JP6166252B2 - 改善された炭化水素変換触媒 - Google Patents

改善された炭化水素変換触媒 Download PDF

Info

Publication number
JP6166252B2
JP6166252B2 JP2014501155A JP2014501155A JP6166252B2 JP 6166252 B2 JP6166252 B2 JP 6166252B2 JP 2014501155 A JP2014501155 A JP 2014501155A JP 2014501155 A JP2014501155 A JP 2014501155A JP 6166252 B2 JP6166252 B2 JP 6166252B2
Authority
JP
Japan
Prior art keywords
catalyst
microns
threshold
particles
particle size
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2014501155A
Other languages
English (en)
Japanese (ja)
Other versions
JP2014510628A (ja
JP2014510628A5 (enExample
Inventor
キニョネス,アウグスト,エレ
Original Assignee
クアンタ テクノロジーズ エルエルシー
クアンタ テクノロジーズ エルエルシー
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by クアンタ テクノロジーズ エルエルシー, クアンタ テクノロジーズ エルエルシー filed Critical クアンタ テクノロジーズ エルエルシー
Publication of JP2014510628A publication Critical patent/JP2014510628A/ja
Publication of JP2014510628A5 publication Critical patent/JP2014510628A5/ja
Application granted granted Critical
Publication of JP6166252B2 publication Critical patent/JP6166252B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G11/00—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G11/14—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid catalysts
    • C10G11/18—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid catalysts according to the "fluidised-bed" technique
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/08—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the faujasite type, e.g. type X or Y
    • B01J29/084—Y-type faujasite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/51—Spheres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0036—Grinding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0045—Drying a slurry, e.g. spray drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/009—Preparation by separation, e.g. by filtration, decantation, screening
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/08—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal with moving catalysts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/42—Catalytic treatment
    • C10G3/44—Catalytic treatment characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1037—Hydrocarbon fractions
    • C10G2300/1044—Heavy gasoline or naphtha having a boiling range of about 100 - 180 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/70—Catalyst aspects
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Catalysts (AREA)
JP2014501155A 2011-03-19 2012-03-16 改善された炭化水素変換触媒 Active JP6166252B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201161465390P 2011-03-19 2011-03-19
US61/465,390 2011-03-19
PCT/US2012/029341 WO2012129065A2 (en) 2011-03-19 2012-03-16 Process to improve formulations of hydrocarbon conversion catalysts through removal and modification of detrimental particles and reuse of modified fractions

Publications (3)

Publication Number Publication Date
JP2014510628A JP2014510628A (ja) 2014-05-01
JP2014510628A5 JP2014510628A5 (enExample) 2015-05-07
JP6166252B2 true JP6166252B2 (ja) 2017-07-19

Family

ID=46828980

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2014501155A Active JP6166252B2 (ja) 2011-03-19 2012-03-16 改善された炭化水素変換触媒

Country Status (12)

Country Link
US (2) US9393556B2 (enExample)
EP (1) EP2688669B1 (enExample)
JP (1) JP6166252B2 (enExample)
KR (1) KR102010281B1 (enExample)
CN (2) CN103547369A (enExample)
AU (1) AU2012231256A1 (enExample)
BR (1) BR112013024064B1 (enExample)
CA (1) CA2830504C (enExample)
MX (1) MX343480B (enExample)
PL (1) PL2688669T3 (enExample)
SG (1) SG193490A1 (enExample)
WO (1) WO2012129065A2 (enExample)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6166252B2 (ja) * 2011-03-19 2017-07-19 クアンタ テクノロジーズ エルエルシー 改善された炭化水素変換触媒
JP6239853B2 (ja) * 2013-04-30 2017-11-29 日揮触媒化成株式会社 流動接触分解触媒の製造方法および流動接触分解触媒
CN104785271B (zh) * 2014-01-21 2017-02-22 万华化学集团股份有限公司 制氯气用催化剂的制法、该催化剂及制氯气的方法
EP3504297A4 (en) * 2016-08-23 2020-06-17 Quanta Technologies, LLC IMPROVING THE EFFICIENCY OF FCCU REFINING ADDITIVES
CN111286359B (zh) * 2018-12-07 2021-12-17 中国石油化工股份有限公司 一种加工重质烃油原料的方法

