JP6054878B2 - フルオロポリマー組成物及びその精製方法 - Google Patents

フルオロポリマー組成物及びその精製方法 Download PDF

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JP6054878B2
JP6054878B2 JP2013546370A JP2013546370A JP6054878B2 JP 6054878 B2 JP6054878 B2 JP 6054878B2 JP 2013546370 A JP2013546370 A JP 2013546370A JP 2013546370 A JP2013546370 A JP 2013546370A JP 6054878 B2 JP6054878 B2 JP 6054878B2
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fluorinated
molecular weight
low molecular
reaction product
polymerization
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JP2014501305A (ja
JP2014501305A5 (cg-RX-API-DMAC7.html
Inventor
ヒンツァー クラウス
ヒンツァー クラウス
ユルゲンス ミハエル
ユルゲンス ミハエル
ヨット.ケンプフ グンター
ヨット.ケンプフ グンター
カスパー ハラルト
カスパー ハラルト
ヘルムート ロハース カイ
ヘルムート ロハース カイ
シュトライター アンドレ
シュトライター アンドレ
シシュコフ オレグ
シシュコフ オレグ
ツェー.ツィップリーズ ティルマン
ツェー.ツィップリーズ ティルマン
ケーニヒスマン ヘルベルト
ケーニヒスマン ヘルベルト
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3M Innovative Properties Co
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3M Innovative Properties Co
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00Post-polymerisation treatments
    • C08F6/001Removal of residual monomers by physical means
    • C08F6/003Removal of residual monomers by physical means from polymer solutions, suspensions, dispersions or emulsions without recovery of the polymer therefrom
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/26Treatment of water, waste water, or sewage by extraction
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/46Treatment of water, waste water, or sewage by electrochemical methods
    • C02F1/461Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F14/00Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F14/02Monomers containing chlorine
    • C08F14/04Monomers containing two carbon atoms
    • C08F14/08Vinylidene chloride
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F14/00Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F14/18Monomers containing fluorine
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/04Polymerisation in solution
    • C08F2/10Aqueous solvent
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/12Polymerisation in non-solvents
    • C08F2/16Aqueous medium
    • C08F2/20Aqueous medium with the aid of macromolecular dispersing agents
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/46Treatment of water, waste water, or sewage by electrochemical methods
    • C02F1/461Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
    • C02F1/46104Devices therefor; Their operating or servicing
    • C02F1/46109Electrodes
    • C02F2001/46133Electrodes characterised by the material
    • C02F2001/46138Electrodes comprising a substrate and a coating
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/46Treatment of water, waste water, or sewage by electrochemical methods
    • C02F1/461Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
    • C02F1/46104Devices therefor; Their operating or servicing
    • C02F1/46109Electrodes
    • C02F2001/46133Electrodes characterised by the material
    • C02F2001/46138Electrodes comprising a substrate and a coating
    • C02F2001/46147Diamond coating
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2800/00Copolymer characterised by the proportions of the comonomers expressed
    • C08F2800/10Copolymer characterised by the proportions of the comonomers expressed as molar percentages
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Hydrology & Water Resources (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Polymerisation Methods In General (AREA)
  • Fertilizers (AREA)
JP2013546370A 2010-12-23 2011-12-21 フルオロポリマー組成物及びその精製方法 Expired - Fee Related JP6054878B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
GB1021790.9 2010-12-23
GBGB1021790.9A GB201021790D0 (en) 2010-12-23 2010-12-23 Fluoropolymer compostions and purification methods thereof
PCT/US2011/066456 WO2012088258A1 (en) 2010-12-23 2011-12-21 Fluoropolymer compositions and purification methods thereof

Publications (3)

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JP2014501305A JP2014501305A (ja) 2014-01-20
JP2014501305A5 JP2014501305A5 (cg-RX-API-DMAC7.html) 2015-01-08
JP6054878B2 true JP6054878B2 (ja) 2016-12-27

