JP6494618B2 - 不燃性で、吸音性で、断熱性のジオポリマー発泡部材用のジオポリマー発泡調製物 - Google Patents
不燃性で、吸音性で、断熱性のジオポリマー発泡部材用のジオポリマー発泡調製物 Download PDFInfo
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- JP6494618B2 JP6494618B2 JP2016527468A JP2016527468A JP6494618B2 JP 6494618 B2 JP6494618 B2 JP 6494618B2 JP 2016527468 A JP2016527468 A JP 2016527468A JP 2016527468 A JP2016527468 A JP 2016527468A JP 6494618 B2 JP6494618 B2 JP 6494618B2
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- alkali metal
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- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 239000005049 silicon tetrachloride Substances 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- GBPOWOIWSYUZMH-UHFFFAOYSA-N sodium;trihydroxy(methyl)silane Chemical compound [Na+].C[Si](O)(O)O GBPOWOIWSYUZMH-UHFFFAOYSA-N 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 239000002341 toxic gas Substances 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N urea group Chemical group NC(=O)N XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 239000010455 vermiculite Substances 0.000 description 1
- 229910052902 vermiculite Inorganic materials 0.000 description 1
- 235000019354 vermiculite Nutrition 0.000 description 1
- 239000011800 void material Substances 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 150000003751 zinc Chemical class 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
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Description
a) 少なくとも1種の無機の石材形成する反応成分と、この少なくとも1種の無機の石材形成する反応成分の硬化反応をアルカリ性領域で引き起こす少なくとも1種の水含有硬化剤と、少なくとも1種の発泡剤、少なくとも1種の有機ケイ素化合物及び少なくとも1種の界面活性剤とを混合する工程、並びに
b) この混合物を少なくとも部分的に硬化させる工程
を有する無機有機ハイブリッド発泡体の製造方法が記載されている。ただし、ここでは純粋に無機発泡体は形成されない。
高炉スラグ3〜60質量%、好ましくは5〜50質量%、
マイクロシリカ及び/又はメタカオリン3〜70質量%、好ましくは5〜50質量%、
フライアッシュ0〜50質量%、
アルカリ性活性剤(固形分として計算)1〜55質量%、
水(全体量)10〜60質量%、
並びに界面活性剤、気相及び場合により他の添加剤を含むことができる。
無機結合材20〜75質量%、
アルカリ性活性剤(固形分として計算)3〜50質量%、
水(全体量)10〜50質量%、
並びに界面活性剤、気相及び場合により他の添加剤を含むことができる。
無機結合材20〜50質量%、
アルカリ性活性剤(固形分として計算)5〜25質量%、
水(全体量)10〜40質量%、
並びに界面活性剤、気相及び場合により他の添加剤を含むことができる。
実施例1:メタカオリンとフライアッシュとからのジオポリマー発泡体の製造
表1に記載された成分:
乾燥見掛け密度:274kg/m3
14日後の早期強度:0.12〜0.24MPa
28日以降の最終密度:1.2MPa
熱伝導率:46〜48mW/mK
乾燥見掛け密度:261kg/m3
7日後の早期強度:1.2MPa
28日以降の最終密度:3.3MPa
熱伝導率:50mW/mK
乾燥粗製密度:270kg/m3
28日以降の最終密度:1.4MPa
熱伝導性:47〜48mW/mK
実施例3により製造された厚さ40mmのジオポリマー発泡部材の、クントの管中での垂直の音波入射の際の吸音率の推移は、図1に示されている。
実施例1を、表4に記載された成分で繰り返した。
この配合を、表5に記載されたように変更して繰り返した。それぞれ900mlの気泡容量にまで発泡させた。スランプ測定は、DIN EN 1015-3に準拠して決定した。
a) 振動による発泡:
振動による発泡のために、beta Mischtechnik GmbH社(Essen)の装置を使用した。この発泡プロセスを、円形の横断面を有しかつ相互に結合されている円柱状に形成された室からなる混合ヘッド中で実施した。各室は2つの交換可能な混合エレメントを有し、この混合エレメントは、好ましくは適合する多孔板を備えていた。この混合ヘッドユニットは、7.2リットルの容積を有し、かつ1つ以上のポンプに出発材料若しくは添加物のそれぞれのスラリー及び圧縮空気を供給し、50〜70Hzの振動周波数で運転した。この方法及び装置は、EP 1716915 B1に詳細に記載されている。この装置を用いて、1100〜1700g/lの密度を示すスラリーを100〜500g/lの見掛け密度を示す発泡体に発泡させることができた。この処理量は約150l/hであった。
発泡を、ロータ/ステータ装置を用いて実施した。Heitec-Auerbach GmbH & Co. KG社(Ellefeld)のSicomix又はMuegromix+のタイプのミキサーが適していることが判明した。このミキサーの主要エレメントは、ロータ/ステータ原理による運転される低剪断(Low Shear)混合ヘッドであった。混合ヘッドの回転数は、50〜300rpmであった。このスラリーの密度は、1100〜1700g/lであり、発泡体の見掛け密度は100〜500g/lであった。この処理量は、約120l/hであった。
