JP5600336B2 - ガス分離装置およびガス分離方法 - Google Patents

ガス分離装置およびガス分離方法 Download PDF

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Publication number
JP5600336B2
JP5600336B2 JP2012137888A JP2012137888A JP5600336B2 JP 5600336 B2 JP5600336 B2 JP 5600336B2 JP 2012137888 A JP2012137888 A JP 2012137888A JP 2012137888 A JP2012137888 A JP 2012137888A JP 5600336 B2 JP5600336 B2 JP 5600336B2
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Japan
Prior art keywords
gas
adsorption tower
separation
adsorbent
mixed gas
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Expired - Fee Related
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JP2012137888A
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English (en)
Japanese (ja)
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JP2014000531A (ja
JP2014000531A5 (enExample
Inventor
智也 藤峰
良文 中島
順 泉
則雄 三浦
正 谷内
学 黒木
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JNC Engineering Co Ltd
Kyushu University
Tokyo Gas Co Ltd
Adsorption Technology Industries Co Ltd
Original Assignee
JNC Engineering Co Ltd
Kyushu University
Tokyo Gas Co Ltd
Adsorption Technology Industries Co Ltd
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Application filed by JNC Engineering Co Ltd, Kyushu University, Tokyo Gas Co Ltd, Adsorption Technology Industries Co Ltd filed Critical JNC Engineering Co Ltd
Priority to JP2012137888A priority Critical patent/JP5600336B2/ja
Priority to IN10865DEN2014 priority patent/IN2014DN10865A/en
Priority to US14/407,558 priority patent/US9216374B2/en
Priority to EP13806229.4A priority patent/EP2862618B1/en
Priority to PCT/JP2013/066448 priority patent/WO2013191097A1/ja
Publication of JP2014000531A publication Critical patent/JP2014000531A/ja
Publication of JP2014000531A5 publication Critical patent/JP2014000531A5/ja
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0407—Constructional details of adsorbing systems
    • B01D53/0423—Beds in columns
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0407—Constructional details of adsorbing systems
    • B01D53/0438—Cooling or heating systems
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0454—Controlling adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/343—Heat recovery
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/041—Oxides or hydroxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/34—Regenerating or reactivating
    • B—PERFORMING OPERATIONS; TRANSPORTING
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    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/34—Regenerating or reactivating
    • B01J20/3433—Regenerating or reactivating of sorbents or filter aids other than those covered by B01J20/3408 - B01J20/3425
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/34—Regenerating or reactivating
    • B01J20/3491—Regenerating or reactivating by pressure treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/02—Preparation of oxygen
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    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/02—Preparation of oxygen
    • C01B13/0229—Purification or separation processes
    • C01B13/0248—Physical processing only
    • C01B13/0259—Physical processing only by adsorption on solids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/04—Purification or separation of nitrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
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    • C01B21/04—Purification or separation of nitrogen
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    • C01B21/045—Physical processing only by adsorption in solids
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    • C01B23/00—Noble gases; Compounds thereof
    • C01B23/001—Purification or separation processes of noble gases
    • C01B23/0036—Physical processing only
    • C01B23/0052—Physical processing only by adsorption in solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/112—Metals or metal compounds not provided for in B01D2253/104 or B01D2253/106
    • B01D2253/1124—Metal oxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/10—Nitrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/10—Single element gases other than halogens
    • B01D2257/104—Oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40007—Controlling pressure or temperature swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/402—Further details for adsorption processes and devices using two beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/65—Employing advanced heat integration, e.g. Pinch technology
    • B01D2259/655—Employing advanced heat integration, e.g. Pinch technology using heat storage materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/60—Use in several different columns
    • B01J2220/606—Use in several different columns parallel disposed columns
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    • C01B2210/00—Purification or separation of specific gases
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    • C01B2210/0034—Argon
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    • C01B2210/0037—Xenon

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  • Chemical & Material Sciences (AREA)
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  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
JP2012137888A 2012-06-19 2012-06-19 ガス分離装置およびガス分離方法 Expired - Fee Related JP5600336B2 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
JP2012137888A JP5600336B2 (ja) 2012-06-19 2012-06-19 ガス分離装置およびガス分離方法
IN10865DEN2014 IN2014DN10865A (enExample) 2012-06-19 2013-06-14
US14/407,558 US9216374B2 (en) 2012-06-19 2013-06-14 Gas separation device and gas separation method
EP13806229.4A EP2862618B1 (en) 2012-06-19 2013-06-14 Gas separation device and gas separation method
PCT/JP2013/066448 WO2013191097A1 (ja) 2012-06-19 2013-06-14 ガス分離装置およびガス分離方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2012137888A JP5600336B2 (ja) 2012-06-19 2012-06-19 ガス分離装置およびガス分離方法

