JP7256600B2 - 電気化学的セルのためのバイポーラプレート並びにそれの製造方法 - Google Patents

電気化学的セルのためのバイポーラプレート並びにそれの製造方法 Download PDF

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JP7256600B2
JP7256600B2 JP2017522673A JP2017522673A JP7256600B2 JP 7256600 B2 JP7256600 B2 JP 7256600B2 JP 2017522673 A JP2017522673 A JP 2017522673A JP 2017522673 A JP2017522673 A JP 2017522673A JP 7256600 B2 JP7256600 B2 JP 7256600B2
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graphene oxide
coating
bipolar plate
reduction
graphene
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JP2018502214A (ja
JP2018502214A5 (https=
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ヴァイスベッカー・ヴィタリ
レーネルト・ヴェルナー
ライマー・ウーヴェ
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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/02—Details
    • H01M8/0202—Collectors; Separators, e.g. bipolar separators; Interconnectors
    • H01M8/0204—Non-porous and characterised by the material
    • H01M8/0206—Metals or alloys
    • H01M8/0208—Alloys
    • H01M8/021—Alloys based on iron
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/02—Details
    • H01M8/0202—Collectors; Separators, e.g. bipolar separators; Interconnectors
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B13/00—Diaphragms; Spacing elements
    • C25B13/04—Diaphragms; Spacing elements characterised by the material
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B13/00—Diaphragms; Spacing elements
    • C25B13/04—Diaphragms; Spacing elements characterised by the material
    • C25B13/05—Diaphragms; Spacing elements characterised by the material based on inorganic materials
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/60—Constructional parts of cells
    • C25B9/65—Means for supplying current; Electrode connections; Electric inter-cell connections
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/02—Details
    • H01M8/0202—Collectors; Separators, e.g. bipolar separators; Interconnectors
    • H01M8/0204—Non-porous and characterised by the material
    • H01M8/0223—Composites
    • H01M8/0228—Composites in the form of layered or coated products
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/50—Fuel cells
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50—Manufacturing or production processes characterised by the final manufactured product

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Sustainable Development (AREA)
  • General Chemical & Material Sciences (AREA)
  • Sustainable Energy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Composite Materials (AREA)
  • Inorganic Chemistry (AREA)
  • Fuel Cell (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Electrodes For Compound Or Non-Metal Manufacture (AREA)
  • Other Surface Treatments For Metallic Materials (AREA)
JP2017522673A 2014-11-03 2015-09-17 電気化学的セルのためのバイポーラプレート並びにそれの製造方法 Active JP7256600B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102014016186.2 2014-11-03
DE102014016186.2A DE102014016186A1 (de) 2014-11-03 2014-11-03 Bipolarplatte für elektrochemische Zellen sowie Verfahren zur Herstellung derselben
PCT/DE2015/000466 WO2016070862A1 (de) 2014-11-03 2015-09-17 Bipolarplatte für elektrochemische zellen sowie verfahren zur herstellung derselben

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JP2018502214A JP2018502214A (ja) 2018-01-25
JP2018502214A5 JP2018502214A5 (https=) 2022-11-01
JP7256600B2 true JP7256600B2 (ja) 2023-04-12

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US (1) US10418643B2 (https=)
EP (1) EP3216075B1 (https=)
JP (1) JP7256600B2 (https=)
CN (1) CN107210456A (https=)
CA (1) CA2965576C (https=)
DE (1) DE102014016186A1 (https=)
WO (1) WO2016070862A1 (https=)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106654315B (zh) * 2016-12-15 2019-03-05 大连理工大学 一种石墨烯增强表面的燃料电池用高性能双极板及其制备方法
DE102017204183A1 (de) 2017-03-14 2018-09-20 Robert Bosch Gmbh Bipolarplatte für eine Brennstoffzelle und Brennstoffzelle sowie Verfahren zur Herstellung einer Bipolarplatte
CN107425209B (zh) * 2017-06-20 2020-09-01 天津大学 一种铝制流场板的导电防腐涂层工艺
CN108199058B (zh) * 2017-12-15 2023-05-05 中国第一汽车股份有限公司 一种导电聚合物-石墨烯复合双极板的制备方法
CN109574004B (zh) * 2019-01-19 2022-09-20 青岛杜科新材料有限公司 膨胀石墨掺杂石墨烯制备高导电氢燃料电池双极板用低密度柔性石墨板的方法
CN109755605B (zh) * 2019-02-19 2021-04-30 中氢新能技术有限公司 基于石墨烯材料的燃料电池双极板、制备方法及甲醇重整燃料电池组
CN109904479A (zh) * 2019-02-22 2019-06-18 佛山科学技术学院 一种复合耐腐燃料电池金属双极板及其制备方法
CN111446461B (zh) * 2020-03-13 2021-05-28 浙江华熔科技有限公司 一种抗燃料电池中酸性介质腐蚀的石墨烯涂层制备方法
DE102020209811A1 (de) * 2020-08-04 2022-02-10 Robert Bosch Gesellschaft mit beschränkter Haftung Verfahren zur Reduzierung des Kontaktwiderstands zwischen einer Separatorplatte und einer Gasdiffusionslage einer Brennstoffzelle, Separatorplatte
DE102020210209A1 (de) 2020-08-12 2022-02-17 Ekpo Fuel Cell Technologies Gmbh Bipolarplatte, Brennstoffzelle und Verfahren zur Herstellung einer Bipolarplatte
CN116472625A (zh) * 2020-09-28 2023-07-21 海易森汽车股份有限公司 燃料电池金属双极板的耐久性的提高
US20220102737A1 (en) * 2020-09-28 2022-03-31 Hyzon Motors Inc. Enhanced durability of fuel cell metallic bipolar plate
CN113690456B (zh) * 2021-08-06 2022-07-22 米库玻璃纤维增强塑料泰州有限责任公司 用于燃料电池的高性能石墨烯双极板及其制备方法
CN114665102A (zh) * 2022-03-21 2022-06-24 北京氢沄新能源科技有限公司 一种燃料电池的金属双极板及其制备方法
DE102022108476A1 (de) 2022-04-07 2023-10-12 Ekpo Fuel Cell Technologies Gmbh Bipolarplatte, Brennstoffzelle und Verfahren zur Herstellung einer Bipolarplatte
CN114824586A (zh) * 2022-04-27 2022-07-29 昆明学院 一种锗/石墨烯复合材料作为阳极的锗空气电池制备方法
CN115011160A (zh) * 2022-06-21 2022-09-06 睿得新材料科技(佛山)有限公司 导电防腐涂料及制备方法和应用
DE102022214339A1 (de) * 2022-12-22 2024-06-27 Cellcentric Gmbh & Co. Kg Verfahren zum herstellen einer bipolarplatte für eine brennstoffzelle
CN116072906B (zh) * 2023-02-08 2025-01-24 深圳市氢瑞燃料电池科技有限公司 一种燃料电池钛基双极板及其制备方法
CN116154204B (zh) * 2023-02-23 2023-07-25 浙江菲尔特过滤科技股份有限公司 一种燃料电池板用碳膜涂层工艺
CN118073593B (zh) * 2024-04-15 2025-05-02 苏州适新金属科技有限公司 用于金属双极板的导电稳定涂层及其制备方法