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JP2013546370A Expired - Fee Related JP6054878B2 (ja) 2010-12-23 2011-12-21 フルオロポリマー組成物及びその精製方法

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US (2) US9453086B2 (cg-RX-API-DMAC7.html)
EP (1) EP2655440B1 (cg-RX-API-DMAC7.html)
JP (1) JP6054878B2 (cg-RX-API-DMAC7.html)
CN (1) CN103270057B (cg-RX-API-DMAC7.html)
GB (1) GB201021790D0 (cg-RX-API-DMAC7.html)
WO (1) WO2012088258A1 (cg-RX-API-DMAC7.html)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2928931B1 (en) 2012-12-04 2017-03-01 3M Innovative Properties Company Partially fluorinated polymers
WO2014088820A1 (en) * 2012-12-04 2014-06-12 3M Innovative Properties Company Highly fluorinated polymers
US11603594B2 (en) 2016-10-21 2023-03-14 Nanjing Daimonte Technology Co., Ltd. Boron doped diamond electrode and preparation method and applications thereof
US20230331595A1 (en) * 2018-08-23 2023-10-19 Evoqua Water Technologies Llc System and Method for Electrochemical Oxidation of Polyfluoroalkyl Substances in Water
TW202033573A (zh) * 2018-12-17 2020-09-16 美商3M新設資產公司 包括可固化氟聚合物及固化劑之組成物及製造及使用其之方法
CN113728014B (zh) * 2019-04-26 2024-07-26 大金工业株式会社 含氟聚合物水性分散液的制造方法、排水的处理方法和含氟聚合物水性分散液
EP3945099A1 (en) * 2020-07-30 2022-02-02 3M Innovative Properties Company Process for removal of fluoroorganic compounds from aqueous media
EP3945074A1 (en) 2020-07-30 2022-02-02 3M Innovative Properties Company Process to reduce the concentration of fluoroorganic acidic compound in aqueous dispersions
EP4219412A1 (en) 2022-01-27 2023-08-02 3M Innovative Properties Company Closed-loop technologies for purifying fluorine containing water streams
US20240102960A1 (en) * 2022-09-23 2024-03-28 Hach Company Dynamic end-point total organic fluoride measurement
JPWO2025135028A1 (cg-RX-API-DMAC7.html) * 2023-12-19 2025-06-26

