JP5957225B2 - 熱水条件下でのリチウム−金属−フォスフェイトの合成 - Google Patents

熱水条件下でのリチウム−金属−フォスフェイトの合成 Download PDF

Info

Publication number
JP5957225B2
JP5957225B2 JP2011542814A JP2011542814A JP5957225B2 JP 5957225 B2 JP5957225 B2 JP 5957225B2 JP 2011542814 A JP2011542814 A JP 2011542814A JP 2011542814 A JP2011542814 A JP 2011542814A JP 5957225 B2 JP5957225 B2 JP 5957225B2
Authority
JP
Japan
Prior art keywords
compound
mixture
oxidation state
general formula
present
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2011542814A
Other languages
English (en)
Japanese (ja)
Other versions
JP2012513945A5 (enExample
JP2012513945A (ja
Inventor
ブラムニク，キリル
ヒプスト，ハルトムート
カイト ラムペルト，ヨルダン
カイト ラムペルト，ヨルダン
シュレドレ，ズィモン
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JP2012513945A publication Critical patent/JP2012513945A/ja
Publication of JP2012513945A5 publication Critical patent/JP2012513945A5/ja
Application granted granted Critical
Publication of JP5957225B2 publication Critical patent/JP5957225B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/45—Phosphates containing plural metal, or metal and ammonium
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/624—Electric conductive fillers
    • H01M4/625—Carbon or graphite
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Compositions Of Oxide Ceramics (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
JP2011542814A 2008-12-29 2009-12-22 熱水条件下でのリチウム−金属−フォスフェイトの合成 Expired - Fee Related JP5957225B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US14111708P 2008-12-29 2008-12-29
US61/141,117 2008-12-29
PCT/EP2009/067742 WO2010076265A2 (en) 2008-12-29 2009-12-22 Synthesis of lithium-metal-phosphates under hydrothermal conditions

Publications (3)

Publication Number Publication Date
JP2012513945A JP2012513945A (ja) 2012-06-21
JP2012513945A5 JP2012513945A5 (enExample) 2016-06-30
JP5957225B2 true JP5957225B2 (ja) 2016-07-27

Family

ID=42199893

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2011542814A Expired - Fee Related JP5957225B2 (ja) 2008-12-29 2009-12-22 熱水条件下でのリチウム−金属−フォスフェイトの合成

Country Status (8)

Country Link
US (1) US9156693B2 (enExample)
EP (1) EP2382156B1 (enExample)
JP (1) JP5957225B2 (enExample)
KR (1) KR20110112387A (enExample)
CN (1) CN102272044A (enExample)
CA (1) CA2746965A1 (enExample)
TW (1) TWI474970B (enExample)
WO (1) WO2010076265A2 (enExample)

