JP5851397B2 - アミノ基を有する有機酸のアシル化のための連続的方法 - Google Patents
アミノ基を有する有機酸のアシル化のための連続的方法 Download PDFInfo
- Publication number
- JP5851397B2 JP5851397B2 JP2012518032A JP2012518032A JP5851397B2 JP 5851397 B2 JP5851397 B2 JP 5851397B2 JP 2012518032 A JP2012518032 A JP 2012518032A JP 2012518032 A JP2012518032 A JP 2012518032A JP 5851397 B2 JP5851397 B2 JP 5851397B2
- Authority
- JP
- Japan
- Prior art keywords
- acid
- group
- reaction
- microwave
- carbon atoms
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
- B01J19/122—Incoherent waves
- B01J19/126—Microwaves
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
- C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C233/45—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups
- C07C233/46—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom
- C07C233/47—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom having the carbon atom of the carboxamide group bound to a hydrogen atom or to a carbon atom of an acyclic saturated carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
- C07C303/22—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof from sulfonic acids, by reactions not involving the formation of sulfo or halosulfonyl groups; from sulfonic halides by reactions not involving the formation of halosulfonyl groups
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B6/00—Heating by electric, magnetic or electromagnetic fields
- H05B6/64—Heating using microwaves
- H05B6/70—Feed lines
- H05B6/701—Feed lines using microwave applicators
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B6/00—Heating by electric, magnetic or electromagnetic fields
- H05B6/64—Heating using microwaves
- H05B6/80—Apparatus for specific applications
- H05B6/806—Apparatus for specific applications for laboratory use
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00027—Process aspects
- B01J2219/00033—Continuous processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J2219/0873—Materials to be treated
- B01J2219/0881—Two or more materials
- B01J2219/0888—Liquid-liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J2219/0873—Materials to be treated
- B01J2219/0892—Materials to be treated involving catalytically active material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J2219/12—Processes employing electromagnetic waves
- B01J2219/1203—Incoherent waves
- B01J2219/1206—Microwaves
- B01J2219/1209—Features relating to the reactor or vessel
- B01J2219/1221—Features relating to the reactor or vessel the reactor per se
- B01J2219/1224—Form of the reactor
- B01J2219/1227—Reactors comprising tubes with open ends
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Clinical Laboratory Science (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102009031056.8 | 2009-06-30 | ||
| DE102009031056A DE102009031056A1 (de) | 2009-06-30 | 2009-06-30 | Kontinuierliches Verfahren zur Acrylierung von Aminogruppen tragenden organischen Säuren |
| PCT/EP2010/003444 WO2011000461A2 (de) | 2009-06-30 | 2010-06-09 | Kontinuierliches verfahren zur acylierung von aminogruppen tragenden organischen säuren |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012531450A JP2012531450A (ja) | 2012-12-10 |
| JP2012531450A5 JP2012531450A5 (https=) | 2014-09-11 |
| JP5851397B2 true JP5851397B2 (ja) | 2016-02-03 |
Family
ID=43128285
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012518032A Expired - Fee Related JP5851397B2 (ja) | 2009-06-30 | 2010-06-09 | アミノ基を有する有機酸のアシル化のための連続的方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20120090983A1 (https=) |
| EP (1) | EP2448913B1 (https=) |
| JP (1) | JP5851397B2 (https=) |
| KR (1) | KR20120060199A (https=) |
| CA (1) | CA2766933A1 (https=) |
| DE (1) | DE102009031056A1 (https=) |
| ES (1) | ES2410632T3 (https=) |
| WO (1) | WO2011000461A2 (https=) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102006047617B4 (de) * | 2006-10-09 | 2008-11-27 | Clariant International Limited | Verfahren zur Herstellung basischer (Meth)acrylamide |
| DE102006047619B4 (de) * | 2006-10-09 | 2008-11-13 | Clariant International Limited | Verfahren zur Herstellung basischer Fettsäureamide |
| DE102008017213B4 (de) * | 2008-04-04 | 2012-08-09 | Clariant International Limited | Kontinuierliches Verfahren zur Herstellung von Amiden aliphatischer Hydroxycarbonsäuren |
