JP6180797B2 - 試料中の水素含有量測定のためのシステム及び方法 - Google Patents

試料中の水素含有量測定のためのシステム及び方法 Download PDF

Info

Publication number
JP6180797B2
JP6180797B2 JP2013116707A JP2013116707A JP6180797B2 JP 6180797 B2 JP6180797 B2 JP 6180797B2 JP 2013116707 A JP2013116707 A JP 2013116707A JP 2013116707 A JP2013116707 A JP 2013116707A JP 6180797 B2 JP6180797 B2 JP 6180797B2
Authority
JP
Japan
Prior art keywords
thermal desorption
desorption chamber
sample
carrier gas
hydrogen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2013116707A
Other languages
English (en)
Japanese (ja)
Other versions
JP2013253970A (ja
JP2013253970A5 (https=
Inventor
カールトン エヌ. クリスティ,
カールトン エヌ. クリスティ,
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Boeing Co
Original Assignee
Boeing Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Boeing Co filed Critical Boeing Co
Publication of JP2013253970A publication Critical patent/JP2013253970A/ja
Publication of JP2013253970A5 publication Critical patent/JP2013253970A5/ja
Application granted granted Critical
Publication of JP6180797B2 publication Critical patent/JP6180797B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00Particle spectrometers or separator tubes
    • H01J49/02Details
    • H01J49/04Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
    • H01J49/0468Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components with means for heating or cooling the sample
    • H01J49/049Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components with means for heating or cooling the sample with means for applying heat to desorb the sample; Evaporation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/20Metals
    • G01N33/202Constituents thereof
    • G01N33/2022Non-metallic constituents
    • G01N33/2025Gaseous constituents
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0009General constructional details of gas analysers, e.g. portable test equipment
    • G01N33/0027General constructional details of gas analysers, e.g. portable test equipment concerning the detector
    • G01N33/0036General constructional details of gas analysers, e.g. portable test equipment concerning the detector specially adapted to detect a particular component
    • G01N33/005H2

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Food Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
  • Investigating And Analyzing Materials By Characteristic Methods (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
JP2013116707A 2012-06-04 2013-06-03 試料中の水素含有量測定のためのシステム及び方法 Expired - Fee Related JP6180797B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US13/487,481 US8754369B2 (en) 2012-06-04 2012-06-04 System and method for measuring hydrogen content in a sample
US13/487,481 2012-06-04

Publications (3)

Publication Number Publication Date
JP2013253970A JP2013253970A (ja) 2013-12-19
JP2013253970A5 JP2013253970A5 (https=) 2016-07-21
JP6180797B2 true JP6180797B2 (ja) 2017-08-16

Family

ID=48670354

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2013116707A Expired - Fee Related JP6180797B2 (ja) 2012-06-04 2013-06-03 試料中の水素含有量測定のためのシステム及び方法

Country Status (5)

Country Link
US (1) US8754369B2 (https=)
EP (2) EP2672267A1 (https=)
JP (1) JP6180797B2 (https=)
CN (1) CN103454125B (https=)
CA (1) CA2814895C (https=)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9417126B2 (en) * 2014-06-27 2016-08-16 International Business Machines Corporation Spectrometer insert for measuring temperature-dependent optical properties
CN105928854B (zh) * 2016-04-20 2018-11-30 中国原子能科学研究院 材料中可控微压吸氚及氚浓度深度分布在线实验装置
JP6934239B2 (ja) * 2017-02-27 2021-09-15 国立大学法人東京工業大学 高感度昇温脱離ガス分析装置
CN106932238A (zh) * 2017-04-24 2017-07-07 云南中烟工业有限责任公司 一种嗅觉物质捕集装置及应用
CN108918340B (zh) * 2018-06-22 2020-11-20 航天材料及工艺研究所 耐烧蚀酚醛树脂热解过程放气量测试装置及测试方法
DE102018115552A1 (de) 2018-06-28 2020-01-02 Schaeffler Technologies AG & Co. KG Verfahren und Vorrichtung zur Wasserstoffmessung in einer Wälzlageranordnung
CN110342455A (zh) * 2019-07-19 2019-10-18 北京卫星环境工程研究所 一种微尺度飞行时间质谱仪
JP2021103133A (ja) * 2019-12-25 2021-07-15 株式会社島津製作所 直接試料導入装置、および試料導入プローブの冷却方法
CN111879652B (zh) * 2020-06-29 2022-06-14 武汉钢铁有限公司 一种定氢仪器的校正方法
CN111751247B (zh) * 2020-07-14 2025-03-04 广东省特种设备检测研究院珠海检测院 一种固态金属中氢含量检测装置
CN111781088B (zh) * 2020-07-14 2023-05-12 广东省特种设备检测研究院珠海检测院 一种固态金属中氢含量检测方法
CN113092374B (zh) * 2021-04-12 2022-11-15 青岛科技大学 小型真空光电测试系统
CN113310773A (zh) * 2021-07-15 2021-08-27 深圳卫十生物科技有限公司 一种用于化妆品重金属检测装置
CN114624145B (zh) * 2022-05-16 2022-09-09 上海景瑞阳实业有限公司 一种金属材料的氢逸出速率的检测系统及方法
US20240307852A1 (en) * 2023-03-17 2024-09-19 Spiritus Technologies, Pbc Desorption apparatus
CN116793893B (zh) * 2023-04-23 2024-03-29 华南理工大学 一种高压临氢材料的氢含量测试装置及测试方法
CN117554245B (zh) * 2024-01-11 2024-03-26 中国航发北京航空材料研究院 基于电阻率的镍基高温合金氢扩散系数的测定装置及方法
CN120352569A (zh) * 2024-01-22 2025-07-22 霍尼韦尔国际公司 用于测试气体传感器的系统、装置和方法
EP4715380A1 (en) * 2024-09-23 2026-03-25 Advanced Monitoring Solutions AS System for hydrogen detection at low volume mixing ratios

