JPH0144839B2 - - Google Patents
Info
- Publication number
- JPH0144839B2 JPH0144839B2 JP57167733A JP16773382A JPH0144839B2 JP H0144839 B2 JPH0144839 B2 JP H0144839B2 JP 57167733 A JP57167733 A JP 57167733A JP 16773382 A JP16773382 A JP 16773382A JP H0144839 B2 JPH0144839 B2 JP H0144839B2
- Authority
- JP
- Japan
- Prior art keywords
- fabric
- ammonia
- treated
- thp
- impregnated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 143
- 239000004744 fabric Substances 0.000 claims description 116
- 229910021529 ammonia Inorganic materials 0.000 claims description 68
- 239000004753 textile Substances 0.000 claims description 36
- 238000000034 method Methods 0.000 claims description 26
- -1 tetrakis(hydroxymethyl)phosphonium compound Chemical class 0.000 claims description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 23
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 20
- 239000007864 aqueous solution Substances 0.000 claims description 10
- 239000004202 carbamide Substances 0.000 claims description 10
- 125000004029 hydroxymethyl group Chemical group [H]OC([H])([H])* 0.000 claims description 2
- NFHFRUOZVGFOOS-UHFFFAOYSA-N palladium;triphenylphosphane Chemical compound [Pd].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 NFHFRUOZVGFOOS-UHFFFAOYSA-N 0.000 claims 1
- 150000004714 phosphonium salts Chemical class 0.000 claims 1
- 238000011282 treatment Methods 0.000 description 28
- 238000004176 ammonification Methods 0.000 description 14
- 238000001723 curing Methods 0.000 description 14
- 238000009736 wetting Methods 0.000 description 11
- 238000001035 drying Methods 0.000 description 10
- 238000005470 impregnation Methods 0.000 description 9
- 239000000243 solution Substances 0.000 description 8
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 4
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- 235000011114 ammonium hydroxide Nutrition 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 229910052698 phosphorus Inorganic materials 0.000 description 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 239000010409 thin film Substances 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 229920000728 polyester Polymers 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 2
- UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 description 2
- 239000002759 woven fabric Substances 0.000 description 2
- NQPJDJVGBDHCAD-UHFFFAOYSA-N 1,3-diazinan-2-one Chemical compound OC1=NCCCN1 NQPJDJVGBDHCAD-UHFFFAOYSA-N 0.000 description 1
- NVHNGVXBCWYLFA-UHFFFAOYSA-N 1,3-diazinane-2-thione Chemical compound S=C1NCCCN1 NVHNGVXBCWYLFA-UHFFFAOYSA-N 0.000 description 1
- 229920003043 Cellulose fiber Polymers 0.000 description 1
- PDQAZBWRQCGBEV-UHFFFAOYSA-N Ethylenethiourea Chemical compound S=C1NCCN1 PDQAZBWRQCGBEV-UHFFFAOYSA-N 0.000 description 1
- 229920000877 Melamine resin Polymers 0.000 description 1
- 235000002597 Solanum melongena Nutrition 0.000 description 1
- 244000061458 Solanum melongena Species 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 238000005273 aeration Methods 0.000 description 1
- 150000007933 aliphatic carboxylic acids Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- JMXMXKRNIYCNRV-UHFFFAOYSA-N bis(hydroxymethyl)phosphanylmethanol Chemical compound OCP(CO)CO JMXMXKRNIYCNRV-UHFFFAOYSA-N 0.000 description 1
- OHJMTUPIZMNBFR-UHFFFAOYSA-N biuret Chemical compound NC(=O)NC(N)=O OHJMTUPIZMNBFR-UHFFFAOYSA-N 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 238000003763 carbonization Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000010981 drying operation Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 201000003373 familial cold autoinflammatory syndrome 3 Diseases 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- YAMHXTCMCPHKLN-UHFFFAOYSA-N imidazolidin-2-one Chemical compound O=C1NCCN1 YAMHXTCMCPHKLN-UHFFFAOYSA-N 0.000 description 1