| DE102008017216B4 (de) * | 2008-04-04 | 2013-08-14 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Fettsäureamiden |
| DE102008017219A1 (de) * | 2008-04-04 | 2009-10-08 | Clariant International Ltd. | Verfahren zur Herstellung von Amiden in Gegenwart von überhitztem Wasser |
| DE102008017215B4 (de) * | 2008-04-04 | 2012-08-09 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Amiden ethylenisch ungesättigter Carbonsäuren |
| DE102008017218B4 (de) * | 2008-04-04 | 2011-09-22 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Amiden niederer aliphatischer Carbonsäuren |
| DE102008017214B4 (de) * | 2008-04-04 | 2012-02-16 | Clariant International Limited | Kontinuierliches Verfahren zur Herstellung von Fettsäurealkanolamiden |
| DE102008017217A1 (de) * | 2008-04-04 | 2009-10-08 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Amiden aromatischer Carbonsäuren |
| DE102009031059A1 (de) | 2009-06-30 | 2011-01-05 | Clariant International Ltd. | Vorrichtung zur kontinuierlichen Durchführung chemischer Reaktionen bei hohen Temperaturen |
| DE102009031058A1 (de) * | 2009-06-30 | 2011-01-27 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Amiden aromatischer Carbonsäuren |
| DE102009042523B4 (de) | 2009-09-22 | 2012-02-16 | Clariant International Ltd. | Vorrichtung und Verfahren zur kontinuierlichen Durchführung heterogen katalysierter chemischer Reaktionen bei hohen Temperaturen |
| DE102009042522A1 (de) | 2009-09-22 | 2011-04-07 | Clariant International Ltd. | Kontinuierliches Umesterungsverfahren |
| DE102010056564A1 (de) | 2010-12-30 | 2012-07-05 | Clariant International Limited | Hydroxylgruppen und Estergruppen tragende Polymere und Verfahren zu ihrer Herstellung |
| DE102010056565A1 (de) | 2010-12-30 | 2012-07-05 | Clariant International Ltd. | Verfahren zur Modifizierung Hydroxylgruppen tragender Polymere |
| CN106588710B (zh) * | 2016-12-12 | 2018-07-10 | 湖北远大生命科学与技术有限责任公司 | 一种应用微波合成n-酰基-n-甲基牛磺酸盐的方法 |
| EP3647303B1 (en) * | 2018-10-31 | 2022-08-31 | Clariant International Ltd | Process for preparing fatty acid chlorides and n-acyl amino acid salts |
| JP2021038146A (ja) * | 2019-08-30 | 2021-03-11 | マイクロ波化学株式会社 | N−アシルアミン類の製造方法 |
| IT202000030185A1 (it) * | 2020-12-09 | 2022-06-09 | Prod Gianni S R L | Alchilesteri di lipoamminoacidi quali spf boosters |
| CN114031516B (zh) * | 2021-11-23 | 2023-09-01 | 长沙普济生物科技股份有限公司 | 一种基于锆催化剂催化合成n-酰基氨基酸表面活性剂的方法 |
| CN114181119B (zh) * | 2021-12-18 | 2023-04-18 | 湖北天安日用化工有限公司 | 一种甲基月桂酰基牛磺酸钠的制备方法 |
| CN115160189B (zh) * | 2022-08-11 | 2023-06-16 | 广州天赐高新材料股份有限公司 | 一种n-酰基甲基牛磺酸钠的连续化制备方法 |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3461261A (en) * | 1966-10-31 | 1969-08-12 | Du Pont | Heating apparatus |
| US3836551A (en) * | 1970-01-30 | 1974-09-17 | Roehm Gmbh | Method for making salts of n-acylamino carboxylic acids |
| JPH01133910A (ja) * | 1987-06-08 | 1989-05-26 | Cil Inc | マイクロ波エネルギ−を使用して発煙硫酸から三酸化硫黄を発生させる方法及び装置 |
| WO1990003840A1 (en) * | 1988-10-10 | 1990-04-19 | Commonwealth Scientific And Industrial Research Organisation | Method and apparatus for continuous chemical reactions |
| JP2784789B2 (ja) * | 1989-03-27 | 1998-08-06 | 山本化成株式会社 | 2―アルキルアントラキノンの製造方法 |
| US6020580A (en) * | 1997-01-06 | 2000-02-01 | International Business Machines Corporation | Microwave applicator having a mechanical means for tuning |
| US6020579A (en) * | 1997-01-06 | 2000-02-01 | International Business Machines Corporation | Microwave applicator having a mechanical means for tuning |
| US5114684A (en) * | 1990-12-13 | 1992-05-19 | Serawaste Systems Corporation | In-line electromagnetic energy wave applicator |
| US5471037A (en) * | 1992-08-18 | 1995-11-28 | E. I. Du Pont De Nemours And Company | Process for preparing polymeric material with microwave |
| FR2698869B1 (fr) * | 1992-12-09 | 1995-02-24 | Morelle Jean | Acylaminoacides obtenus à partir de fibres issues du Bombyx Mori. |
| DE4433977A1 (de) * | 1994-09-23 | 1996-03-28 | Basf Ag | Verfahren zur Herstellung von N-Acylaminocarbonsäuren und N-Acylaminosulfonsäuren sowie deren Alkalimetallsalzen |
| US5710295A (en) * | 1995-06-06 | 1998-01-20 | Hampshire Chemical Corp. | Preparation of alkali metal acyl amino acids |
| US5646319A (en) * | 1995-06-23 | 1997-07-08 | The Procter & Gamble Company | Synthesis of N-acyl-N-alkylcarboxylates |
| FR2751830B1 (fr) * | 1996-07-23 | 1998-10-23 | Prolabo Sa | Dispositif pour realiser des reactions chimiques sous micro-ondes sur une grande quantite de produits |