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3589171A (en) * 1969-08-25 1971-06-29 California Inst Of Techn Gas analysis system and palladium tube separator therefor
DE2727252C3 (de) * 1976-06-19 1981-07-16 Japan Analyst Corp., Tokyo Verfahren zur Vorrichtung zur Messung des in einer Metallprobe enthaltenen Wasserstoff
US4192175A (en) * 1978-03-03 1980-03-11 Kobe Steel, Ltd. Process and apparatus for measurement of diffusible hydrogen
US4660297A (en) * 1985-11-01 1987-04-28 Philip Danielson Desorption of water molecules in a vacuum system using ultraviolet radiation
US5142143A (en) * 1990-10-31 1992-08-25 Extrel Corporation Method and apparatus for preconcentration for analysis purposes of trace constitutes in gases
JPH07306182A (ja) * 1994-05-13 1995-11-21 Oki Electric Ind Co Ltd 昇温脱離ガス分析装置
JPH0894505A (ja) * 1994-09-21 1996-04-12 Hitachi Ltd 脱離ガス分析装置
GB9608041D0 (en) * 1996-04-18 1996-06-19 Ion Science Ltd A device for hydrogen collection
JP4162138B2 (ja) * 2003-10-27 2008-10-08 株式会社リガク 昇温脱離ガス分析装置
JP4155409B2 (ja) * 2006-01-23 2008-09-24 日鋼検査サービス株式会社 トレーサー水素による材料劣化性状評価方法および評価装置
JP5405218B2 (ja) 2008-07-31 2014-02-05 電子科学株式会社 試料分析方法、試料搬入部材、試料搬入方法および昇温脱離分析装置

Also Published As

Publication number Publication date
EP2863218A3 (en) 2015-06-24
US8754369B2 (en) 2014-06-17
JP2013253970A (ja) 2013-12-19
CA2814895C (en) 2018-03-27
EP2672267A1 (en) 2013-12-11
CN103454125B (zh) 2017-10-13
US20130320206A1 (en) 2013-12-05
EP2863218A2 (en) 2015-04-22
CN103454125A (zh) 2013-12-18
CA2814895A1 (en) 2013-12-04
EP2863218B1 (en) 2016-08-17

Similar Documents

Publication Publication Date Title
JP6180797B2 (ja) 試料中の水素含有量測定のためのシステム及び方法
JP5926191B2 (ja) 漏れを測定する方法および装置
CN106501125B (zh) 气体吸附脱附测试装置及测试方法
Redhead Recommended practices for measuring and reporting outgassing data
CN109755097B (zh) 一种四极杆质谱仪及其使用方法
JP5076143B2 (ja) 細孔微粒子のガス吸着特性測定装置及びその測定方法
CN111238884A (zh) 滤膜固定结构、样品炉及ocec分析仪
JP5648992B2 (ja) 高感度ガス分析装置、ガス定量方法及び分析装置システム
CN113607769B (zh) 一种利用核磁共振的仲氢含量检测装置及方法
CN113808906B (zh) 超高耐压深海膜进样结构及质谱系统
Ramasamy et al. Oxygen sensor via the quenching of room-temperature phosphorescence of perdeuterated phenanthrene adsorbed on Whatman 1PS filter paper
JP4911502B2 (ja) ガス分析装置
CN105702554A (zh) 消色谱效应的超高真空腔对高压气体采样装置
US11953488B2 (en) Systems and methods for determining concentrations of mobile hydrogen of metallic objects and/or reducing concentrations of mobile hydrogen of metallic objects
JPS6125047A (ja) 圧力容器における水素侵食の事前検出方法
CN112362721A (zh) 连续流模式下检测气体中硫同位素的装置和方法
CN206420726U (zh) 气体吸附脱附测试装置
EP2543995A1 (en) Helium ionization detector
JP2006300569A (ja) 水素貯蔵材料の評価装置及び評価方法
JP2012247202A (ja) 分析方法および装置
WO2020065135A1 (en) Arrangement and method for thermal desorption measurement
RU147559U1 (ru) Устройство ввода газов и их смесей в масс-спектрометр
JP5508118B2 (ja) 発生気体分析装置
CN119880840A (zh) 逸出气体成份的分析系统
KR20250154710A (ko) 가스 크로마토그래피를 이용한 수소 열탈착 거동 분석 시스템

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20160601

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20160601

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20170519

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20170704

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20170719

R150 Certificate of patent or registration of utility model

Ref document number: 6180797

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees