JP5597203B2 - 浄化フローストリームの採取システム - Google Patents
浄化フローストリームの採取システム Download PDFInfo
- Publication number
- JP5597203B2 JP5597203B2 JP2011536318A JP2011536318A JP5597203B2 JP 5597203 B2 JP5597203 B2 JP 5597203B2 JP 2011536318 A JP2011536318 A JP 2011536318A JP 2011536318 A JP2011536318 A JP 2011536318A JP 5597203 B2 JP5597203 B2 JP 5597203B2
- Authority
- JP
- Japan
- Prior art keywords
- gas
- flow stream
- liquid separator
- pressure
- collection system
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000746 purification Methods 0.000 title description 2
- 239000007788 liquid Substances 0.000 claims description 55
- 239000002904 solvent Substances 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 11
- 238000004808 supercritical fluid chromatography Methods 0.000 claims description 8
- 230000008569 process Effects 0.000 claims description 7
- 238000004587 chromatography analysis Methods 0.000 claims description 6
- 239000012530 fluid Substances 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000003306 harvesting Methods 0.000 claims 2
- 239000007789 gas Substances 0.000 description 31
- 239000012071 phase Substances 0.000 description 11
- 239000007791 liquid phase Substances 0.000 description 9
- 238000012387 aerosolization Methods 0.000 description 5
- 239000006184 cosolvent Substances 0.000 description 4
- 238000005070 sampling Methods 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 239000000443 aerosol Substances 0.000 description 3
- 238000012864 cross contamination Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 230000001629 suppression Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 2
- 238000004128 high performance liquid chromatography Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 239000012156 elution solvent Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000004366 reverse phase liquid chromatography Methods 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000000194 supercritical-fluid extraction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/80—Fraction collectors
- G01N30/82—Automatic means therefor
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/32—Control of physical parameters of the fluid carrier of pressure or speed
- G01N2030/324—Control of physical parameters of the fluid carrier of pressure or speed speed, flow rate
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US19902608P | 2008-11-12 | 2008-11-12 | |
| US61/199,026 | 2008-11-12 | ||
| PCT/US2009/006059 WO2010056313A1 (en) | 2008-11-12 | 2009-11-12 | Collection system for purification flowstreams |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012508882A JP2012508882A (ja) | 2012-04-12 |
| JP2012508882A5 JP2012508882A5 (enExample) | 2012-12-27 |
| JP5597203B2 true JP5597203B2 (ja) | 2014-10-01 |
Family
ID=41591639
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011536318A Expired - Fee Related JP5597203B2 (ja) | 2008-11-12 | 2009-11-12 | 浄化フローストリームの採取システム |
Country Status (5)
| Country | Link |
|---|---|
| US (2) | US9205350B2 (enExample) |
| EP (1) | EP2344873B1 (enExample) |
| JP (1) | JP5597203B2 (enExample) |
| CN (1) | CN102216769B (enExample) |
| WO (1) | WO2010056313A1 (enExample) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103619433B (zh) * | 2011-06-17 | 2016-10-19 | 沃特世科技公司 | 用于超临界流体色谱的开床式常压收集的方法与装置 |
| EP3250325A4 (en) | 2015-01-30 | 2018-09-12 | Agilent Technologies, Inc. | Impact centrifugal separator and associated methods for fraction collection in supercritical fluid systems |
| CN107615063B (zh) * | 2015-04-10 | 2021-04-20 | 沃特世科技公司 | 气液分离后二氧化碳基色谱系统的冷却液体洗脱液 |
| WO2017143158A1 (en) * | 2016-02-18 | 2017-08-24 | Waters Technologies Corporation | Method of using chemical tags to improve the identification, quantification and spatial localization of components in a sample |
| CN109564200B (zh) * | 2016-08-15 | 2022-07-08 | 安捷伦科技有限公司 | 用于收集色谱级分的气液分离器 |
| US11015142B1 (en) * | 2016-10-20 | 2021-05-25 | Unified Science, LLC | Extraction system and methods for preparing a botanical oil |
| US10717024B2 (en) * | 2016-10-25 | 2020-07-21 | Waters Technologies Corporation | Gas liquid separator and associated systems and methods |
| DE102017130820A1 (de) * | 2017-05-16 | 2018-11-22 | Alexander Bozic | Gas-Flüssig-Abscheider für eine Chromatographie-Anlage |
| CN109357976A (zh) * | 2018-10-25 | 2019-02-19 | 中国海洋石油集团有限公司 | 一种多相流自动采集计量系统 |
| JP7063249B2 (ja) * | 2018-11-22 | 2022-05-09 | 株式会社島津製作所 | 分析支援方法、分析支援装置、分析支援プログラムおよび分析システム |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1255395A (en) * | 1916-05-05 | 1918-02-05 | Arthur E Duram | Liquid-separator and the like. |
| US1416632A (en) * | 1921-12-27 | 1922-05-16 | Fothergill Harry | Apparatus for removing gases from liquids |
| US1823301A (en) * | 1928-03-19 | 1931-09-15 | Guy O Marchant | Method of and means for separating and flowing oil and gas |
| US2336430A (en) * | 1941-02-15 | 1943-12-07 | Western Electric Co | Separating apparatus |
| US2884366A (en) * | 1958-03-21 | 1959-04-28 | Foxboro Co | Bubble trap for liquid systems |
| US3003580A (en) * | 1958-10-13 | 1961-10-10 | Phillips Petroleum Co | Separation of reaction products of hydrogenation of crude oil |
| USRE30836E (en) * | 1972-11-10 | 1981-12-29 | Kobe, Inc. | Liquid-gas separator unit |
| FR2527934A1 (fr) * | 1982-06-03 | 1983-12-09 | Elf Aquitaine | Procede de fractionnement de melanges par chromatographie d'elution avec fluide en etat supercritique et installation pour sa mise en oeuvre |
| FR2584618B1 (fr) * | 1985-07-09 | 1989-11-24 | Elf Aquitaine | Dispositif pour la mise en oeuvre de procedes d'extraction-separation-fractionnement par fluides supercritiques |
| US4681606A (en) * | 1986-02-26 | 1987-07-21 | Cobe Laboratories, Inc. | Drip chamber |
| JP2563133B2 (ja) * | 1989-01-20 | 1996-12-11 | 日本電子株式会社 | 超臨界流体クロマトグラフィー装置 |
| JP2839276B2 (ja) * | 1989-01-23 | 1998-12-16 | 日本分光工業株式会社 | 超臨界流体抽出・分離方法及び装置 |
| JPH04134402U (ja) * | 1991-05-31 | 1992-12-15 | 三菱重工業株式会社 | トラツプ |
| JP3437737B2 (ja) * | 1997-04-10 | 2003-08-18 | オルガノ株式会社 | 超臨界水反応装置 |
| US6685828B2 (en) * | 1999-09-16 | 2004-02-03 | Berger Instruments, Inc. | Automated sample collection in supercritical fluid chromatography |
| US6413428B1 (en) * | 1999-09-16 | 2002-07-02 | Berger Instruments, Inc. | Apparatus and method for preparative supercritical fluid chromatography |
| US6632353B2 (en) | 2000-06-26 | 2003-10-14 | Berger Instruments, Inc. | Rapid sample collection in supercritical fluid chromatography |
| CN2623314Y (zh) * | 2003-02-18 | 2004-07-07 | 张荣华 | 超临界流体气液相分离装置 |
| JP4365170B2 (ja) * | 2003-08-29 | 2009-11-18 | ヤンマー株式会社 | 超臨界流体又は亜臨界流体による有機物質の反応装置における被処理材供給方法 |
| JP4319551B2 (ja) * | 2004-01-05 | 2009-08-26 | ダイセル化学工業株式会社 | 超臨界流体クロマトグラフィーによる物質の分離方法及びこれに用いられる気液分離装置 |
| US7131292B2 (en) * | 2004-02-18 | 2006-11-07 | Denso Corporation | Gas-liquid separator |
| JP2006136838A (ja) | 2004-11-15 | 2006-06-01 | Jasco Corp | 捕集物採取用ノズル |
| CN100348290C (zh) * | 2005-03-28 | 2007-11-14 | 浙江大学 | 四分区的超临界流体模拟移动床色谱装置 |
| FR2889665B1 (fr) * | 2005-08-12 | 2007-11-09 | Pic Solution Soc Par Actions S | Procede et installation pour la regulation du taux de modificateur dans une chromatographie ou extraction supercritique avec recyclage |
| JP2007120972A (ja) * | 2005-10-25 | 2007-05-17 | Jasco Corp | 超臨界システム |
| EP1779911A1 (en) * | 2005-10-28 | 2007-05-02 | M-I Epcon As | A separator tank |
| US7964029B2 (en) * | 2006-07-17 | 2011-06-21 | Thar Instrument, Inc. | Process flowstream collection system |
| JP2008093572A (ja) * | 2006-10-12 | 2008-04-24 | Toshiba Corp | 高圧流体抜出しシステムおよび高圧流体抜出し装置 |
| WO2008066861A1 (en) * | 2006-11-30 | 2008-06-05 | Westlake Longview Corporation | High-pressure separator |
-
2009
- 2009-11-12 WO PCT/US2009/006059 patent/WO2010056313A1/en not_active Ceased
- 2009-11-12 JP JP2011536318A patent/JP5597203B2/ja not_active Expired - Fee Related
- 2009-11-12 CN CN200980145138.8A patent/CN102216769B/zh active Active
- 2009-11-12 US US13/063,571 patent/US9205350B2/en active Active
- 2009-11-12 EP EP09756585.7A patent/EP2344873B1/en active Active
-
2013
- 2013-11-20 US US14/085,387 patent/US9205351B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN102216769B (zh) | 2014-10-29 |
| JP2012508882A (ja) | 2012-04-12 |
| US20140190890A1 (en) | 2014-07-10 |
| US9205350B2 (en) | 2015-12-08 |
| CN102216769A (zh) | 2011-10-12 |
| EP2344873B1 (en) | 2018-05-30 |
| US9205351B2 (en) | 2015-12-08 |
| US20130186831A1 (en) | 2013-07-25 |
| WO2010056313A1 (en) | 2010-05-20 |
| EP2344873A1 (en) | 2011-07-20 |
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