JP7082794B2 - 油性固形毛髪化粧料 - Google Patents
油性固形毛髪化粧料 Download PDFInfo
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- JP7082794B2 JP7082794B2 JP2018022835A JP2018022835A JP7082794B2 JP 7082794 B2 JP7082794 B2 JP 7082794B2 JP 2018022835 A JP2018022835 A JP 2018022835A JP 2018022835 A JP2018022835 A JP 2018022835A JP 7082794 B2 JP7082794 B2 JP 7082794B2
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- 239000007787 solid Substances 0.000 title claims description 51
- 239000003676 hair preparation Substances 0.000 title claims description 20
- 239000003921 oil Substances 0.000 claims description 37
- 239000002537 cosmetic Substances 0.000 claims description 26
- 239000001993 wax Substances 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 11
- -1 Polyethylene Polymers 0.000 claims description 9
- 239000010696 ester oil Substances 0.000 claims description 9
- 239000002253 acid Substances 0.000 claims description 8
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 8
- 239000000194 fatty acid Substances 0.000 claims description 8
- 229930195729 fatty acid Natural products 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 8
- 150000004665 fatty acids Chemical class 0.000 claims description 7
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 claims description 6
- OKTJSMMVPCPJKN-NJFSPNSNSA-N Carbon-14 Chemical compound [14C] OKTJSMMVPCPJKN-NJFSPNSNSA-N 0.000 claims description 4
- 150000001298 alcohols Chemical class 0.000 claims description 4
- 239000004200 microcrystalline wax Substances 0.000 claims description 4
- 235000019808 microcrystalline wax Nutrition 0.000 claims description 4
- 239000004698 Polyethylene Substances 0.000 claims description 2
- 229920001577 copolymer Polymers 0.000 claims description 2
- HQQADJVZYDDRJT-UHFFFAOYSA-N ethene;prop-1-ene Chemical group C=C.CC=C HQQADJVZYDDRJT-UHFFFAOYSA-N 0.000 claims description 2
- 125000003976 glyceryl group Chemical group [H]C([*])([H])C(O[H])([H])C(O[H])([H])[H] 0.000 claims description 2
- 239000012188 paraffin wax Substances 0.000 claims description 2
- 229920000573 polyethylene Polymers 0.000 claims description 2
- 235000019198 oils Nutrition 0.000 description 35
- 230000000694 effects Effects 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 6
- ULQISTXYYBZJSJ-UHFFFAOYSA-N 12-hydroxyoctadecanoic acid Chemical compound CCCCCCC(O)CCCCCCCCCCC(O)=O ULQISTXYYBZJSJ-UHFFFAOYSA-N 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 230000007547 defect Effects 0.000 description 4
- 229920001296 polysiloxane Polymers 0.000 description 4
- 235000015112 vegetable and seed oil Nutrition 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 239000004166 Lanolin Chemical class 0.000 description 3
- 240000007594 Oryza sativa Species 0.000 description 3
- 235000007164 Oryza sativa Nutrition 0.000 description 3
- 239000004359 castor oil Substances 0.000 description 3
- 235000019438 castor oil Nutrition 0.000 description 3
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 3
- 235000019388 lanolin Nutrition 0.000 description 3