| ES2256546T3 (es) * | 2001-10-19 | 2006-07-16 | Biotage Ab | Aparato para calentar por microondas. |
| FR2849343B1 (fr) * | 2002-12-23 | 2009-01-23 | Aldivia | Synthese chimique comportant un traitement thermique par chauffage dielectrique intermittent, combine a un systeme de recirculation |
| US7393920B2 (en) * | 2003-06-23 | 2008-07-01 | Cem Corporation | Microwave-assisted peptide synthesis |
| JP4759668B2 (ja) * | 2004-05-11 | 2011-08-31 | 株式会社Idx | マイクロ波加熱装置 |
| JP2006272055A (ja) * | 2005-03-28 | 2006-10-12 | Idx Corp | マイクロ波化学反応装置 |
| JP2006181533A (ja) * | 2004-12-28 | 2006-07-13 | Idx Corp | マイクロ波化学反応装置 |
| JP2007222696A (ja) * | 2005-12-23 | 2007-09-06 | Tokyo Electric Power Co Inc:The | マイクロ波反応用の触媒カラム及びそれを用いた分解処理方法 |
| CN100352793C (zh) * | 2006-01-20 | 2007-12-05 | 杨鸿生 | 用于以天然气制乙烯的槽波导微波化学反应设备及制备方法 |
| DE102006047619B4 (de) * | 2006-10-09 | 2008-11-13 | Clariant International Limited | Verfahren zur Herstellung basischer Fettsäureamide |
| WO2008043493A1 (de) * | 2006-10-09 | 2008-04-17 | Clariant Finance (Bvi) Limited | Verfahren zur herstellung von fettsäurealkanolamiden |
| US8128788B2 (en) * | 2008-09-19 | 2012-03-06 | Rf Thummim Technologies, Inc. | Method and apparatus for treating a process volume with multiple electromagnetic generators |
-
2009
- 2009-06-30 DE DE102009031056A patent/DE102009031056A1/de not_active Withdrawn
-
2010
- 2010-06-09 CA CA2766933A patent/CA2766933A1/en not_active Abandoned
- 2010-06-09 US US13/378,181 patent/US20120090983A1/en not_active Abandoned
- 2010-06-09 EP EP10724308.1A patent/EP2448913B1/de not_active Not-in-force
- 2010-06-09 WO PCT/EP2010/003444 patent/WO2011000461A2/de not_active Ceased
- 2010-06-09 ES ES10724308T patent/ES2410632T3/es active Active
- 2010-06-09 JP JP2012518032A patent/JP5851397B2/ja not_active Expired - Fee Related
- 2010-06-09 KR KR1020127002479A patent/KR20120060199A/ko not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| KR20120060199A (ko) | 2012-06-11 |
| US20120090983A1 (en) | 2012-04-19 |
| WO2011000461A3 (de) | 2011-03-31 |
| CA2766933A1 (en) | 2011-01-06 |
| JP2012531450A (ja) | 2012-12-10 |
| EP2448913A2 (de) | 2012-05-09 |
| WO2011000461A2 (de) | 2011-01-06 |
| ES2410632T3 (es) | 2013-07-02 |
| DE102009031056A1 (de) | 2011-01-27 |
| EP2448913B1 (de) | 2013-04-24 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP5851397B2 (ja) | アミノ基を有する有機酸のアシル化のための連続的方法 | |
| JP5773538B2 (ja) | 脂肪族カルボン酸のアミドの連続的製法 | |
| US8884040B2 (en) | Continuous method for producing fatty acid amides | |
| JP5731495B2 (ja) | 芳香族カルボン酸のアミドの連続的製法 | |
| CN101910115B (zh) | 制备脂族羟基羧酸的酰胺的连续方法 | |
| US20110083956A1 (en) | Continuous Method For Producing Fatty Acid Alkanol Amides | |
| US20110137081A1 (en) | Continuous Method For Producing Amides Of Low Aliphatic Carboxylic Acids | |
| US20110089019A1 (en) | Continuous Method For Producing Amides of Aromatic Carboxylic Acids | |
| JP2012531384A (ja) | 芳香族カルボン酸のエステルの連続的製造方法 | |
| JP2013505275A (ja) | 連続的エステル交換方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20130124 |
|
| A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20131211 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20140128 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20140425 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20140507 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20140527 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20140603 |
|
| A524 | Written submission of copy of amendment under article 19 pct |
Free format text: JAPANESE INTERMEDIATE CODE: A524 Effective date: 20140724 |
|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20140725 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20150212 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20150508 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20150609 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20150709 |
|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20150804 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20151104 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20151202 |
|
| R150 | Certificate of patent or registration of utility model |
Ref document number: 5851397 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| LAPS | Cancellation because of no payment of annual fees |