JP5759903B2 - 単結晶ダイヤモンドを製造するための高圧高温(hpht)方法 - Google Patents
単結晶ダイヤモンドを製造するための高圧高温(hpht)方法 Download PDFInfo
- Publication number
- JP5759903B2 JP5759903B2 JP2011545791A JP2011545791A JP5759903B2 JP 5759903 B2 JP5759903 B2 JP 5759903B2 JP 2011545791 A JP2011545791 A JP 2011545791A JP 2011545791 A JP2011545791 A JP 2011545791A JP 5759903 B2 JP5759903 B2 JP 5759903B2
- Authority
- JP
- Japan
- Prior art keywords
- seed
- single crystal
- growth
- crystal diamond
- growth surface
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/02—Elements
- C30B29/04—Diamond
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B01J23/745—Iron
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B01J23/75—Cobalt
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B01J23/755—Nickel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/06—Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies
- B01J3/062—Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies characterised by the composition of the materials to be processed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2203/00—Processes utilising sub- or super atmospheric pressure
- B01J2203/06—High pressure synthesis
- B01J2203/0605—Composition of the material to be processed
- B01J2203/061—Graphite
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2203/00—Processes utilising sub- or super atmospheric pressure
- B01J2203/06—High pressure synthesis
- B01J2203/0605—Composition of the material to be processed
- B01J2203/062—Diamond
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2203/00—Processes utilising sub- or super atmospheric pressure
- B01J2203/06—High pressure synthesis
- B01J2203/065—Composition of the material produced
- B01J2203/0655—Diamond
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2203/00—Processes utilising sub- or super atmospheric pressure
- B01J2203/06—High pressure synthesis
- B01J2203/0675—Structural or physico-chemical features of the materials processed
- B01J2203/068—Crystal growth
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Metallurgy (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Carbon And Carbon Compounds (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB0900771.7 | 2009-01-16 | ||
| GB0900771A GB0900771D0 (en) | 2009-01-16 | 2009-01-16 | Diamond |
| PCT/GB2010/000059 WO2010082029A1 (en) | 2009-01-16 | 2010-01-15 | High pressure high temperature (hpht) method for the production of single crystal diamonds |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012515079A JP2012515079A (ja) | 2012-07-05 |
| JP2012515079A5 JP2012515079A5 (enExample) | 2013-03-07 |
| JP5759903B2 true JP5759903B2 (ja) | 2015-08-05 |
Family
ID=40445953
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011545791A Active JP5759903B2 (ja) | 2009-01-16 | 2010-01-15 | 単結晶ダイヤモンドを製造するための高圧高温(hpht)方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US9039832B2 (enExample) |
| EP (1) | EP2379214B1 (enExample) |
| JP (1) | JP5759903B2 (enExample) |
| KR (1) | KR20110104562A (enExample) |
| GB (1) | GB0900771D0 (enExample) |
| WO (1) | WO2010082029A1 (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB0704516D0 (en) | 2007-03-08 | 2007-04-18 | Element Six Ltd | Diamond |
| US9017633B2 (en) * | 2010-01-18 | 2015-04-28 | Element Six Technologies Limited | CVD single crystal diamond material |
| GB201204533D0 (en) * | 2012-03-15 | 2012-04-25 | Element Six Ltd | Process for manufacturing synthetic single crystal diamond material |
| TWI605113B (zh) * | 2012-07-05 | 2017-11-11 | 江陰貝卡爾特合金材料有限公司 | 具有立方八面體鑽石粒子之固定磨料鋸線 |
| KR101811761B1 (ko) * | 2014-10-11 | 2017-12-22 | 허난 페이머스 다이아몬드 인더스트리얼 씨오. 엘티디 | 거친 표면의 금강석의 합성방법 |
| JP6217949B2 (ja) * | 2016-11-10 | 2017-10-25 | 住友電気工業株式会社 | 単結晶ダイヤモンド |
| CN111020698A (zh) * | 2019-12-16 | 2020-04-17 | 吉林大学 | 一种异形{111}籽晶合成金刚石单晶的方法 |
| CN112892411B (zh) * | 2021-01-25 | 2022-05-31 | 四川大学 | 一种高温高压下生长大颗粒金刚石的方法 |
| WO2022210934A1 (ja) * | 2021-03-31 | 2022-10-06 | 住友電気工業株式会社 | 単結晶ダイヤモンド及びその製造方法 |
| WO2022210723A1 (ja) * | 2021-03-31 | 2022-10-06 | 住友電気工業株式会社 | 単結晶ダイヤモンド及びこれを備えるダイヤモンド複合体 |