Claims (22)
- 高炉スラグと、更にマイクロシリカ及び/又はメタカオリンを含む、少なくとも1種の無機結合材;
アルカリ金属水酸化物、アルカリ金属炭酸塩、アルカリ金属アルミン酸塩、アルカリ金属ケイ酸塩、及びこれらの混合物からなる群から選択される、少なくとも1種のアルカリ性活性剤;
少なくとも1種の界面活性剤であるアルキルポリグルコシド;
気相並びに
水
を含む、ジオポリマー発泡調製物。 - 前記アルカリ性活性剤は、式MOHのアルカリ金属水酸化物及び式m SiO2・n M2Oのアルカリ金属ケイ酸塩から選択され、前記式中、Mは、アルカリ金属であり、m:nのモル比は、≦4.0であることを特徴とする、請求項1に記載の調製物。
- 前記アルカリ性活性剤は、アルカリ金属水酸化物とアルカリ金属ケイ酸塩との混合物を含むことを特徴とする、請求項2に記載の調製物。
- 前記調製物は、
高炉スラグ3〜60質量%、
マイクロシリカ及び/又はメタカオリン3〜70質量%、
フライアッシュ0〜50質量%、
アルカリ性活性剤(固形分として計算)1〜55質量%、
水(全体量)10〜60質量%、
並びに界面活性剤及び気相を含むことを特徴とする、請求項1から3までのいずれか1項に記載の調製物。 - アルキルポリグルコシドは、式H−(C6H10O5)m−O−R1を示し、前記式中、(C6H10O5)は、グルコース単位を表し、かつR1は、C8〜C12−アルキル基を表し、m=1〜5であることを特徴とする、請求項1から4までのいずれか1項に記載の調製物。
- 前記気相は、空気、窒素、希ガス、炭化水素並びにこれらの混合物からなる群から選択されることを特徴とする、請求項1から5までのいずれか1項に記載の調製物。
- 前記調製物は、20〜90体積%が気相からなることを特徴とする、請求項1から6までのいずれか1項に記載の調製物。
- 前記調製物は、水10〜60質量%を含むことを特徴とする、請求項1から7までのいずれか1項に記載の調製物。
- 前記調製物は、更に、セメントを最大20質量%含むことを特徴とする、請求項1から8までのいずれか1項に記載の調製物。
- 前記調製物は、更に、気泡を安定化するため、収縮を抑制するため、柔軟化するため、疎水化するため、分散するための少なくとも1種の添加剤、繊維及び充填剤並びにこれらの混合物を含むことを特徴とする、請求項1から9までのいずれか1項に記載の調製物。
- 前記気泡を安定化するための添加剤は、熱分解ケイ酸、タンパク質、レオロジー改質剤、及びこれらの混合物からなる群から選択されることを特徴とする、請求項10に記載の調製物。
- 前記収縮を抑制するための添加剤は、アミン、アルカノールアミン、ベタイン(類)、グリコール、ポリオール、アルミノケイ酸塩中空球、ガラス中空球、発泡ガラス及びこれらの混合物からなる群から選択されることを特徴とする、請求項10に記載の調製物。
- 前記柔軟化するための添加剤は、再分散可能なポリマー粉末、ポリイソシアナート、ポリイソシアナートプレポリマー、エポキシ樹脂、エポキシ化合物及びこれらの混合物からなる群から選択されることを特徴とする、請求項10に記載の調製物。
- 前記疎水化するための添加剤は、トリグリセリド、パラフィン、ポリシロキサン、ヒドロゲンシラン、アルコキシシラン、ナトリウムメチルシリコナート、及びこれらの混合物からなる群から選択されることを特徴とする、請求項10に記載の調製物。
- 前記分散するための添加剤は、櫛形ポリマーから選択されることを特徴とする、請求項10に記載の調製物。
- 前記繊維は、鉱物繊維、ガラス繊維、炭素繊維、変性された有機繊維、セルロース繊維、リグノセルロース繊維、金属繊維及びこれらの混合物からなる群から選択されることを特徴とする、請求項10に記載の調製物。
- 前記充填剤は、石英砂、炭酸カルシウム、岩石粉、顔料、金属塩及びこれらの混合物からなる群から選択されることを特徴とする、請求項10に記載の調製物。
- 全ての構成成分が一つの成分として一緒に存在するか、又は固体構成成分は第1の固体成分中に準備されかつ水は第2の液体成分中に準備されることを特徴とする、請求項1から17までのいずれか1項に記載の調製物。
- 発泡を、空気の機械的導入によって実施することを特徴とする、請求項1から18までのいずれか1項に記載の調製物の製造方法。
- 前記発泡を、ステータ−ロータ法によって、振動法によって又は機械的攪拌によって実施することを特徴とする、請求項19に記載の方法。
- 不燃性で、吸音性で、断熱性のジオポリマー発泡部材を製造するための、請求項1から18までのいずれか1項に記載のジオポリマー発泡調製物の使用。
- 請求項1から18までのいずれか1項に記載のジオポリマー発泡調製物を含む、不燃性で、吸音性で、断熱性のジオポリマー発泡部材。
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PCT/EP2014/072027 WO2015062860A1 (de) | 2013-10-31 | 2014-10-14 | Geopolymerschaum-formulierung für ein nicht brennbares, schallabsorbierendes, wärmedämmendes geopolymerschaumelement |
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EP3063100A1 (de) | 2016-09-07 |
EP2868637A1 (de) | 2015-05-06 |
US20190152853A1 (en) | 2019-05-23 |
KR102271604B1 (ko) | 2021-07-01 |
CN105683120A (zh) | 2016-06-15 |
EP3530631A1 (de) | 2019-08-28 |
US20160244366A1 (en) | 2016-08-25 |
JP2016534965A (ja) | 2016-11-10 |
WO2015062860A1 (de) | 2015-05-07 |
KR20160081947A (ko) | 2016-07-08 |
EP3063100B1 (de) | 2019-03-20 |
CN105683120B (zh) | 2018-11-30 |
US10214452B2 (en) | 2019-02-26 |
US10597326B2 (en) | 2020-03-24 |
EP3530631B1 (de) | 2020-12-09 |
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