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8758957B2 (en) * 2008-07-29 2014-06-24 GM Global Technology Operations LLC Graphene coated SS bipolar plates
US8871821B2 (en) * 2008-12-04 2014-10-28 Tyco Electronics Corporation Graphene and graphene oxide aerogels
US7977012B2 (en) * 2009-04-23 2011-07-12 GM Global Technology Operations LLC Method of coating a surface of a fuel cell plate
JP5612679B2 (ja) * 2009-06-09 2014-10-22 シバラジャン，ラメッシュ 燃料電池用バイポーラプレートの液体ベースナノ構造カーボン材料（ｎｃｍ）コーティング
US8226801B2 (en) * 2009-07-27 2012-07-24 Nanotek Instruments, Inc. Mass production of pristine nano graphene materials
CN101752561B (zh) * 2009-12-11 2012-08-22 宁波艾能锂电材料科技股份有限公司 石墨烯改性磷酸铁锂正极活性材料及其制备方法以及锂离子二次电池
WO2011116369A2 (en) * 2010-03-19 2011-09-22 Board Of Regents, The University Of Texas System Electrophoretic deposition and reduction of graphene oxide to make graphene film coatings and electrode structures
JP4886884B2 (ja) * 2010-07-20 2012-02-29 株式会社神戸製鋼所 チタン製燃料電池セパレータおよびその製造方法
KR101271249B1 (ko) * 2010-12-22 2013-06-10 한국과학기술원 질소가 도핑된 투명 그래핀 필름 및 이의 제조방법
CN105174252B (zh) * 2011-06-24 2018-12-14 株式会社半导体能源研究所 多层石墨烯及蓄电装置
WO2013024727A1 (en) * 2011-08-18 2013-02-21 Semiconductor Energy Laboratory Co., Ltd. Method for forming graphene and graphene oxide salt, and graphene oxide salt
CN104039695B (zh) * 2011-09-19 2018-06-05 卧龙岗大学 还原氧化石墨烯及其生产方法
KR102514830B1 (ko) * 2011-09-30 2023-03-30 가부시키가이샤 한도오따이 에네루기 켄큐쇼 양극, 리튬 이차 전지, 전기 자동차, 하이브리드 자동차, 이동체, 시스템, 및 전기 기기
US9487880B2 (en) * 2011-11-25 2016-11-08 Semiconductor Energy Laboratory Co., Ltd. Flexible substrate processing apparatus
KR101344216B1 (ko) * 2011-12-26 2013-12-23 한국생산기술연구원 그래핀을 이용한 고분자전해질 연료전지의 분리판 및 이의 제조방법
JP6122589B2 (ja) * 2012-07-20 2017-04-26 株式会社神戸製鋼所 燃料電池セパレータ
ES2708355T3 (es) 2013-11-19 2019-04-09 Tata Steel Uk Ltd Método para preparar una composición a base de grafeno
GB2521678A (en) * 2013-12-31 2015-07-01 Intelligent Energy Ltd Fuel cell flow plate

Non-Patent Citations (11)

* Cited by examiner, † Cited by third party
Title
国際公開第２０１３／０４７６３０号
特表２０１２－５２９７４９号公報
特表２０１３－５１３９０４号公報
特開２０１３－１２９９１３号公報
特開２０１７－０１７０３５号公報
特開２０１７－０８２３３２号公報
特開２０１８－０７６２２１号公報
米国特許出願公開第２０１１／０２２７０００号明細書
米国特許出願公開第２０１２／０１６１１９２号明細書
米国特許出願公開第２０１３／００４５１５６号明細書
韓国公開特許第１０－２０１３－００７４３４２号公報

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Publication number Publication date
WO2016070862A1 (de) 2016-05-12
EP3216075A1 (de) 2017-09-13
CA2965576C (en) 2023-07-11
DE102014016186A1 (de) 2016-05-04
US10418643B2 (en) 2019-09-17
CN107210456A (zh) 2017-09-26
JP2018502214A (ja) 2018-01-25
EP3216075B1 (de) 2025-05-28
EP3216075C0 (de) 2025-05-28
CA2965576A1 (en) 2016-05-12
US20170309925A1 (en) 2017-10-26

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