Families Citing this family (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW201010944A (en) * 2008-04-17 2010-03-16 Basf Se Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials
KR20110139281A (ko) 2009-03-17 2011-12-28 바스프 에스이 열수 조건 하의 리튬-철-포스페이트의 합성 방법
CA2873825C (en) 2009-05-22 2017-02-28 Sharp Kabushiki Kaisha Cathode active material containing lithium and having transition metal oxide, cathode containing lithium and having transition metal oxide, and nonaqueous secondary battery containing lithium and having transition metal oxide
WO2011019493A1 (en) * 2009-08-09 2011-02-17 American Lithium Energy Corporation Electroactive particles, and electrodes and batteries comprising the same
JP5551019B2 (ja) * 2009-09-02 2014-07-16 シャープ株式会社 正極活物質、正極及び非水二次電池
US9373844B2 (en) 2010-07-01 2016-06-21 Sharp Kabushiki Kaisha Positive electrode active substance containing lithium-containing metal oxide
JP5132727B2 (ja) 2010-07-12 2013-01-30 シャープ株式会社 正極活物質、正極及び非水電解質二次電池
WO2013091573A1 (zh) * 2011-12-21 2013-06-27 台湾立凯电能科技股份有限公司 具氧空缺的正极材料及其制法
CN102496714A (zh) * 2011-12-27 2012-06-13 天津力神电池股份有限公司 一种正极活性物质及其生产方法和所应用的锂离子电池
US20150162611A1 (en) * 2012-07-31 2015-06-11 Sharp Kabushiki Kaisha Cathode active material for non-aqueous electrolyte secondary battery
US20140147586A1 (en) * 2012-11-27 2014-05-29 Universite De Montreal Process for making an alkali metal oxyanion comprising iron
KR20140076107A (ko) * 2012-12-12 2014-06-20 한국전자통신연구원 리튬 알루미늄 티타늄 포스페이트 제조방법
GB201223473D0 (en) * 2012-12-28 2013-02-13 Faradion Ltd Metal-containing compounds
US10086351B2 (en) 2013-05-06 2018-10-02 Llang-Yuh Chen Multi-stage process for producing a material of a battery cell
CN103500829B (zh) * 2013-08-15 2016-12-28 江苏华东锂电技术研究院有限公司 磷酸亚铁锂的制备方法
CN103441265B (zh) * 2013-09-24 2015-10-28 上海空间电源研究所 一种共掺杂富锂复合正极材料及其制备方法
CN103779566A (zh) * 2014-02-21 2014-05-07 张萍 一种多元素掺杂磷酸锰锂-碳复合正极材料的制备方法
US10673065B2 (en) * 2015-04-07 2020-06-02 Brown University Cation energy storage device and methods
CN104966832A (zh) * 2015-06-02 2015-10-07 中国科学院青海盐湖研究所 一种电化学-化学反应制备金属氧化物或多金属氧化物电极材料的方法
CN106169570A (zh) * 2016-08-25 2016-11-30 合肥国轩高科动力能源有限公司 一种金属元素掺杂锂离子电池用磷酸钒锂正极材料的制备方法
DE102017106912A1 (de) 2017-03-30 2018-10-04 Chemische Fabrik Budenheim Kg Verfahren zur Herstellung von Fe(II)P / Fe(II)MetP-Verbindungen
DE102017106913A1 (de) 2017-03-30 2018-10-04 Chemische Fabrik Budenheim Kg Verfahren zur Herstellung von elektrisch leitenden Strukturen auf einem Trägermaterial
DE102017106911A1 (de) 2017-03-30 2018-10-04 Chemische Fabrik Budenheim Kg Verwendung von kristallwasserfreien Fe(II)-Verbindungen als Strahlungsabsorber
CN108530053B (zh) * 2018-03-30 2021-03-30 华南理工大学 一种pH值敏感变色无机材料及其制备方法
US11673112B2 (en) 2020-06-28 2023-06-13 eJoule, Inc. System and process with assisted gas flow inside a reaction chamber
US11121354B2 (en) 2019-06-28 2021-09-14 eJoule, Inc. System with power jet modules and method thereof
KR102761480B1 (ko) 2019-06-28 2025-02-03 이줄르, 인크 반응 챔버 내부에 보조 가스 흐름을 갖는 시스템 및 공정
US11376559B2 (en) 2019-06-28 2022-07-05 eJoule, Inc. Processing system and method for producing a particulate material
KR20240101831A (ko) * 2021-11-19 2024-07-02 크라이스타페이즈 프로덕츠, 인크. 산성 매질을 사용하여 불용성 용질 부가물을 형성하는 방법