| KR20240098386A (ko) * | 2022-12-21 | 2024-06-28 | 일진다이아몬드(주) | 초정밀 연삭용 다이아몬드 지립 및 그 제조방법 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4034066A (en) | 1973-11-02 | 1977-07-05 | General Electric Company | Method and high pressure reaction vessel for quality control of diamond growth on diamond seed |
| US4617181A (en) | 1983-07-01 | 1986-10-14 | Sumitomo Electric Industries, Ltd. | Synthetic diamond heat sink |
| JPH0779958B2 (ja) | 1987-05-08 | 1995-08-30 | 住友電気工業株式会社 | 大型ダイヤモンドの合成方法 |
| JP2932559B2 (ja) * | 1990-01-19 | 1999-08-09 | 住友電気工業株式会社 | 大型ダイヤモンド単結晶の合成方法 |
| AU4245693A (en) | 1992-05-04 | 1993-11-29 | Case Western Reserve University | Growth of diamond crystals |
| US5474021A (en) | 1992-09-24 | 1995-12-12 | Sumitomo Electric Industries, Ltd. | Epitaxial growth of diamond from vapor phase |
| ATE248020T1 (de) * | 1995-12-21 | 2003-09-15 | Element Six Pty Ltd | Diamantsynthese |
| JP4032482B2 (ja) | 1997-04-18 | 2008-01-16 | 住友電気工業株式会社 | 単結晶ダイヤモンドの製造方法 |
| EP1671726B1 (en) | 2003-10-10 | 2013-02-13 | Sumitomo Electric Industries, Ltd. | Diamond tool |
| JP5362993B2 (ja) | 2004-12-09 | 2013-12-11 | エレメント シックス テクノロジーズ (プロプライアタリー)リミテッド | ダイヤモンド結晶の結晶完全性を改良する方法 |
| JP5002982B2 (ja) | 2005-04-15 | 2012-08-15 | 住友電気工業株式会社 | 単結晶ダイヤモンドの製造方法 |
| JP4613314B2 (ja) | 2005-05-26 | 2011-01-19 | 独立行政法人産業技術総合研究所 | 単結晶の製造方法 |
| JP5323492B2 (ja) | 2005-12-09 | 2013-10-23 | エレメント シックス テクノロジーズ (プロプライアタリー) リミテッド | 高結晶品質の合成ダイヤモンド |
| GB0704516D0 (en) * | 2007-03-08 | 2007-04-18 | Element Six Ltd | Diamond |
-
2009
- 2009-01-16 GB GB0900771A patent/GB0900771D0/en not_active Ceased
-
2010
- 2010-01-15 KR KR1020117018874A patent/KR20110104562A/ko not_active Withdrawn
- 2010-01-15 JP JP2011545791A patent/JP5759903B2/ja active Active
- 2010-01-15 US US13/144,512 patent/US9039832B2/en active Active
- 2010-01-15 EP EP10700758.5A patent/EP2379214B1/en active Active
- 2010-01-15 WO PCT/GB2010/000059 patent/WO2010082029A1/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| GB0900771D0 (en) | 2009-03-04 |
| JP2012515079A (ja) | 2012-07-05 |
| CN103097011A (zh) | 2013-05-08 |
| US9039832B2 (en) | 2015-05-26 |
| US20110271900A1 (en) | 2011-11-10 |
| CN103097011B (zh) | 2015-11-25 |
| WO2010082029A1 (en) | 2010-07-22 |
| EP2379214B1 (en) | 2017-11-15 |
| KR20110104562A (ko) | 2011-09-22 |
| EP2379214A1 (en) | 2011-10-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP5759903B2 (ja) | 単結晶ダイヤモンドを製造するための高圧高温(hpht)方法 | |
| JP5522606B2 (ja) | ダイヤモンド | |
| US5882786A (en) | Gemstones formed of silicon carbide with diamond coating | |
| JP4972554B2 (ja) | 極超靭性cvd単結晶ダイヤモンドおよびその三次元成長 | |
| CN102959138B (zh) | 单晶金刚石材料 | |
| US7404399B2 (en) | Diamond tool, synthetic single crystal diamond and method of synthesizing single crystal diamond, and diamond jewelry | |
| KR20170126926A (ko) | 단결정 다이아몬드 및 이것을 성장시키는 방법 | |
| EP1848526B1 (en) | A method of improving the crystalline perfection of diamond crystals | |
| JP2024538212A (ja) | Cvd単結晶ダイヤモンド | |
| Hei et al. | Interface features of the HPHT Ib substrate and homoepitaxial CVD diamond layer | |
| JP5547774B2 (ja) | ダイヤモンド結晶の結晶完全性を改良する方法 | |
| CN103097011B9 (zh) | 用于制备单晶金刚石的高温高压(hpht)方法 | |
| GB2535572A (en) | A method of fabricating single crystal synthetic diamond products and single crystal synthetic diamond products fabricated using said method | |
| RU2334550C2 (ru) | Алмазный инструмент, синтетический монокристаллический алмаз, способ синтеза монокристаллического алмаза и алмазное ювелирное изделие | |
| JPH06227895A (ja) | ダイヤモンドの合成法 | |
| JPH0576747A (ja) | ダイヤモンド単結晶の合成方法 | |
| JPH0442360B2 (enExample) |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20130115 |
|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20130115 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20140604 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20140903 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20140910 |
|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20141204 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20150507 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20150608 |
|
| R150 | Certificate of patent or registration of utility model |
Ref document number: 5759903 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |