JP6658747B2 - エポキシ樹脂組成物、プリプレグ、繊維強化プラスチック材料および繊維強化プラスチック材料の製造方法 - Google Patents
エポキシ樹脂組成物、プリプレグ、繊維強化プラスチック材料および繊維強化プラスチック材料の製造方法 Download PDFInfo
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- JP6658747B2 JP6658747B2 JP2017518306A JP2017518306A JP6658747B2 JP 6658747 B2 JP6658747 B2 JP 6658747B2 JP 2017518306 A JP2017518306 A JP 2017518306A JP 2017518306 A JP2017518306 A JP 2017518306A JP 6658747 B2 JP6658747 B2 JP 6658747B2
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- SOLNRIROLBHRDJ-UHFFFAOYSA-N propyl 3-nitrobenzoate Chemical compound CCCOC(=O)C1=CC=CC([N+]([O-])=O)=C1 SOLNRIROLBHRDJ-UHFFFAOYSA-N 0.000 description 1
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- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
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- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 125000000297 undecanoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
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- 238000009849 vacuum degassing Methods 0.000 description 1
- 125000003774 valeryl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/4007—Curing agents not provided for by the groups C08G59/42 - C08G59/66
- C08G59/4014—Nitrogen containing compounds
- C08G59/4021—Ureas; Thioureas; Guanidines; Dicyandiamides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/42—Polycarboxylic acids; Anhydrides, halides or low molecular weight esters thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/42—Polycarboxylic acids; Anhydrides, halides or low molecular weight esters thereof
- C08G59/4223—Polycarboxylic acids; Anhydrides, halides or low molecular weight esters thereof aromatic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/50—Amines
- C08G59/5046—Amines heterocyclic
- C08G59/5053—Amines heterocyclic containing only nitrogen as a heteroatom
- C08G59/5073—Amines heterocyclic containing only nitrogen as a heteroatom having two nitrogen atoms in the ring
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/62—Alcohols or phenols
- C08G59/621—Phenols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/24—Impregnating materials with prepolymers which can be polymerised in situ, e.g. manufacture of prepregs
- C08J5/241—Impregnating materials with prepolymers which can be polymerised in situ, e.g. manufacture of prepregs using inorganic fibres
- C08J5/243—Impregnating materials with prepolymers which can be polymerised in situ, e.g. manufacture of prepregs using inorganic fibres using carbon fibres
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/24—Impregnating materials with prepolymers which can be polymerised in situ, e.g. manufacture of prepregs
- C08J5/249—Impregnating materials with prepolymers which can be polymerised in situ, e.g. manufacture of prepregs characterised by the additives used in the prepolymer mixture
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2363/00—Characterised by the use of epoxy resins; Derivatives of epoxy resins
- C08J2363/02—Polyglycidyl ethers of bis-phenols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2429/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal, or ketal radical; Hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Derivatives of such polymer
- C08J2429/14—Homopolymers or copolymers of acetals or ketals obtained by polymerisation of unsaturated acetals or ketals or by after-treatment of polymers of unsaturated alcohols
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Epoxy Resins (AREA)
- Reinforced Plastic Materials (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (5)
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| US201462086428P | 2014-12-02 | 2014-12-02 | |
| US62/086,428 | 2014-12-02 | ||
| US201562248012P | 2015-10-29 | 2015-10-29 | |
| US62/248,012 | 2015-10-29 | ||
| PCT/IB2015/002421 WO2016087935A1 (en) | 2014-12-02 | 2015-12-01 | Epoxy resin composition, prepreg, fiber-reinforced plastic material, and manufacturing method for fiber-reinforced plastic material |
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| JP2017536441A JP2017536441A (ja) | 2017-12-07 |
| JP2017536441A5 JP2017536441A5 (enExample) | 2020-01-16 |
| JP6658747B2 true JP6658747B2 (ja) | 2020-03-04 |
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| GB201514516D0 (en) * | 2015-08-14 | 2015-09-30 | Cytec Ind Inc | Fast-cure pre-preg |
| GB201515715D0 (en) * | 2015-09-04 | 2015-10-21 | Gurit Uk Ltd | Prepregs and production of composite material using prepregs |
| CN108473660B (zh) * | 2016-01-19 | 2021-06-25 | 三菱化学株式会社 | 环氧树脂组合物、纤维增强复合材料用预浸料及纤维增强复合材料 |
| US11168189B2 (en) | 2016-06-27 | 2021-11-09 | Dow Global Technologies Llc | Storage stable epoxy prepregs from dicyandiamide solutions and methods for making the same |
| KR102428285B1 (ko) * | 2016-09-13 | 2022-08-08 | 주식회사 테크위드 | 자전거 림을 위한 고온 수지 조성물 및 이를 이용한 자전거 림 |
| FR3071789B1 (fr) * | 2017-10-04 | 2020-07-17 | Valeo Systemes Thermiques | Boitier de support pour batterie |
| WO2019098028A1 (ja) * | 2017-11-16 | 2019-05-23 | 三菱ケミカル株式会社 | 熱硬化性樹脂組成物、プリプレグ、ならびに繊維強化複合材料およびその製造方法 |
| GB2569614B (en) | 2017-12-21 | 2022-04-06 | Hexcel Composites Ltd | A curative composition and a resin composition containing the curative composition |
| TR201722994A2 (tr) * | 2017-12-29 | 2019-07-22 | Kordsa Teknik Tekstil As | Bi̇r sicak eri̇yi̇k epoksi̇ reçi̇ne si̇stemi̇ ve yapimi i̇çi̇n proses |
| JP7209470B2 (ja) | 2018-03-13 | 2023-01-20 | 帝人株式会社 | プリプレグ及び炭素繊維強化複合材料 |
| CN108410134B (zh) * | 2018-03-29 | 2021-04-20 | 苏州银禧新能源复合材料有限公司 | 一种纤维复合材料用环氧树脂组合物及其应用 |
| GB2576875B (en) * | 2018-08-30 | 2022-08-31 | Hexcel Composites Ltd | Improvements in or relating to curing agents |
| JP7178850B2 (ja) * | 2018-09-28 | 2022-11-28 | 日鉄ケミカル＆マテリアル株式会社 | 繊維強化複合材料用エポキシ樹脂組成物、繊維強化複合材料及び成形体 |
| GB2580087B (en) * | 2018-12-20 | 2022-09-07 | Hexcel Composites Ltd | Improved thermocurable moulding process |
| CN113474393B (zh) * | 2019-02-26 | 2024-01-16 | 富士胶片株式会社 | 内窥镜用粘接剂及其固化物、以及内窥镜及其制造方法 |
| GB201905741D0 (en) | 2019-04-24 | 2019-06-05 | Hexcel Composites Ltd | Improvements in or relating to curatives |
| GB201911998D0 (en) * | 2019-08-21 | 2019-10-02 | Hexcel Composites Ltd | Improved thermocurable moulding process |
| CN111138636A (zh) * | 2019-12-31 | 2020-05-12 | 浙江华正新材料股份有限公司 | 一种树脂组合物、预浸料及层压板 |
| JPWO2023053834A1 (enExample) * | 2021-09-29 | 2023-04-06 | ||
| KR102789355B1 (ko) * | 2023-01-10 | 2025-04-03 | 한국화학연구원 | 디카르복실산을 이용하여 제조된 고유연성 경화제를 포함하는 에폭시 수지 조성물 및 이의 경화물 |
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| US20030082385A1 (en) * | 2001-07-13 | 2003-05-01 | Toray Composites (America), Inc. | Quick cure carbon fiber reinforced epoxy resin |
| JP2008174577A (ja) * | 2007-01-16 | 2008-07-31 | Kyocera Chemical Corp | ダイボンディングペーストおよびそれを用いた半導体装置 |
| JP5243441B2 (ja) * | 2007-09-21 | 2013-07-24 | 日本曹達株式会社 | 包接錯体を含有する半導体封止用エポキシ樹脂組成物 |
| JP5357576B2 (ja) * | 2009-02-27 | 2013-12-04 | パナソニック株式会社 | 半導体封止用エポキシ樹脂組成物、及び半導体装置 |
| US20130059942A1 (en) * | 2010-05-21 | 2013-03-07 | Nippon Soda Co., Ltd. | Curable powder coating composition, and cured product of same |
| JP5660443B2 (ja) * | 2010-08-06 | 2015-01-28 | 大日本印刷株式会社 | 粘接着シートおよびそれを用いた接着方法 |
| JP5902494B2 (ja) * | 2012-01-30 | 2016-04-13 | 日本曹達株式会社 | 硬化性粉体塗料組成物及びその硬化物 |
| JP2013213168A (ja) * | 2012-04-04 | 2013-10-17 | Nippon Soda Co Ltd | プリプレグ用エポキシ樹脂組成物 |
| TWI621639B (zh) * | 2013-01-07 | 2018-04-21 | 東麗股份有限公司 | 環氧樹脂組成物及預浸漬物 |
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- 2015-12-01 CN CN201580065618.9A patent/CN107001594B/zh not_active Expired - Fee Related
- 2015-12-01 WO PCT/IB2015/002421 patent/WO2016087935A1/en not_active Ceased
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- 2015-12-01 US US15/532,385 patent/US20170362376A1/en not_active Abandoned
- 2015-12-01 JP JP2017518306A patent/JP6658747B2/ja not_active Expired - Fee Related
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| Publication number | Publication date |
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| US20170362376A1 (en) | 2017-12-21 |
| KR20170091639A (ko) | 2017-08-09 |
| EP3230339A1 (en) | 2017-10-18 |
| WO2016087935A1 (en) | 2016-06-09 |
| EP3230339A4 (en) | 2018-06-27 |
| EP3230339B1 (en) | 2022-03-23 |
| JP2017536441A (ja) | 2017-12-07 |
| CN107001594B (zh) | 2019-07-23 |
| CN107001594A (zh) | 2017-08-01 |
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