Family Cites Families (31)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE569961A (enExample) 1957-08-15
US3373102A (en) 1965-12-17 1968-03-12 Exxon Research Engineering Co Pretreatment of catalytic cracking feed stocks
US3748251A (en) 1971-04-20 1973-07-24 Mobil Oil Corp Dual riser fluid catalytic cracking with zsm-5 zeolite
AT364745B (de) 1975-03-24 1981-11-10 Ashland Oil Inc Verfahren und vorrichtung zum abscheiden feiner feststoffteilchen aus stroemenden gasen
US4209273A (en) 1978-01-16 1980-06-24 Lehnen Peter E Machine tool speed control system
US4309280A (en) * 1980-07-18 1982-01-05 Mobil Oil Corporation Promotion of cracking catalyst octane yield performance
US4828679A (en) * 1984-03-12 1989-05-09 Mobil Oil Corporation Octane improvement with large size ZSM-5 catalytic cracking
US5051164A (en) * 1987-09-04 1991-09-24 Mobil Oil Corporation Crystalline porous silicate composite and its use in catalytic cracking
US4895636A (en) 1988-06-10 1990-01-23 Mobil Oil Corporation FCC process with catalyst separation
US5393412A (en) * 1991-05-03 1995-02-28 Ashland Oil, Inc. Combination magnetic separation, classification and attrition process for renewing and recovering particulates
US5209840A (en) 1991-10-02 1993-05-11 Texaco Inc. Separation of active catalyst particles from spent catalyst particles by air elutriation
JPH05261301A (ja) * 1992-03-18 1993-10-12 Mitsubishi Kasei Corp 流動床触媒の製造法
BR9203110A (pt) 1992-08-12 1994-03-01 Petroleo Brasileiro Sa Composicao catalitica passivadora para o craqueamento de hidrocarbonetos,alumina e processo de craqueamento catalitico fluido
US5854161A (en) 1996-04-24 1998-12-29 Abb Lummus Global Inc. Process for the regeneration of a catalyst
JP2001029788A (ja) * 1999-07-21 2001-02-06 Mitsubishi Rayon Co Ltd モリブデン−ビスマス−鉄含有金属酸化物流動層触媒の製法
US6509290B1 (en) * 2000-07-17 2003-01-21 Exxon Mobil Chemical Patents, Inc. Catalyst composition including attrition particles and method for making same
TWI304359B (en) 2001-12-04 2008-12-21 Bp Chem Int Ltd Oxidation process in fluidised bed reactor
US6800579B2 (en) * 2002-01-29 2004-10-05 Exxonmobil Research And Engineering Company Catalyst regeneration
US7655704B2 (en) * 2002-04-16 2010-02-02 Sasol Technology (Proprietary) Ltd. Hydrocarbon synthesis process using an alkali promoted iron catalyst
US7718811B2 (en) 2002-11-26 2010-05-18 Ineos Europe Limited Oxidation process in fluidised bed reactor
US7223896B2 (en) * 2004-04-29 2007-05-29 Exxonmobil Chemical Patents Inc. Fines co-feed for maintaining efficient reactor hydrodynamics
WO2005025744A1 (en) 2003-09-05 2005-03-24 Exxonmobil Chemical Patents Inc. Processes for formulating catalyst compositions having desirable particle size characteristics
US7090081B2 (en) * 2003-09-05 2006-08-15 Exxonmobil Chemical Patents Inc. Selectively removing undesirably sized catalyst particles from a reaction system
US7431826B2 (en) 2004-02-26 2008-10-07 Metal Alloy Reclaimers, Inc. Ii. Discarded FCC equilibrium catalyst through reclamation
MX2007010667A (es) * 2005-03-01 2007-11-08 Carbo Ceramics Inc Metodos para producir particulas sinterizadas a partir de una suspension espesa de una materia prima que contiene alumina.
US7439414B2 (en) * 2005-10-13 2008-10-21 Uop Llc Oxygenate conversion catalyst processing
AU2008286950B2 (en) * 2007-08-10 2013-11-07 Res Usa, Llc Precipitated iron catalyst for hydrogenation of carbon monoxide
KR101503069B1 (ko) * 2008-10-17 2015-03-17 에스케이이노베이션 주식회사 유동층 접촉 분해 공정의 경질 사이클 오일로부터 고부가 방향족 및 올레핀을 제조하는 방법
EP2448676B1 (en) * 2009-05-18 2024-07-31 Integrated & Proven Catalyst Technologies Corp. Separation of fluid catalytic cracking equilibrium catalysts to improve value and reduce waste
US8715487B2 (en) 2010-03-11 2014-05-06 Exxonmobil Research And Engineering Company Low small mesoporous peak cracking catalyst and method of using
JP6166252B2 (ja) * 2011-03-19 2017-07-19 クアンタ テクノロジーズ エルエルシー 改善された炭化水素変換触媒