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JP2014000531A JP2014000531A (ja) 2014-01-09
JP2014000531A5 JP2014000531A5 (enExample) 2014-03-06
JP5600336B2 true JP5600336B2 (ja) 2014-10-01

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JP2012137888A Expired - Fee Related JP5600336B2 (ja) 2012-06-19 2012-06-19 ガス分離装置およびガス分離方法

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US (1) US9216374B2 (enExample)
EP (1) EP2862618B1 (enExample)
JP (1) JP5600336B2 (enExample)
IN (1) IN2014DN10865A (enExample)
WO (1) WO2013191097A1 (enExample)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6378981B2 (ja) * 2014-09-05 2018-08-22 フタムラ化学株式会社 真空下で圧力変動吸着を行うガス分離装置、および、真空下で圧力変動吸着を行うガス分離方法
JP6028081B1 (ja) * 2015-10-02 2016-11-16 東京瓦斯株式会社 酸素吸着剤、酸素吸着剤を用いた酸素製造装置、および、酸素製造方法
CN105692570A (zh) * 2016-03-11 2016-06-22 北京市飞达捷能气体分离技术有限公司 一种可替代膜分离制氮的变压吸附制氮装置
EP3528941B1 (en) 2016-10-21 2025-11-26 Corning Incorporated Sorbent structures with resistive heating capability and methods of making the same
US10315152B2 (en) 2017-06-08 2019-06-11 DK Engineering Consulting LLC Method and system for pressure swing adsorption
CN109289515B (zh) * 2018-11-29 2024-01-19 国电环境保护研究院有限公司 一种再生塔停机防腐蚀系统和停机操作方法
CN113731103A (zh) * 2021-09-07 2021-12-03 福建师范大学 一种挥发性有机物高效节能处理装备
CN116550087B (zh) * 2023-04-23 2026-02-27 中国科学院合肥物质科学研究院 一种内置式氦气杂质吸附装置及吸附方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2661808A (en) * 1949-10-14 1953-12-08 Linde Eismasch Ag Process for the purification and separation of gas mixtures
JPS5561915A (en) * 1978-11-06 1980-05-10 Hitachi Ltd Pressure swing type adsorption tower
US4398927A (en) * 1980-07-30 1983-08-16 Exxon Research And Engineering Co. Cyclic adsorption process
JPH08257340A (ja) * 1995-03-07 1996-10-08 Praxair Technol Inc 圧力スイング式吸着法における熱回収
US5989314A (en) * 1995-09-26 1999-11-23 Praxair Technology, Inc. Pressure swing adsorption air prepurifier
JPH10263352A (ja) * 1997-03-21 1998-10-06 Mitsui Eng & Shipbuild Co Ltd 圧力変動用吸着塔および吸着分離装置ならびに圧力変動吸着分離方法
JPH10263351A (ja) * 1997-03-28 1998-10-06 Mitsubishi Heavy Ind Ltd ガス分離装置
DE102004063613A1 (de) * 2004-12-27 2006-07-06 Elementar Analysensysteme Gmbh Verfahren und Vorrichtung zur Elementaranalyse und/oder zum präparativen Trennen von mindestens zwei Gasen im Trägergas eines Hauptgasstroms
JP4721967B2 (ja) * 2006-07-06 2011-07-13 吸着技術工業株式会社 高温酸素吸着剤を利用した圧力スイング法による酸素製造方法及び装置
JP5298291B2 (ja) * 2008-07-01 2013-09-25 吸着技術工業株式会社 酸素選択型吸着剤を利用した圧力スイング吸着法による酸素製造方法及び装置

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JP2014000531A (ja) 2014-01-09
EP2862618A4 (en) 2015-09-30
EP2862618B1 (en) 2016-11-16
US9216374B2 (en) 2015-12-22
IN2014DN10865A (enExample) 2015-09-11
US20150151239A1 (en) 2015-06-04
EP2862618A1 (en) 2015-04-22
WO2013191097A1 (ja) 2013-12-27

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