JP6424232B2 - 非水性流体を用いたエレクトロクロミックフィルムからの粒子除去 - Google Patents
非水性流体を用いたエレクトロクロミックフィルムからの粒子除去 Download PDFInfo
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- JP6424232B2 JP6424232B2 JP2016555466A JP2016555466A JP6424232B2 JP 6424232 B2 JP6424232 B2 JP 6424232B2 JP 2016555466 A JP2016555466 A JP 2016555466A JP 2016555466 A JP2016555466 A JP 2016555466A JP 6424232 B2 JP6424232 B2 JP 6424232B2
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/004—Surface-active compounds containing F
- C11D1/006—Surface-active compounds containing fluorine and phosphorus
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
-
- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/15—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on an electrochromic effect
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K71/00—Manufacture or treatment specially adapted for the organic devices covered by this subclass
- H10K71/60—Forming conductive regions or layers, e.g. electrodes
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K77/00—Constructional details of devices covered by this subclass and not covered by groups H10K10/80, H10K30/80, H10K50/80 or H10K59/80
- H10K77/10—Substrates, e.g. flexible substrates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
- C11D2111/14—Hard surfaces
- C11D2111/18—Glass; Plastics
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
- C11D2111/14—Hard surfaces
- C11D2111/22—Electronic devices, e.g. PCBs or semiconductors
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E10/00—Energy generation through renewable energy sources
- Y02E10/50—Photovoltaic [PV] energy
- Y02E10/549—Organic PV cells
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Description
Claims (12)
- エレクトロクロミックデバイスを作製する方法であって、
第1導電層を基板に堆積させることと、
第1電極層を前記第1導電層に堆積させることであって、前記第1電極層がエレクトロクロミック層または対電極層の一方である、堆積させることと、
イオン伝導体層を前記第1電極層に堆積させることとであって、第1フィルムスタックが前記第1導電層、前記第1電極層および前記イオン伝導体層を含んでいる、堆積させることと、
前記第1フィルムスタックを非水性液体に曝した後に第2電極層を前記第1フィルムスタックに堆積させることであって、前記第2電極層が前記エレクトロクロミック層または前記対電極層の他方である、堆積させることと、
第2導電層を前記第2電極層に堆積させることと、および
フィルムスタックを非水性液体に曝し、0.1μmと1000μmの間のサイズを有する粒子状材料を除去することと、を備え、
前記フィルムスタックは、前記第1導電層、前記第1電極層、前記イオン伝導体層、前記第2電極層、または前記第2導電層を含み、
前記非水性液体は、フッ素化アルキル基を含むエーテルである材料から実質的になり、
前記エレクトロクロミックデバイスは1欠陥/m2未満の欠陥密度を有する、方法。 - 前記方法が、前記第1導電層または前記イオン伝導体層をパターン化することをさらに含み、前記粒子状材料が、パターン化の際に発生し、表面を曝すことが、前記層をパターン化した後で実施される、請求項1に記載の方法。
- 前記方法が前記第1電極層または前記第2電極層をリチウム化することをさらに含む、請求項1または2に記載の方法。
- 前記エーテルがパーフルオロアルキル−アルキルエーテルである、請求項1ないし3のいずれか1項に記載の方法。
- 前記エーテルはR1−O−R2の一般式を有し、R1はC3からC7のパーフルオロアルキル基であり、R2はCH3基またはCH3CH2基である、請求項1ないし3のいずれか1項に記載の方法。
- 前記欠陥密度が1可視欠陥/m2未満である、請求項1ないし5のいずれか1項に記載の方法。
- 前記欠陥密度が1短絡/m2未満である、請求項1ないし6のいずれか1項に記載の方法。
- 前記非水性液体は、それが作用する前記フィルムスタックの表面から粒子を取り除くのに十分な速度のストリームまたはジェットの形態で送達される、請求項1ないし7のいずれか1項に記載の方法。
- 前記非水性液体が、0.0デバイから1.1デバイの範囲の極性を有する、請求項1ないし8のいずれか1項に記載の方法。
- 前記非水性液体が、1.4デバイから5.0デバイの範囲の極性を有する、請求項1ないし9のいずれか1項に記載の方法。
- 前記粒子状材料が、1ミクロンから500ミクロンの範囲のサイズを有する、請求項1ないし10のいずれか1項に記載の方法。
- 前記フィルムスタックを非水性液体に曝している間にエネルギーが印加され、該エネルギーが、前記非水性液体の超音波撹拌、バブルジェット(登録商標)撹拌、前記非水性液体の熱的加熱、またはこれらの任意の組み合わせである、請求項1ないし11のいずれか1項に記載の方法。
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US14/198,824 US10767143B2 (en) | 2014-03-06 | 2014-03-06 | Particle removal from electrochromic films using non-aqueous fluids |
PCT/US2015/018980 WO2015134756A1 (en) | 2014-03-06 | 2015-03-05 | Particle removal from electrochromic films using non-aqueous fluids |
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