JP5973423B2 - アニーリングされたナノ構造薄膜触媒 - Google Patents

アニーリングされたナノ構造薄膜触媒 Download PDF

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JP5973423B2
JP5973423B2 JP2013508165A JP2013508165A JP5973423B2 JP 5973423 B2 JP5973423 B2 JP 5973423B2 JP 2013508165 A JP2013508165 A JP 2013508165A JP 2013508165 A JP2013508165 A JP 2013508165A JP 5973423 B2 JP5973423 B2 JP 5973423B2
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JP2013531551A5 (enExample
JP2013531551A (ja
Inventor
ケー.ディーベ マーク
ケー.ディーべ マーク
エル.ダブリュ.スミスソン ロバート
エル.ダブリュ.スミスソン ロバート
ジェイ.ステュディナー,ザ フォース チャールズ
ジェイ.ステュディナー,ザ フォース チャールズ
エム.ヘンドリックス スーザン
エム.ヘンドリックス スーザン
ジェイ.クルコウスキー マイケル
ジェイ.クルコウスキー マイケル
ジェイ.エル.シュタインバッハ アンドリュー
ジェイ.エル.シュタインバッハ アンドリュー
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3M Innovative Properties Co
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/86Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/90Selection of catalytic material
    • H01M4/92Metals of platinum group
    • H01M4/921Alloys or mixtures with metallic elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B01J23/8913Cobalt and noble metals
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B01J23/892Nickel and noble metals
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B01J23/8933Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals also combined with metals, or metal oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/8986Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals also combined with metals, or metal oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with manganese, technetium or rhenium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/34Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation
    • B01J37/341Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00Fuel cells; Manufacture thereof
    • H01M8/10Fuel cells with solid electrolytes
    • H01M2008/1095Fuel cells with polymeric electrolytes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30Hydrogen technology
    • Y02E60/50Fuel cells

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Toxicology (AREA)
  • Optics & Photonics (AREA)
  • Health & Medical Sciences (AREA)
  • Plasma & Fusion (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Catalysts (AREA)
  • Inert Electrodes (AREA)
  • Fuel Cell (AREA)
JP2013508165A 2010-04-26 2011-04-26 アニーリングされたナノ構造薄膜触媒 Active JP5973423B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US32806410P 2010-04-26 2010-04-26
US61/328,064 2010-04-26
PCT/US2011/033972 WO2011139705A1 (en) 2010-04-26 2011-04-26 Annealed nanostructured thin film catalyst

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2016078165A Division JP2016135489A (ja) 2010-04-26 2016-04-08 アニーリングされたナノ構造薄膜触媒

Publications (3)

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JP2013531551A JP2013531551A (ja) 2013-08-08
JP2013531551A5 JP2013531551A5 (enExample) 2016-06-09
JP5973423B2 true JP5973423B2 (ja) 2016-08-23

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JP2013508165A Active JP5973423B2 (ja) 2010-04-26 2011-04-26 アニーリングされたナノ構造薄膜触媒
JP2016078165A Withdrawn JP2016135489A (ja) 2010-04-26 2016-04-08 アニーリングされたナノ構造薄膜触媒

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JP2016078165A Withdrawn JP2016135489A (ja) 2010-04-26 2016-04-08 アニーリングされたナノ構造薄膜触媒

Country Status (5)

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US (1) US8748330B2 (enExample)
EP (1) EP2564455B1 (enExample)
JP (2) JP5973423B2 (enExample)
CN (1) CN102947989B (enExample)
WO (1) WO2011139705A1 (enExample)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9246177B2 (en) 2011-09-30 2016-01-26 Uchicago Argonne, Llc Bimetallic alloy electrocatalysts with multilayered platinum-skin surfaces
CA2851494A1 (en) 2011-10-10 2013-04-18 3M Innovative Properties Company Catalyst electrodes, and methods of making and using the same
JP6126130B2 (ja) 2011-12-29 2017-05-10 スリーエム イノベイティブ プロパティズ カンパニー 電気化学電池電極
CN106715760B (zh) 2014-09-08 2018-08-10 3M创新有限公司 用于二氧化碳电解槽的离子聚合物膜
KR20190076999A (ko) 2016-10-26 2019-07-02 쓰리엠 이노베이티브 프로퍼티즈 캄파니 촉매
WO2018080794A1 (en) 2016-10-26 2018-05-03 3M Innovative Properties Company Catalyst
EP3533099B1 (en) 2016-10-26 2020-11-25 3M Innovative Properties Company Pt-ni-ir catalyst for fuel cell
JP7055971B2 (ja) 2016-10-26 2022-04-19 スリーエム イノベイティブ プロパティズ カンパニー 燃料電池用pt-ni-ir触媒
WO2019177953A1 (en) 2018-03-12 2019-09-19 Laskowski Carl A Hydrocarbon polymers containing ammonium functionality
KR20200130333A (ko) 2018-03-12 2020-11-18 쓰리엠 이노베이티브 프로퍼티즈 캄파니 질소-함유 멀티-블록 공중합체 및 이의 제조 방법
WO2019177968A1 (en) 2018-03-12 2019-09-19 3M Innovative Properties Company Cationic polymers for use as anion exchange polyelectrolytes
US11834544B2 (en) 2018-03-12 2023-12-05 3M Innovative Properties Company Anion exchange membranes based on polymerization of long chain alpha olefins
WO2019193458A1 (en) 2018-04-04 2019-10-10 3M Innovative Properties Company Catalyst comprising pt, ni, and ta
WO2019193460A1 (en) 2018-04-04 2019-10-10 3M Innovative Properties Company Catalyst comprising pt, ni, and ru
CN112243541A (zh) 2018-04-04 2021-01-19 3M创新有限公司 催化剂
WO2019193461A1 (en) 2018-04-04 2019-10-10 3M Innovative Properties Company Catalyst comprising pt, ni, and cr
CN111971830B (zh) 2018-04-13 2023-10-27 3M创新有限公司 催化剂
CN118738423A (zh) 2018-04-13 2024-10-01 3M创新有限公司 催化剂
US11955645B2 (en) 2018-04-13 2024-04-09 3M Innovative Properties Company Catalyst
US10833332B2 (en) 2018-06-01 2020-11-10 Uchicago Argonne, Llc Systems and methods for scale-up synthesis multi-layered Pt-skin nanoparticle catalysts
US10637072B2 (en) 2018-06-12 2020-04-28 Uchicago Argonne, Llc Systems and methods for PTNI nanocages
CN110215920A (zh) * 2019-07-03 2019-09-10 中溶科技股份有限公司 丙酮加氢制备异丙醇用催化剂及其制备方法和应用
US12103087B2 (en) 2019-09-30 2024-10-01 Uchicago Argonne, Llc Systems and methods for platinum nanocatalyst synthesis via continuous flow reactor
EP4077415B1 (en) 2019-12-19 2023-06-14 3M Innovative Properties Company Copolymers containing pendant ionomeric carbosilane groups
US11679377B2 (en) 2020-01-28 2023-06-20 Uchicago Argonne, Llc Control of nanostructure and activity by alloying and/or segregation
US11628427B2 (en) 2020-01-28 2023-04-18 Uchicago Argonne, Llc Segregation induced core-shell structure
EP4493622A1 (en) 2022-03-14 2025-01-22 3M Innovative Properties Company Anion exchange membrane and method of making

