 description 3
229910052725 zinc Inorganic materials 0.000 description 3
WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 2
OOCCDEMITAIZTP-QPJJXVBHSA-N (E)-cinnamyl alcohol Chemical compound OC\C=C\C1=CC=CC=C1 OOCCDEMITAIZTP-QPJJXVBHSA-N 0.000 description 2
WYUIWKFIFOJVKW-UHFFFAOYSA-N 1,2-dichloro-4-methylbenzene Chemical compound CC1=CC=C(Cl)C(Cl)=C1 WYUIWKFIFOJVKW-UHFFFAOYSA-N 0.000 description 2
QRMPKOFEUHIBNM-UHFFFAOYSA-N 1,4-dimethylcyclohexane Chemical compound CC1CCC(C)CC1 QRMPKOFEUHIBNM-UHFFFAOYSA-N 0.000 description 2
CHLICZRVGGXEOD-UHFFFAOYSA-N 1-Methoxy-4-methylbenzene Chemical compound COC1=CC=C(C)C=C1 CHLICZRVGGXEOD-UHFFFAOYSA-N 0.000 description 2
UAJRSHJHFRVGMG-UHFFFAOYSA-N 1-ethenyl-4-methoxybenzene Chemical compound COC1=CC=C(C=C)C=C1 UAJRSHJHFRVGMG-UHFFFAOYSA-N 0.000 description 2
VFPOSDWMSCLPHL-UHFFFAOYSA-N 2,3-dihexadecylnaphthalene-1-sulfonic acid Chemical class C1=CC=C2C(S(O)(=O)=O)=C(CCCCCCCCCCCCCCCC)C(CCCCCCCCCCCCCCCC)=CC2=C1 VFPOSDWMSCLPHL-UHFFFAOYSA-N 0.000 description 2
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