- 238000011221 initial treatment Methods 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- OLAPPGSPBNVTRF-UHFFFAOYSA-N naphthalene-1,4,5,8-tetracarboxylic acid Chemical compound C1=CC(C(O)=O)=C2C(C(=O)O)=CC=C(C(O)=O)C2=C1C(O)=O OLAPPGSPBNVTRF-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229910000069 nitrogen hydride Inorganic materials 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000001384 succinic acid Substances 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- FAUOSXUSCVJWAY-UHFFFAOYSA-N tetrakis(hydroxymethyl)phosphanium Chemical group OC[P+](CO)(CO)CO FAUOSXUSCVJWAY-UHFFFAOYSA-N 0.000 description 1
- 230000004584 weight gain Effects 0.000 description 1
- 235000019786 weight gain Nutrition 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
- D06M11/59—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides with ammonia; with complexes of organic amines with inorganic substances
- D06M11/60—Ammonia as a gas or in solution
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/39—Aldehyde resins; Ketone resins; Polyacetals
- D06M15/423—Amino-aldehyde resins
- D06M15/43—Amino-aldehyde resins modified by phosphorus compounds
- D06M15/431—Amino-aldehyde resins modified by phosphorus compounds by phosphines or phosphine oxides; by oxides or salts of the phosphonium radical
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB8129272 | 1981-09-28 | ||
| GB8129272 | 1981-09-28 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5865069A JPS5865069A (ja) | 1983-04-18 |
| JPH0144839B2 true JPH0144839B2 (cg-RX-API-DMAC7.html) | 1989-09-29 |
Family
ID=10524791
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP57167733A Granted JPS5865069A (ja) | 1981-09-28 | 1982-09-28 | セルロ−ス性編織布の不燃化方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US4494951A (cg-RX-API-DMAC7.html) |
| EP (1) | EP0076138B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JPS5865069A (cg-RX-API-DMAC7.html) |
| KR (1) | KR880000926B1 (cg-RX-API-DMAC7.html) |
| AU (1) | AU559336B2 (cg-RX-API-DMAC7.html) |
| CA (1) | CA1199153A (cg-RX-API-DMAC7.html) |
| DE (1) | DE3274131D1 (cg-RX-API-DMAC7.html) |
| GB (1) | GB2106944B (cg-RX-API-DMAC7.html) |
| ZA (1) | ZA826861B (cg-RX-API-DMAC7.html) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4842609A (en) * | 1986-06-05 | 1989-06-27 | Burlington Industries, Inc. | Flame retardant treatments for polyester/cotton fabrics |
| US4748705A (en) * | 1986-06-05 | 1988-06-07 | Burlington Industries, Inc. | Flame resistant polyester/cotton fabric and process for its production |
| US4732789A (en) * | 1986-10-28 | 1988-03-22 | Burlington Industries, Inc. | Flame-resistant cotton blend fabrics |
| AU603391B2 (en) * | 1986-09-26 | 1990-11-15 | Burlington Industries, Inc. | Flame-resistant cotton blend fabrics |
| US5135541A (en) * | 1986-10-13 | 1992-08-04 | Albright & Wilson Limited | Flame retardant treatment of cellulose fabric with crease recovery: tetra-kis-hydroxy-methyl phosphonium and methylolamide |
| US5139531A (en) * | 1987-01-19 | 1992-08-18 | Albright & Wilson Limited | Fabric treatment processes |
| GB8713224D0 (en) * | 1987-06-05 | 1987-07-08 | Albright & Wilson | Textile treatment |
| JPH02234974A (ja) * | 1989-03-06 | 1990-09-18 | Koichi Nishimoto | 難燃化植物繊維材料の製造方法 |
| GB9004633D0 (en) | 1990-03-01 | 1990-04-25 | Albright & Wilson | Flame retardant composition and method of use |
| IL98728A0 (en) * | 1990-08-03 | 1992-07-15 | Pfersee Chem Fab | Flameproofing compositions containing phosphono compounds and organic acids |
| GB9017537D0 (en) * | 1990-08-10 | 1990-09-26 | Albright & Wilson | Cure unit |
| US5468545A (en) | 1994-09-30 | 1995-11-21 | Fleming; George R. | Long wear life flame-retardant cotton blend fabrics |
| AT401656B (de) * | 1994-11-07 | 1996-11-25 | Chemiefaser Lenzing Ag | Flammfestes nicht gewebtes textiles gebilde |
| US5766746A (en) * | 1994-11-07 | 1998-06-16 | Lenzing Aktiengesellschaft | Flame retardant non-woven textile article |
| US7741233B2 (en) * | 2006-08-10 | 2010-06-22 | Milliken & Company | Flame-retardant treatments for cellulose-containing fabrics and the fabrics so treated |
