JP5717735B2 - 気相におけるイソシアネートの調製方法 - Google Patents
気相におけるイソシアネートの調製方法 Download PDFInfo
- Publication number
- JP5717735B2 JP5717735B2 JP2012518791A JP2012518791A JP5717735B2 JP 5717735 B2 JP5717735 B2 JP 5717735B2 JP 2012518791 A JP2012518791 A JP 2012518791A JP 2012518791 A JP2012518791 A JP 2012518791A JP 5717735 B2 JP5717735 B2 JP 5717735B2
- Authority
- JP
- Japan
- Prior art keywords
- amine
- reaction
- inert
- reactor
- phosgene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
- C07C255/49—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
- C07C255/50—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton to carbon atoms of non-condensed six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/18—Separation; Purification; Stabilisation; Use of additives
- C07C263/20—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102009032414.3 | 2009-07-09 | ||
| DE102009032414A DE102009032414A1 (de) | 2009-07-09 | 2009-07-09 | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| PCT/EP2010/003915 WO2011003531A1 (de) | 2009-07-09 | 2010-06-26 | Verfahren zur herstellung von isocyanaten in der gasphase |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012532159A JP2012532159A (ja) | 2012-12-13 |
| JP2012532159A5 JP2012532159A5 (cg-RX-API-DMAC7.html) | 2013-08-15 |
| JP5717735B2 true JP5717735B2 (ja) | 2015-05-13 |
Family
ID=42599688
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012518791A Expired - Fee Related JP5717735B2 (ja) | 2009-07-09 | 2010-06-26 | 気相におけるイソシアネートの調製方法 |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US8563767B2 (cg-RX-API-DMAC7.html) |
| EP (1) | EP2451774B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JP5717735B2 (cg-RX-API-DMAC7.html) |
| KR (1) | KR20120038436A (cg-RX-API-DMAC7.html) |
| CN (1) | CN102498092B (cg-RX-API-DMAC7.html) |
| DE (1) | DE102009032414A1 (cg-RX-API-DMAC7.html) |
| HU (1) | HUE025762T2 (cg-RX-API-DMAC7.html) |
| IN (1) | IN2012DN00244A (cg-RX-API-DMAC7.html) |
| RU (1) | RU2543381C2 (cg-RX-API-DMAC7.html) |
| TW (1) | TWI457315B (cg-RX-API-DMAC7.html) |
| WO (1) | WO2011003531A1 (cg-RX-API-DMAC7.html) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2559658A1 (en) * | 2011-08-19 | 2013-02-20 | Huntsman International LLC | A process to separate phosgene and hydrogen chloride from a fluid stream comprising phosgene and hydrogen chloride |
| US8816126B2 (en) | 2011-09-02 | 2014-08-26 | Basf Se | Process for preparing isocyanates |
| WO2013029918A1 (de) * | 2011-09-02 | 2013-03-07 | Basf Se | Verfahren zur herstellung von isocyanaten |
| CN105214568B (zh) | 2014-06-10 | 2018-04-20 | 万华化学集团股份有限公司 | 一种加热器、该加热器的用途和应用该加热器制备异氰酸酯的方法 |
| US10851048B2 (en) * | 2018-11-13 | 2020-12-01 | Covestro Deutschland Ag | Process for preparing an isocyanate by partly adiabatically operated phosgenation of the corresponding amine |
| CN114044745A (zh) * | 2021-12-06 | 2022-02-15 | 甘肃银光聚银化工有限公司 | 一种气相光气化法合成1,5-戊二异氰酸酯的方法 |
| CN114195683B (zh) * | 2021-12-14 | 2023-03-17 | 山东新和成维生素有限公司 | 一种采用气相反应器制备异氰酸酯的方法及气相反应器 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3714439A1 (de) | 1987-04-30 | 1988-11-10 | Bayer Ag | Verfahren zur herstellung von (cyclo)aliphatischen diisocyanaten |
| DE4217019A1 (de) | 1992-05-22 | 1993-11-25 | Bayer Ag | Verfahren zur Herstellung von aromatischen Diisocyanaten |
| FR2723585B1 (fr) * | 1994-08-12 | 1996-09-27 | Rhone Poulenc Chimie | Procede de preparation de composes du type polyisocyanates aromatiques en phase gazeuse. |
| DE19523385A1 (de) | 1995-06-23 | 1997-01-09 | Bayer Ag | Verfahren zur Herstellung von Triisocyanaten |
| DE10222023A1 (de) | 2002-05-17 | 2003-11-27 | Bayer Ag | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| DE10235476A1 (de) | 2002-08-02 | 2004-02-12 | Basf Ag | Integriertes Verfahren zur Herstellung von Isocyanaten |
| DE10245704A1 (de) | 2002-09-30 | 2004-04-01 | Bayer Ag | Verfahren zum Quenchen eines gasförmigen Reaktionsgemisches bei der Gasphasenphosgenierung von Diaminen |
| DE10307141A1 (de) | 2003-02-20 | 2004-09-02 | Bayer Ag | Verfahren zur Herstellung von (Poly)isocyanaten in der Gasphase |
| DE102005036870A1 (de) | 2005-08-02 | 2007-02-08 | Bayer Materialscience Ag | Verfahren zur Gasphasenphosgenierung |
