JPH0118067B2 - - Google Patents

Info

Publication number
JPH0118067B2
JPH0118067B2 JP53094449A JP9444978A JPH0118067B2 JP H0118067 B2 JPH0118067 B2 JP H0118067B2 JP 53094449 A JP53094449 A JP 53094449A JP 9444978 A JP9444978 A JP 9444978A JP H0118067 B2 JPH0118067 B2 JP H0118067B2
Authority
JP
Japan
Prior art keywords
isocyanate
reaction
reaction mixture
solvent
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP53094449A
Other languages
English (en)
Japanese (ja)
Other versions
JPS5439018A (en
Inventor
Heiboaa Niko
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Akzo NV
Original Assignee
Akzo NV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Akzo NV filed Critical Akzo NV
Publication of JPS5439018A publication Critical patent/JPS5439018A/ja
Publication of JPH0118067B2 publication Critical patent/JPH0118067B2/ja
Granted legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/72—Copper
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/18—Separation; Purification; Stabilisation; Use of additives
    • C07C263/20—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
JP9444978A 1977-08-02 1978-08-02 Process for preparing isocyanate from formamide Granted JPS5439018A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL7708510 1977-08-02

Publications (2)

Publication Number Publication Date
JPS5439018A JPS5439018A (en) 1979-03-24
JPH0118067B2 true JPH0118067B2 (enExample) 1989-04-03

Family

ID=19828957

Family Applications (1)

Application Number Title Priority Date Filing Date
JP9444978A Granted JPS5439018A (en) 1977-08-02 1978-08-02 Process for preparing isocyanate from formamide

Country Status (6)

Country Link
US (1) US4207251A (enExample)
EP (1) EP0000602B1 (enExample)
JP (1) JPS5439018A (enExample)
CA (1) CA1117962A (enExample)
DE (1) DE2860856D1 (enExample)
IT (1) IT1097592B (enExample)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4430262A (en) * 1981-06-05 1984-02-07 Shell Oil Company Preparation of isocyanates and/or derivatives thereof
DE3229323A1 (de) * 1982-08-06 1984-02-09 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung aliphatischer isocyanate durch oxidative dehydrierung von formamiden
US4469640A (en) * 1983-03-14 1984-09-04 E. I. Du Pont De Nemours And Company Catalytic conversion of formamides to isocyanates
US4694101A (en) * 1984-08-09 1987-09-15 E. I. Du Pont De Nemours And Company Process for separating methyl isocyanate
US4824991A (en) * 1984-08-09 1989-04-25 E. I. Du Pont De Nemours And Company Process for separating methyl isocyanate
US4537726A (en) * 1984-11-09 1985-08-27 E. I. Du Pont De Nemours And Company Multi-stage process with adiabatic reactors for the preparation of isocyanates
US4698438A (en) * 1985-04-26 1987-10-06 E. I. Du Pont De Nemours And Company Process for the preparation of methyl carbamates and thioimidates
US4603016A (en) * 1985-11-14 1986-07-29 E. I. Du Pont De Nemours And Company Cryogenic brine separation of water and isocyanates
ATE46500T1 (de) * 1985-12-12 1989-10-15 Du Pont Verfahren zum abtrennen von methylisocyanat.
US4683329A (en) * 1986-04-16 1987-07-28 E. I. Dupont De Nemours And Company Beneficial use of water in catalytic conversion of formamides to isocyanates
US4795830A (en) * 1986-09-02 1989-01-03 E. I. Du Pont De Nemours And Company Use of water to inhibit decomposition of monoalkylformamides
US5126480A (en) * 1990-06-01 1992-06-30 Arco Chemical Technology, L.P. Isocyanate preparation
US5155267A (en) * 1991-10-24 1992-10-13 Arco Chemical Technology, L.P. Synthesis of isocyanate precursors from primary formamides
WO2010058430A1 (en) * 2008-11-24 2010-05-27 Reliance Life Sciences Pvt. Ltd. Process for the preparation of tetrazine derivatives
US8822718B2 (en) * 2009-12-01 2014-09-02 Basf Se Process for preparing isocyanates by thermally cleaving carbamates
PT2507206E (pt) 2009-12-04 2014-12-26 Basf Se Método para a produção de isocianatos
BR112013027184A2 (pt) * 2011-04-26 2016-12-27 Basf Se processo para produzir aldeídos c1-c10 por desidrogenação oxidativa de álcoois c1-c10 ao longo de um corpo catalisador moldado
CN107473989B (zh) * 2016-06-08 2020-04-28 中国科学院大连化学物理研究所 一种催化甲醇转化制氨基甲酸甲酯的方法
US20240336561A1 (en) 2021-06-28 2024-10-10 MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. Catalytic synthesis of free isocyanates
KR102806436B1 (ko) * 2024-03-29 2025-05-09 한화솔루션 주식회사 이소시아네이트 조성물, 이를 포함하는 광학렌즈 및 이를 이용한 이소시아네이트 조성물 보관방법

