JP5823982B2 - カルバメートの熱的分離によるイソシアネートの調製方法 - Google Patents

カルバメートの熱的分離によるイソシアネートの調製方法 Download PDF

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Publication number
JP5823982B2
JP5823982B2 JP2012549324A JP2012549324A JP5823982B2 JP 5823982 B2 JP5823982 B2 JP 5823982B2 JP 2012549324 A JP2012549324 A JP 2012549324A JP 2012549324 A JP2012549324 A JP 2012549324A JP 5823982 B2 JP5823982 B2 JP 5823982B2
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carbamate
column
inert solvent
alcohol
dissociation
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JP2012549324A
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Japanese (ja)
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JP2013517312A (ja
JP2013517312A5 (https=
Inventor
ボック，ミヒャエル
フランツケ，アクセル
バウマン，ローベルト
シュトレファー，エックハルト
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/04—Preparation of derivatives of isocyanic acid from or via carbamates or carbamoyl halides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2012549324A 2010-01-19 2011-01-18 カルバメートの熱的分離によるイソシアネートの調製方法 Expired - Fee Related JP5823982B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP10151089.9 2010-01-19
EP10151089 2010-01-19
PCT/EP2011/050557 WO2011089098A1 (de) 2010-01-19 2011-01-18 Verfahren zur herstellung von isocyanaten durch thermische spaltung von carbamaten

Publications (3)

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JP2013517312A JP2013517312A (ja) 2013-05-16
JP2013517312A5 JP2013517312A5 (https=) 2015-08-27
JP5823982B2 true JP5823982B2 (ja) 2015-11-25

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JP2012549324A Expired - Fee Related JP5823982B2 (ja) 2010-01-19 2011-01-18 カルバメートの熱的分離によるイソシアネートの調製方法

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EP (1) EP2526085B1 (https=)
JP (1) JP5823982B2 (https=)
KR (1) KR20120120945A (https=)
CN (1) CN102712580B (https=)
BR (1) BR112012017877A2 (https=)
ES (1) ES2552837T3 (https=)
HU (1) HUE028076T2 (https=)
PL (1) PL2526085T3 (https=)
PT (1) PT2526085E (https=)
WO (1) WO2011089098A1 (https=)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5612115B2 (ja) * 2010-10-04 2014-10-22 旭化成ケミカルズ株式会社 分離方法及びイソシアネートの製造方法
US8933262B2 (en) 2011-05-24 2015-01-13 Basf Se Process for preparing polyisocyanates from biomass
CN103848758A (zh) * 2012-12-06 2014-06-11 中国科学院成都有机化学有限公司 一种催化热分解制备异氰酸酯的方法
US10898217B2 (en) 2014-05-09 2021-01-26 Kci Licensing, Inc. Dressing providing apertures with multiple orifice sizes for negative-pressure therapy
EP3791837B1 (en) 2014-05-09 2024-07-17 Solventum Intellectual Properties Company Disruptive dressing for use with negative pressure and fluid instillation
WO2015172104A1 (en) 2014-05-09 2015-11-12 Kci Licensing, Inc. Debriding dressing for use with negative pressure and fluid instillation
EP3797744A1 (en) 2014-05-09 2021-03-31 3M Innovative Properties Company Dressing with contracting layer for linear tissue sites
WO2016120167A1 (de) 2015-01-30 2016-08-04 Basf Se Nebenproduktarme polyphenylenpolymethylenpolyisocyanate
JP6757468B2 (ja) * 2017-05-15 2020-09-16 旭化成株式会社 イソシアネートの製造方法
EP3450424A1 (de) * 2017-09-04 2019-03-06 Covestro Deutschland AG Verfahren zur herstellung von isocyanaten
EP3876885B1 (en) 2018-11-08 2023-11-29 3M Innovative Properties Company Wound dressing with semi-rigid support to increase disruption using perforated dressing and negative pressure wound therapy
EP4069171A1 (en) 2019-12-05 2022-10-12 KCI Licensing, Inc. Multi-layer negative pressure incisional wound therapy dressing

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3215591A1 (de) 1982-04-27 1983-10-27 Bayer Ag, 5090 Leverkusen Verfahren zur kontinuierlichen thermischen spaltung von carbamidsaeureestern
JPS60231640A (ja) * 1984-05-02 1985-11-18 Asahi Chem Ind Co Ltd イソシアナ−トの連続的製法
JPH02250857A (ja) * 1989-03-23 1990-10-08 Sumitomo Metal Ind Ltd ポリイソシアネートの製造方法
US5326903A (en) 1992-01-10 1994-07-05 Nippon Shokubai Co., Ltd. Process for preparing isocyanates using sintered oxides
JPH05194351A (ja) * 1992-01-22 1993-08-03 Nkk Corp イソシアネート化合物の連続的製造装置及び方法
DE59705128D1 (de) * 1996-03-15 2001-12-06 Bayer Ag Verfahren zur thermischen Spaltung von Carbamidsäureestern
DE19907648A1 (de) 1999-02-23 2000-08-24 Basf Ag Verfahren zur Herstellung von Isocyanaten durch Spaltung von Urethanen
DE10329491A1 (de) 2003-07-01 2005-01-27 Basf Ag Reaktor für gas/flüssig oder gas/flüssig/fest Reaktionen
CN101200436A (zh) * 2006-12-31 2008-06-18 中国科学院成都有机化学有限公司 连续制备1,6-六亚甲基二异氰酸酯的方法
PL2265571T3 (pl) 2008-03-18 2015-08-31 Basf Se Sposób wytwarzania uretanów z jedno- i dwufunkcyjnych amin aromatycznych

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Publication number Publication date
WO2011089098A1 (de) 2011-07-28
PT2526085E (pt) 2015-11-24
KR20120120945A (ko) 2012-11-02
CN102712580B (zh) 2014-11-26
PL2526085T3 (pl) 2016-01-29
JP2013517312A (ja) 2013-05-16
ES2552837T3 (es) 2015-12-02
CN102712580A (zh) 2012-10-03
EP2526085A1 (de) 2012-11-28
HUE028076T2 (en) 2016-11-28
BR112012017877A2 (pt) 2016-05-03
EP2526085B1 (de) 2015-08-12

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