| US8012890B1 (en) | 2007-06-19 | 2011-09-06 | Milliken & Company | Flame resistant fabrics having a high synthetic content and process for making |
| US7713891B1 (en) | 2007-06-19 | 2010-05-11 | Milliken & Company | Flame resistant fabrics and process for making |
| GB2465819A (en) * | 2008-12-03 | 2010-06-09 | Rhodia Operations | Flame-retardant treatment of textile materials |
| US8174826B2 (en) | 2010-05-27 | 2012-05-08 | International Business Machines Corporation | Liquid cooling system for stackable modules in energy-efficient computing systems |
| EP2402416A1 (de) | 2010-06-30 | 2012-01-04 | Huntsman Textile Effects (Germany) GmbH | Flammschutzmittelzusammensetzung für Baumwollartikel |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB938989A (en) * | 1960-10-19 | 1963-10-09 | Albright & Wilson | Insolubilisation of further-polymerisable methylol-phosphorus polymeric materials |
| BE626626A (cg-RX-API-DMAC7.html) * | 1961-12-29 | |||
| DE1288556B (de) * | 1964-09-23 | 1969-02-06 | Hoechst Ag | Verfahren zum Flammfestmachen von Cellulosefasern |
| US3607356A (en) * | 1968-10-04 | 1971-09-21 | Us Agriculture | Imparting flame resistance to fibrous textiles from an alkaline medium |
| US3799738A (en) * | 1972-02-17 | 1974-03-26 | Hooker Chemical Corp | Flame retardant process for cellulosics |
| US4068026A (en) * | 1972-04-17 | 1978-01-10 | Hooker Chemicals & Plastics Corporation | Process for flame retarding cellulosics |
| US4123574A (en) * | 1972-04-17 | 1978-10-31 | Hooker Chemicals & Plastics Corp. | Process for flame retarding cellulosics |
| US4156747A (en) * | 1972-04-17 | 1979-05-29 | Hooker Chemicals & Plastics Corp. | Process for flame retarding cellulosics |
| GB1571617A (en) * | 1972-04-17 | 1980-07-16 | Hooker Chemicals Plastics Corp | Apparatus for flame retarding textile materials |
| US4154890A (en) * | 1972-04-17 | 1979-05-15 | Hooker Chemicals & Plastics Corp. | Process for imparting flame retardant property to cellulosic containing materials |
| US4137346A (en) * | 1972-04-17 | 1979-01-30 | Hooker Chemicals & Plastics Corp. | Flame retarding process for proteinaceous material |
| US3846155A (en) * | 1972-04-17 | 1974-11-05 | Hooker Chemical Corp | Flame retardant process for cellulosics |
| US4078101A (en) * | 1972-08-11 | 1978-03-07 | Albright & Wilson Ltd. | Flameproofing of textiles |
| GB1439608A (en) * | 1972-08-21 | 1976-06-16 | Albright & Wilson | Flameproofing of textiles |
| NL7701574A (nl) * | 1976-03-08 | 1977-09-12 | American Cyanamid Co | Vlamvertragende samenstellingen. |
| EP0023469B1 (de) * | 1979-07-16 | 1983-07-20 | Ciba-Geigy Ag | Nachbehandlung von mit Flammschutzmitteln veredelten, cellulosehaltigen Fasermaterialien mit flüssigem Ammoniak |
-
1982
- 1982-09-17 ZA ZA826861A patent/ZA826861B/xx unknown
- 1982-09-24 US US06/423,052 patent/US4494951A/en not_active Expired - Lifetime
- 1982-09-27 DE DE8282305097T patent/DE3274131D1/de not_active Expired
- 1982-09-27 AU AU88719/82A patent/AU559336B2/en not_active Expired
- 1982-09-27 GB GB08227473A patent/GB2106944B/en not_active Expired
- 1982-09-27 EP EP82305097A patent/EP0076138B1/en not_active Expired
- 1982-09-27 KR KR8204338A patent/KR880000926B1/ko not_active Expired
- 1982-09-28 JP JP57167733A patent/JPS5865069A/ja active Granted
- 1982-09-28 CA CA000412353A patent/CA1199153A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CA1199153A (en) | 1986-01-14 |
| GB2106944B (en) | 1985-08-07 |
| AU8871982A (en) | 1983-04-14 |
| US4494951A (en) | 1985-01-22 |
| EP0076138A3 (en) | 1984-01-11 |
| EP0076138B1 (en) | 1986-11-05 |
| JPS5865069A (ja) | 1983-04-18 |
| AU559336B2 (en) | 1987-03-05 |
| GB2106944A (en) | 1983-04-20 |
| ZA826861B (en) | 1983-07-27 |
| EP0076138A2 (en) | 1983-04-06 |
| DE3274131D1 (en) | 1986-12-11 |
| KR840001657A (ko) | 1984-05-16 |
| KR880000926B1 (ko) | 1988-05-31 |
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