Also Published As

Publication number Publication date
MX2013010588A (es) 2014-03-27
SG193490A1 (en) 2013-10-30
CN103547369A (zh) 2014-01-29
BR112013024064A2 (pt) 2017-06-27
EP2688669B1 (en) 2023-09-27
EP2688669A4 (en) 2014-09-03
US9393556B2 (en) 2016-07-19
CN107626340A (zh) 2018-01-26
AU2012231256A1 (en) 2013-10-03
PL2688669T3 (pl) 2024-03-11
US20160319204A1 (en) 2016-11-03
US10093866B2 (en) 2018-10-09
KR102010281B1 (ko) 2019-08-13
US20120238790A1 (en) 2012-09-20
CA2830504A1 (en) 2012-09-27
JP2014510628A (ja) 2014-05-01
MX343480B (es) 2016-11-07
WO2012129065A3 (en) 2012-12-06
KR20140024864A (ko) 2014-03-03
WO2012129065A2 (en) 2012-09-27
EP2688669A2 (en) 2014-01-29
BR112013024064B1 (pt) 2020-03-03
CA2830504C (en) 2021-05-04

Similar Documents

Publication Publication Date Title
US10093866B2 (en) Process to improve formulations of hydrocarbon conversion catalysts through removal and modification of detrimental particles and reuse of modified fractions
US2567207A (en) Maintenance of catalytic activity in hydrocarbon conversion systems
RU2540859C2 (ru) Усовершенствованный сокатализатор улавливания тяжелых металлов для процесса флюид каталитического крекинга
RU2672919C2 (ru) Повышение активности присадки zsm-5 с помощью улучшенного взаимодействия цеолита и фосфора
JP5469294B2 (ja) 構造的に強化された分解触媒
US9901916B2 (en) Separation of fluid catalytic cracking equilibrium catalysts to improve value and reduce waste
CN102631945A (zh) 一种耐磨催化剂的制备方法
CN102527445A (zh) 一种低磨耗流化床微球催化剂的制备方法
TW200938573A (en) Enhanced fine agglomerate mixture
WO2002070132A2 (en) Attrition resistant inorganic microspheroidal particles
CN102319582A (zh) 一种催化裂化催化剂的制备方法
CA2914006A1 (en) Method of producing fcc catalysts with reduced attrition rates
KR102366730B1 (ko) 고강도 성형된 알루미나들 및 이러한 고강도 성형된 알루미나들을 제조하는 방법
CN1309471C (zh) 具有超高动力学转化活性的基于沸石的催化剂
CN104487167B (zh) 镁稳定的超低苏打裂化催化剂
TW201138966A (en) Process for making improved catalysts from clay-derived zeolites
US20200197919A1 (en) Catalyst Formulations with Improved Performance via Variable Composition Control as a Function of Particle Size
JP2009274061A (ja) 触媒及びその製造方法
US3006864A (en) Process for preparing an attrition resistant catalyst or catalyst support

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20150316

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20150316

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20151202

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20151215

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20160307

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20160412

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20160719

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20161014

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20161215

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20170418

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20170425

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20170523

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20170622

R150 Certificate of patent or registration of utility model

Ref document number: 6166252

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250