- 229940039717 lanolin Drugs 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 235000009566 rice Nutrition 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- RKJGFHYCZPZJPE-UHFFFAOYSA-N 2,2-bis(16-methylheptadecanoyloxymethyl)butyl 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCC(=O)OCC(CC)(COC(=O)CCCCCCCCCCCCCCC(C)C)COC(=O)CCCCCCCCCCCCCCC(C)C RKJGFHYCZPZJPE-UHFFFAOYSA-N 0.000 description 2
- KIHBGTRZFAVZRV-UHFFFAOYSA-N 2-Hydroxyoctadecanoic acid Natural products CCCCCCCCCCCCCCCCC(O)C(O)=O KIHBGTRZFAVZRV-UHFFFAOYSA-N 0.000 description 2
- NCLNAHJFXIKYBY-UHFFFAOYSA-N 2-hexyldecyl 16-methylheptadecanoate Chemical compound CCCCCCCCC(CCCCCC)COC(=O)CCCCCCCCCCCCCCC(C)C NCLNAHJFXIKYBY-UHFFFAOYSA-N 0.000 description 2
- 240000001548 Camellia japonica Species 0.000 description 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 2
- 239000004743 Polypropylene Substances 0.000 description 2
- 235000021355 Stearic acid Nutrition 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 235000013871 bee wax Nutrition 0.000 description 2
- 239000012166 beeswax Substances 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 235000018597 common camellia Nutrition 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000004205 dimethyl polysiloxane Substances 0.000 description 2
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 2
- 239000011737 fluorine Substances 0.000 description 2
- 229910052731 fluorine Inorganic materials 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 230000001771 impaired effect Effects 0.000 description 2
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 2
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 2
- 229940062000 polyglyceryl-2 triisostearate Drugs 0.000 description 2
- 229920001155 polypropylene Polymers 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 241000894007 species Species 0.000 description 2
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 2
- 239000008117 stearic acid Substances 0.000 description 2
- 229940118594 trimethylolpropane triisostearate Drugs 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- ALSTYHKOOCGGFT-KTKRTIGZSA-N (9Z)-octadecen-1-ol Chemical compound CCCCCCCC\C=C/CCCCCCCCO ALSTYHKOOCGGFT-KTKRTIGZSA-N 0.000 description 1
- ICHWOIDNXFYVKZ-UHFFFAOYSA-N 1-(16-methylheptadecanoyloxy)propyl 16-methylheptadecanoate Chemical compound CCC(OC(=O)CCCCCCCCCCCCCCC(C)C)OC(=O)CCCCCCCCCCCCCCC(C)C ICHWOIDNXFYVKZ-UHFFFAOYSA-N 0.000 description 1
- 229940114072 12-hydroxystearic acid Drugs 0.000 description 1
- ABEXEQSGABRUHS-UHFFFAOYSA-N 16-methylheptadecyl 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCCOC(=O)CCCCCCCCCCCCCCC(C)C ABEXEQSGABRUHS-UHFFFAOYSA-N 0.000 description 1
- BGRXBNZMPMGLQI-UHFFFAOYSA-N 2-octyldodecyl tetradecanoate Chemical compound CCCCCCCCCCCCCC(=O)OCC(CCCCCCCC)CCCCCCCCCC BGRXBNZMPMGLQI-UHFFFAOYSA-N 0.000 description 1
- BRORPGSJXSLXKN-UHFFFAOYSA-N 6-methylheptyl 3,5,5-trimethylhexanoate Chemical compound CC(C)CCCCCOC(=O)CC(C)CC(C)(C)C BRORPGSJXSLXKN-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- XMSXQFUHVRWGNA-UHFFFAOYSA-N Decamethylcyclopentasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 XMSXQFUHVRWGNA-UHFFFAOYSA-N 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 240000007049 Juglans regia Species 0.000 description 1
- 235000009496 Juglans regia Nutrition 0.000 description 1