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS59108272A (ja) * 1982-12-10 1984-06-22 Mitsubishi Electric Corp 燃料電池用電極の製造方法
US5039561A (en) 1986-08-25 1991-08-13 Minnesota Mining And Manufacturing Company Method for preparing an article having surface layer of uniformly oriented, crystalline, organic microstructures
US4812352A (en) 1986-08-25 1989-03-14 Minnesota Mining And Manufacturing Company Article having surface layer of uniformly oriented, crystalline, organic microstructures
US5176786A (en) 1988-07-13 1993-01-05 Minnesota Mining And Manufacturing Company Organic thin film controlled molecular epitaxy
US5069987A (en) * 1990-07-06 1991-12-03 Igr Enterprises, Inc. Solid oxide fuel cell assembly
US5336558A (en) 1991-06-24 1994-08-09 Minnesota Mining And Manufacturing Company Composite article comprising oriented microstructures
US5338430A (en) * 1992-12-23 1994-08-16 Minnesota Mining And Manufacturing Company Nanostructured electrode membranes
US5964537A (en) 1993-04-20 1999-10-12 Hill, Jr.; William C. Skate bearing inserts and method of removal and insertion into a skate wheel
GB9405518D0 (en) 1994-03-21 1994-05-04 Mupor Ltd Porous metal composite body
US5879828A (en) 1997-10-10 1999-03-09 Minnesota Mining And Manufacturing Company Membrane electrode assembly
US5879827A (en) 1997-10-10 1999-03-09 Minnesota Mining And Manufacturing Company Catalyst for membrane electrode assembly and method of making
US6482763B2 (en) * 1999-12-29 2002-11-19 3M Innovative Properties Company Suboxide fuel cell catalyst for enhanced reformate tolerance
EP1254711A1 (de) * 2001-05-05 2002-11-06 OMG AG & Co. KG Edelmetallhaltiger Trägerkatalysator und Verfahren zu seiner Herstellung
US7361426B2 (en) 2002-04-10 2008-04-22 Hewlett-Packard Development Company, L.P. Surface structure for enhancing catalyst reactivity and method of manufacturing thereof
US7419741B2 (en) 2003-09-29 2008-09-02 3M Innovative Properties Company Fuel cell cathode catalyst
JP2005251550A (ja) * 2004-03-04 2005-09-15 Toyota Motor Corp 燃料電池
US20060141138A1 (en) * 2004-12-29 2006-06-29 3M Innovative Properties Company Microwave annealing of membranes for use in fuel cell assemblies
WO2006088194A1 (ja) * 2005-02-21 2006-08-24 Nissan Motor Co., Ltd. 電極触媒およびその製造方法
JP2008540070A (ja) * 2005-04-29 2008-11-20 ユニバーシティー オブ ロチェスター 超薄多孔質ナノスケール膜、その製造方法および使用
US20070059452A1 (en) * 2005-09-13 2007-03-15 Debe Mark K Formation of nanostructured layers through continued screw dislocation growth
US7622217B2 (en) 2005-10-12 2009-11-24 3M Innovative Properties Company Fuel cell nanocatalyst

Also Published As

Publication number Publication date
US20130045859A1 (en) 2013-02-21
WO2011139705A1 (en) 2011-11-10
CN102947989B (zh) 2015-12-16
EP2564455B1 (en) 2016-09-28
CN102947989A (zh) 2013-02-27
JP2016135489A (ja) 2016-07-28
JP2013531551A (ja) 2013-08-08
US8748330B2 (en) 2014-06-10
EP2564455A1 (en) 2013-03-06

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