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3099673A (en) * 1959-08-19 1963-07-30 Bayer Ag Process for the production of organic isocyanates
US3277140A (en) * 1963-07-16 1966-10-04 Air Prod & Chem Preparation of aliphatic isocyanates
DE1277851B (de) 1966-04-20 1968-09-19 Bayer Ag Verfahren zur Herstellung von 2-Chlorcarbonylphenylisocyanaten
US3929859A (en) * 1974-11-18 1975-12-30 Standard Oil Co Ohio Manufacture of dinitriles from thiodinitriles
US3960914A (en) * 1975-05-06 1976-06-01 Sun Ventures, Inc. Conversion of formamides to isocyanates
DE2520219C3 (de) 1975-05-07 1983-02-24 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von Formaldehyd

Also Published As

Publication number Publication date
EP0000602B1 (en) 1981-07-22
IT1097592B (it) 1985-08-31
CA1117962A (en) 1982-02-09
US4207251A (en) 1980-06-10
IT7826324A0 (it) 1978-07-31
EP0000602A1 (en) 1979-02-07
JPS5439018A (en) 1979-03-24
DE2860856D1 (en) 1981-10-29

Similar Documents

Publication Publication Date Title
JPH0118067B2 (enExample)
US2942036A (en) Manufacture of halopropane
US4123466A (en) Process for nitrating aromatic hydrocarbons
JP3516322B2 (ja) １，１，１，３，３−ペンタフルオロプロパンの脱水方法
EP0648731B1 (fr) Procédé d'hydroxycarbonylation du butadiène
EP0242203B1 (en) Beneficial use of water in catalytic conversion of formamides to isocyanates
JPS6320218B2 (enExample)
JPS62221639A (ja) １，２−ジクロルエタンの製造法
RU2051892C1 (ru) Способ жидкофазного хлорирования 1,3-бутадиена
US3568408A (en) Continuous process for the recovery of useful components of a gaseous mixture formed in the catalytic production of cyanogen chloride from hydrocyanic acid and chlorine or in the subsequent trimerization of cyanogen chloride to cyanuric chloride in the vapor phase
US2917546A (en) Manufacture of sym-tetrafluoroacetone
JP3557624B2 (ja) ４，６−ジニトロハロベンゼンの製造方法
JP4241968B2 (ja) ジニトロトルエンの断熱製造法
RU2200729C2 (ru) Способ получения пергалоидированного циклопентена
US4603016A (en) Cryogenic brine separation of water and isocyanates
US3987150A (en) Production of ammonium nitrate
FR2515640A1 (fr) Procede de fabrication d'isocyanates aromatiques par carbonylation des derives nitres en presence de catalyseurs supportes prepares a partir de complexes heteropolymetalliques
US2870213A (en) Difluorochloroacetaldehyde and process
US3852356A (en) Production of aliphatic and cycloaliphatic alpha-nitroketones
US2847481A (en) Production of octachloromethylenecyclopentene
US3944656A (en) Process for the production of cyanogen chloride
US3923860A (en) Vapor phase chlorination of acetonitrile in the presence of water
RU2069211C1 (ru) Способ получения 1,2-дифтортрихлорэтана
US4255350A (en) Process for preparing methyl isocyanate
RU2156756C2 (ru) Способ получения гексафторацетона