- 244000062730 Melissa officinalis Species 0.000 description 1
- 235000010654 Melissa officinalis Nutrition 0.000 description 1
- 239000004909 Moisturizer Substances 0.000 description 1
- 235000021314 Palmitic acid Nutrition 0.000 description 1
- 229920002367 Polyisobutene Polymers 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- LPGFSDGXTDNTCB-UHFFFAOYSA-N [3-(16-methylheptadecanoyloxy)-2,2-bis(16-methylheptadecanoyloxymethyl)propyl] 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCC(=O)OCC(COC(=O)CCCCCCCCCCCCCCC(C)C)(COC(=O)CCCCCCCCCCCCCCC(C)C)COC(=O)CCCCCCCCCCCCCCC(C)C LPGFSDGXTDNTCB-UHFFFAOYSA-N 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000010775 animal oil Substances 0.000 description 1
- 239000002518 antifoaming agent Substances 0.000 description 1
- KQZNFGJQTPAURD-NBWQQBAWSA-N ascorbyl dipalmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](OC(=O)CCCCCCCCCCCCCCC)[C@H]1OC(=O)C(O)=C1O KQZNFGJQTPAURD-NBWQQBAWSA-N 0.000 description 1
- 239000004204 candelilla wax Substances 0.000 description 1
- 235000013868 candelilla wax Nutrition 0.000 description 1
- 229940073532 candelilla wax Drugs 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000004203 carnauba wax Substances 0.000 description 1
- 235000013869 carnauba wax Nutrition 0.000 description 1
- 229960000541 cetyl alcohol Drugs 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- IUJAMGNYPWYUPM-UHFFFAOYSA-N hentriacontane Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCC IUJAMGNYPWYUPM-UHFFFAOYSA-N 0.000 description 1
- XJNUECKWDBNFJV-UHFFFAOYSA-N hexadecyl 2-ethylhexanoate Chemical compound CCCCCCCCCCCCCCCCOC(=O)C(CC)CCCC XJNUECKWDBNFJV-UHFFFAOYSA-N 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229940060384 isostearyl isostearate Drugs 0.000 description 1
- 229940119170 jojoba wax Drugs 0.000 description 1
- 239000000865 liniment Substances 0.000 description 1
- 229940057995 liquid paraffin Drugs 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000001333 moisturizer Effects 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 description 1
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 description 1
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 1
- HMMGMWAXVFQUOA-UHFFFAOYSA-N octamethylcyclotetrasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 HMMGMWAXVFQUOA-UHFFFAOYSA-N 0.000 description 1
- 229940073665 octyldodecyl myristate Drugs 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 229940055577 oleyl alcohol Drugs 0.000 description 1
- XMLQWXUVTXCDDL-UHFFFAOYSA-N oleyl alcohol Natural products CCCCCCC=CCCCCCCCCCCO XMLQWXUVTXCDDL-UHFFFAOYSA-N 0.000 description 1
- 239000004006 olive oil Substances 0.000 description 1
- 235000008390 olive oil Nutrition 0.000 description 1
- 239000010702 perfluoropolyether Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 229920001083 polybutene Polymers 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 210000004761 scalp Anatomy 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 229940032094 squalane Drugs 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- BPCXHCSZMTWUBW-UHFFFAOYSA-N triethoxy(1,1,2,2,3,3,4,4,5,5,8,8,8-tridecafluorooctyl)silane Chemical compound CCO[Si](OCC)(OCC)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)CCC(F)(F)F BPCXHCSZMTWUBW-UHFFFAOYSA-N 0.000 description 1