| DE102005037328A1 (de) * | 2005-08-04 | 2007-02-08 | Basf Ag | Verfahren zur Herstellung von Isocyanaten |
| US20070049482A1 (en) | 2005-08-11 | 2007-03-01 | Shin-Etsu Chemical Co., Ltd. | Synthetic quartz glass substrate for excimer lasers and making method |
| DE102005042392A1 (de) | 2005-09-06 | 2007-03-08 | Basf Ag | Verfahren zur Herstellung von Isocyanaten |
| JP5460327B2 (ja) | 2006-11-07 | 2014-04-02 | ビーエーエスエフ ソシエタス・ヨーロピア | イソシアネートの製造方法 |
| DE102006058633A1 (de) | 2006-12-13 | 2008-06-19 | Bayer Materialscience Ag | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| DE102006058634A1 (de) | 2006-12-13 | 2008-06-19 | Bayer Materialscience Ag | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| PT2511259T (pt) * | 2007-01-17 | 2016-07-01 | Basf Se | Processo para a produção de isocianatos |
| EP2179985B1 (en) * | 2007-08-21 | 2013-04-10 | Ningbo Wanhua Polyurethanes Co., Ltd. | Jet reactor with flow ducts and process for preparing isocyanates using it |
| US8558026B2 (en) * | 2007-08-30 | 2013-10-15 | Basf Se | Method for producing isocyanates |
| WO2009037179A1 (de) * | 2007-09-19 | 2009-03-26 | Basf Se | Verfahren zur herstellung von isocyanaten |
| EP2060560B1 (en) * | 2007-11-14 | 2016-04-13 | Covestro Deutschland AG | Preparation of light-colored isocyanates |
-
2009
- 2009-07-09 DE DE102009032414A patent/DE102009032414A1/de not_active Withdrawn
-
2010
- 2010-06-26 KR KR1020127000445A patent/KR20120038436A/ko not_active Abandoned
- 2010-06-26 RU RU2012104325/04A patent/RU2543381C2/ru not_active IP Right Cessation
- 2010-06-26 JP JP2012518791A patent/JP5717735B2/ja not_active Expired - Fee Related
- 2010-06-26 CN CN201080031231.9A patent/CN102498092B/zh active Active
- 2010-06-26 US US13/382,609 patent/US8563767B2/en active Active
- 2010-06-26 IN IN244DEN2012 patent/IN2012DN00244A/en unknown
- 2010-06-26 EP EP10729809.3A patent/EP2451774B1/de active Active
- 2010-06-26 HU HUE10729809A patent/HUE025762T2/en unknown
- 2010-06-26 WO PCT/EP2010/003915 patent/WO2011003531A1/de not_active Ceased
- 2010-07-08 TW TW099122408A patent/TWI457315B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| TW201116506A (en) | 2011-05-16 |
| HUE025762T2 (en) | 2016-05-30 |
| RU2012104325A (ru) | 2013-08-20 |
| DE102009032414A1 (de) | 2011-01-13 |
| TWI457315B (zh) | 2014-10-21 |
| EP2451774B1 (de) | 2015-07-22 |
| IN2012DN00244A (cg-RX-API-DMAC7.html) | 2015-08-21 |
| US8563767B2 (en) | 2013-10-22 |
| US20120302785A1 (en) | 2012-11-29 |
| EP2451774A1 (de) | 2012-05-16 |
| RU2543381C2 (ru) | 2015-02-27 |
| WO2011003531A1 (de) | 2011-01-13 |
| CN102498092A (zh) | 2012-06-13 |
| JP2012532159A (ja) | 2012-12-13 |
| KR20120038436A (ko) | 2012-04-23 |
| CN102498092B (zh) | 2015-01-14 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101205197B (zh) | 在气相中制备异氰酸酯的方法 | |
| JP3219903B2 (ja) | 芳香族ジイソシアネートの製造方法 | |
| JP5574684B2 (ja) | 気相中でイソシアナートを製造する方法 | |
| JP5366393B2 (ja) | 気相中でのイソシアネートの製造方法 | |
| JP5717735B2 (ja) | 気相におけるイソシアネートの調製方法 | |
| TWI429619B (zh) | 氣相中芳香族二異氰酸酯之製造方法 | |
| JP2009051838A (ja) | 低塩素イソシアネートの製造方法 | |
| KR102733348B1 (ko) | 디이소시아네이트의 기체 상 제조 방법 | |
| JP5851488B2 (ja) | 気相におけるイソシアネートの製造方法 | |
| HK1130766A (en) | Process for the production of aromatic diisocyanates in the gas phase | |
| HK1122792A (en) | Process for the preparation of isocyanates in the gas phase | |
| HK1118532A (en) | Process for the preparation of isocyanates in the gas phase |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20130625 |
|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20130625 |
|
| A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20140515 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20140520 |
|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20140819 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20150217 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20150317 |
|
| R150 | Certificate of patent or registration of utility model |
Ref document number: 5717735 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| RD02 | Notification of acceptance of power of attorney |
Free format text: JAPANESE INTERMEDIATE CODE: R3D02 |
|
| LAPS | Cancellation because of no payment of annual fees |