Family Cites Families (31)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2908001C2 (de) 1979-03-01 1981-02-19 Hoechst Ag, 6000 Frankfurt Verfahren zur Herstellung konzentrierter Dispersionen von Fluorpolymeren
JPS5715885A (en) * 1980-06-30 1982-01-27 Nippon Rensui Kk Method for recovery of high-purity waste water of washing
JP3006049B2 (ja) 1990-07-26 2000-02-07 ダイキン工業株式会社 溶融加工可能なテトラフルオロエチレン共重合体の低分子量体除去方法
US5453477A (en) 1992-05-01 1995-09-26 Alliedsignal Inc. Process of polymerizing chloroetrifluoroethylene with alkyl hydroperoxide and metal metabisulfite
US5364508A (en) * 1992-11-12 1994-11-15 Oleh Weres Electrochemical method and device for generating hydroxyl free radicals and oxidizing chemical substances dissolved in water
JP3441193B2 (ja) 1994-09-30 2003-08-25 日本ゼオン株式会社 高純度の重合体の製造方法
US5955556A (en) 1995-11-06 1999-09-21 Alliedsignal Inc. Method of manufacturing fluoropolymers
US6315886B1 (en) 1998-12-07 2001-11-13 The Electrosynthesis Company, Inc. Electrolytic apparatus and methods for purification of aqueous solutions
CN1290880C (zh) * 2001-05-02 2006-12-20 3M创新有限公司 制备氟聚合物的无乳化剂水乳液聚合方法
EP1452571B1 (en) 2003-02-28 2005-08-17 3M Innovative Properties Company Fluoropolymer dispersion containing no or little low molecular weight fluorinated surfactant
US7071271B2 (en) 2003-10-30 2006-07-04 3M Innovative Properties Company Aqueous emulsion polymerization of functionalized fluoromonomers
US7659335B2 (en) * 2004-10-13 2010-02-09 Dupont-Mitsui Fluorochemicals Co Ltd Fluoropolymer dispersion and electrode composition containing same
US7666927B2 (en) 2004-12-22 2010-02-23 E.I. Du Pont De Nemours And Company Removing fluorosurfactant from aqueous fluoropolymer dispersions using anion exchange polymer with functional groups resistant to degradation to trialkylamines
US20070015937A1 (en) 2005-07-15 2007-01-18 3M Innovative Properties Company Process for recovery of fluorinated carboxylic acid surfactants from exhaust gas
GB0514398D0 (en) * 2005-07-15 2005-08-17 3M Innovative Properties Co Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant
GB2430437A (en) 2005-09-27 2007-03-28 3M Innovative Properties Co Method of making a fluoropolymer
RU2425056C2 (ru) 2005-10-17 2011-07-27 Асахи Гласс Компани, Лимитед Водная политетрафторэтиленовая эмульсия, политетрафторэтиленовый мелкодисперсный порошок и пористый материал, полученный из него
RU2409592C2 (ru) * 2005-10-26 2011-01-20 Асахи Гласс Компани, Лимитед Фторсодержащий полимер с низким остаточным содержанием фторированного эмульгатора и способ его получения
EP1849809A1 (en) * 2006-04-26 2007-10-31 Solvay Solexis S.p.A. Tetrafluoroethylene polymer particles
US7754795B2 (en) 2006-05-25 2010-07-13 3M Innovative Properties Company Coating composition
CN101506136B (zh) 2006-08-31 2013-06-12 旭硝子株式会社 全氟羧酸盐及其制造方法
GB0625071D0 (en) 2006-12-15 2007-01-24 3M Innovative Properties Co Process for removing fluorinated emulsifier from fluoropolmer dispersions using an ion-exchange resin and dispersions obtained therefrom
EP2132143B1 (en) 2007-02-16 2012-12-26 3M Innovative Properties Company System and process for the removal of fluorochemicals from water
GB0712191D0 (en) * 2007-06-25 2007-08-01 3M Innovative Properties Co Process for removing fluorinated compounds for an aqueous phase originating from the preparation of fluoropolymers
WO2009014167A1 (ja) * 2007-07-24 2009-01-29 Daikin Industries, Ltd. 新規化合物、その製造方法及びフルオロポリマーの製造方法
WO2009049168A1 (en) 2007-10-12 2009-04-16 3M Innovative Properties Company Process for manufacturing clean fluoropolymers
US20110247929A1 (en) * 2008-09-24 2011-10-13 Sumitomo Electric Hardmetal Corp. Diamond electrode and method for manufacturing diamond electrode
US8153738B2 (en) * 2008-12-23 2012-04-10 E I Du Pont De Nemours And Company Fluoropolymer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer
CN103994953A (zh) 2009-02-04 2014-08-20 莱泽尔诊断公司 用于分离和分析流体中的组分的装置和方法
DE102009013380A1 (de) 2009-03-09 2010-09-16 Hansgrohe Ag Verfahren zum Abbau von teilfluorierten und perfluorierten Tensiden
DE102009038125A1 (de) 2009-08-14 2011-02-17 Hansgrohe Ag Verfahren zur Aufarbeitung von tensidhaltigen Abfällen oder Abwässern

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Publication number Publication date
EP2655440B1 (en) 2016-08-17
GB201021790D0 (en) 2011-02-02
WO2012088258A1 (en) 2012-06-28
EP2655440A1 (en) 2013-10-30
US20160362508A1 (en) 2016-12-15
JP2014501305A (ja) 2014-01-20
CN103270057B (zh) 2016-08-17
CN103270057A (zh) 2013-08-28
US20130281607A1 (en) 2013-10-24
US9809658B2 (en) 2017-11-07
US9453086B2 (en) 2016-09-27

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