- VLPFTAMPNXLGLX-UHFFFAOYSA-N trioctanoin Chemical compound CCCCCCCC(=O)OCC(OC(=O)CCCCCCC)COC(=O)CCCCCCC VLPFTAMPNXLGLX-UHFFFAOYSA-N 0.000 description 1
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 1
- 229940099259 vaseline Drugs 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 235000020234 walnut Nutrition 0.000 description 1
Description
料が上記目的を達成できることを見出し、本発明を完成するに至った。
(A)分岐鎖を持つワックス
(B)分子量が250以上であって炭素14以上の脂肪酸と分岐高級アルコールからなる
25℃で液状のエステル油から選択される一種又は二種以上
(C)成分(A)以外の固形油から選択される一種又は二種以上
(A)分岐鎖を持つワックス 油性固形毛髪化粧料全量に対し2.0~5.0質量%
(B)分子量が250以上であって炭素14以上の脂肪酸と分岐高級アルコールからなる
25℃で液状のエステル油から選択される一種又は二種以上
油性固形毛髪化粧料全量に対し10.0~15.0質量%
(C)成分(A)以外の固形油から選択される一種又は二種以上
油性固形毛髪化粧料全量に対し20.0~30.0質量%
各実施例および各比較例で得られた油性固形毛髪化粧料を、長さ10cm、重さ1gに調整した毛束に塗布し、30℃湿度90%の高湿度下状態で2時間放置し、塗布直後から高湿度下2時間後までの髪の広がりを測定し、下記基準に従って評価した。
<評価基準>
〇:髪の広がりが10.0mm未満で、殆ど髪の広がりが認められない
△:髪の広がりが10.0mm以上20.0mm未満で、やや髪の広がりが認められる
×:髪の広がりが20.0mm以上で、明らかな髪の広がりが認められる
各成分を90℃以上で溶解させ、均一混合を行い、ポリプロピレン容器(直径35mm、
深さ15mm)に流し込み、引抜強度測定用治具を容器中央部に差し入れ冷却し、引抜強度測定用治具を油性固形毛髪化粧料に固定する。その後、A&D社製フォーステスターMCT-2150を用いて、油性固形毛髪化粧料を300mm/min.の速度で引っ張り、ポリプロピレン容器から油性固形毛髪化粧料が引き剥がされる際の力を計測。本測定値が30.0N未満であった場合、離型性が良好とした。
10名の被験者によって25℃に保たれた室内で、各実施例および各比較例で得られた油性固形毛髪化粧料を、長さ10cm、重さ5gに調整した毛束に塗布し、塗布時の伸びの良さを下記基準に従って評価した。
<評価基準>
◎:被験者の8名以上が塗布時の伸びが良いと判断
〇:被験者の6名以上が塗布時の伸びが良いと判断
△:被験者の4名以上6名未満が塗布時の伸びが良いと判断
×:被験者の4名未満が塗布時の伸びが良いと判断
50℃の恒温槽に1週間より保存した各油性固形毛髪化粧料を取出し、直ちに上蓋を取り、下記基準に従って、各組成物を目視により評価した。
<評価基準>
◎:外観に全く変化は見られず、折れや欠損もない
〇:折れや欠損はないが、外観に僅かな変化が見られる
△:外観の変化が認められ、折れや欠損がある
×:組成物が溶け出し、容器の外部に漏れ出ている。
表1および表2に記載の油性固形毛髪化粧料を常法により調製し、耐圧容器に充填した後、前記各種試験を実施して評価を行なった。その結果を表1および表2に併せて示す。
配合量(質量%)
(1)マイクロクリスタリンワックス 3.0
(2)ミリスチン酸オクチルドデシル 12.0
(3)コメヌカロウ 10.0
(4)ミツロウ 15.0
(5)ヒマシ油 52.29
(6)コメ胚芽油 2.0
(7)ツバキ種子油 1.0
(8)クルミ種子油 1.0
(9)ユチャ種子油 3.0
(10)ジパルミチン酸アスコルビル 0.2
(11)パラメトキシケイ皮酸エチルヘキシル 0.01
(13)香料 0.5
上記組成の油性固形毛髪化粧料は、常法に従い、80~100℃で加熱・溶融した油性成分を充分に攪拌混合し、溶融状態で、容器、樹脂又は金属等のモールド等に充填し、放冷して製造した。
Claims (1)
- 下記成分(A)~(C)を含有し、成分(A)~(B)の配合量が下記であることを特徴とする油性固形毛髪化粧料。
(A)ポリエチレンワックス、(エチレン/プロピレン)コポリマー、マイクロクリスタリンワックス、パラフィンワックス、トリ(ベヘン酸/イソステアリン酸/エイコサンニ酸)グリセリル
油性固形毛髪化粧料全量に対し2.0~5.0質量%
(B)分子量が250以上であって炭素14以上の脂肪酸と分岐高級アルコールからなる25℃で液状のエステル油から選択される一種又は二種以上
油性固形毛髪化粧料全量に対し10.0~15.0質量%
(C)成分(A)以外のロウ類又は硬化油類からなる固形油から選択される一種又は二種以上
油性固形毛髪化粧料全量に対し20.0~30.0質量%
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JP7082794B2 true JP7082794B2 (ja) | 2022-06-09 |
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JP2002302415A (ja) | 2001-02-01 | 2002-10-18 | Shiseido Co Ltd | 油性固型化粧料 |
JP2008094790A (ja) | 2006-10-13 | 2008-04-24 | Nippon Shikizai Inc | 棒状油性固形化粧料 |
JP2009235007A (ja) | 2008-03-27 | 2009-10-15 | Kose Corp | 油性化粧料 |
WO2010087004A1 (ja) | 2009-01-30 | 2010-08-05 | 高級アルコール工業株式会社 | 油性毛髪化粧料 |
JP2010202621A (ja) | 2009-03-06 | 2010-09-16 | Kracie Home Products Ltd | 整髪料 |
JP2010235759A (ja) | 2009-03-31 | 2010-10-21 | Kose Corp | 油性固形香料組成物 |
JP2015101581A (ja) | 2013-11-28 | 2015-06-04 | 日本メナード化粧品株式会社 | 油性固形化粧料 |
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2018
- 2018-02-13 JP JP2018022835A patent/JP7082794B2/ja active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
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