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6514640B1 (en) 1996-04-23 2003-02-04 Board Of Regents, The University Of Texas System Cathode materials for secondary (rechargeable) lithium batteries
US6203946B1 (en) 1998-12-03 2001-03-20 Valence Technology, Inc. Lithium-containing phosphates, method of preparation, and uses thereof
US6528033B1 (en) 2000-01-18 2003-03-04 Valence Technology, Inc. Method of making lithium-containing materials
US6777132B2 (en) 2000-04-27 2004-08-17 Valence Technology, Inc. Alkali/transition metal halo—and hydroxy-phosphates and related electrode active materials
US8057769B2 (en) * 2000-04-27 2011-11-15 Valence Technology, Inc. Method for making phosphate-based electrode active materials
CA2483918C (en) * 2002-05-17 2007-01-09 Valence Technology, Inc. Synthesis of metal compounds useful as cathode active materials
CN100334755C (zh) * 2002-12-19 2007-08-29 威伦斯技术公司 电极活性材料及其制造方法
FR2852148B1 (fr) 2003-03-07 2014-04-11 Batscap Sa Materiau pour electrode composite, procede pour sa preparation
CN1233054C (zh) 2003-12-17 2005-12-21 北京科技大学 一种采用微波法制备LiFePO4材料的方法
JP2006155941A (ja) 2004-11-25 2006-06-15 Kyushu Univ 電極活物質の製造方法
DE102005012640B4 (de) * 2005-03-18 2015-02-05 Süd-Chemie Ip Gmbh & Co. Kg Kreisprozess zur nasschemischen Herstellung von Lithiummetallphosphaten
DE102005015613A1 (de) 2005-04-05 2006-10-12 Süd-Chemie AG Kristallines Ionenleitendes Nanomaterial und Verfahren zu seiner Herstellung
JP4869629B2 (ja) * 2005-05-30 2012-02-08 住友大阪セメント株式会社 リチウム電池用正極活物質の製造方法及びリチウム電池用正極活物質並びにリチウム電池
JP5084131B2 (ja) 2005-10-28 2012-11-28 トヨタ自動車株式会社 ＬｉＭｎＰＯ４の製造方法
EP1989747B1 (en) 2006-02-14 2017-04-12 Dow Global Technologies LLC Lithium manganese phosphate positive material for lithium secondary battery
EP2004548A1 (en) 2006-04-06 2008-12-24 High Power Lithium S.A. Synthesis of nanoparticles of lithium metal phosphate positive material for lithium secondary battery
JP5213213B2 (ja) * 2006-11-27 2013-06-19 日立マクセル株式会社 電気化学素子用活物質、その製造方法、および電気化学素子
JP5115697B2 (ja) 2007-05-22 2013-01-09 Ｎｅｃエナジーデバイス株式会社 リチウム二次電池用正極及びそれを用いたリチウム二次電池
TW201010944A (en) 2008-04-17 2010-03-16 Basf Se Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials
KR20110139281A (ko) 2009-03-17 2011-12-28 바스프 에스이 열수 조건 하의 리튬-철-포스페이트의 합성 방법
US20140147586A1 (en) * 2012-11-27 2014-05-29 Universite De Montreal Process for making an alkali metal oxyanion comprising iron

Also Published As

Publication number Publication date
KR20110112387A (ko) 2011-10-12
JP2012513945A (ja) 2012-06-21
CA2746965A1 (en) 2010-07-08
US9156693B2 (en) 2015-10-13
EP2382156A2 (en) 2011-11-02
US20110272639A1 (en) 2011-11-10
TWI474970B (zh) 2015-03-01
EP2382156B1 (en) 2016-05-25
TW201026598A (en) 2010-07-16
CN102272044A (zh) 2011-12-07
WO2010076265A3 (en) 2011-01-06
WO2010076265A2 (en) 2010-07-08

Similar Documents

Publication Publication Date Title
JP5957225B2 (ja) 熱水条件下でのリチウム−金属−フォスフェイトの合成
JP5701756B2 (ja) 熱水条件下におけるＬｉＦｅＰＯ４の製造
JP5722866B2 (ja) リチウム−イオン−フォスフェイトの合成
JP5318969B2 (ja) 電極活物質であるアニオン不足型リン酸遷移金属リチウム化合物、その製造方法、及びそれを利用した電気化学素子
KR101592051B1 (ko) 결정질 리튬-, 철- 및 포스페이트- 함유 물질의 제조 방법
KR101371356B1 (ko) pH 조절을 이용한 FePO₄제조 방법 및 이를 이용한 리튬이차전지 양극용 LiFePO₄/C 복합재 제조 방법
JP5886193B2 (ja) ＬｉＦｅＰＯ４−炭素合成物を製造するための方法
KR101070174B1 (ko) 전극 활물질인 음이온 부족형 리튬 전이금속 인산화합물, 그 제조방법, 및 그를 이용한 전기화학 소자
HK1144616B (en) Electrode active material for anion-deficient lithium transition metal phosphate compound, method of preparing same, and electrochemical device using same

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20121221

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20121221

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20140610

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20140829

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20140905

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20141003

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20150203

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20150423

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20150521

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20150611

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20150804

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20151124

A911 Transfer to examiner for re-examination before appeal (zenchi)

Free format text: JAPANESE INTERMEDIATE CODE: A911

Effective date: 20151202

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20160119

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20160407

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20160510

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20160531

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20160620

R150 Certificate of patent or registration of utility model

Ref document number: 5957225

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

LAPS Cancellation because of no payment of annual fees