JP5561984B2 - 新規飲料 - Google Patents
新規飲料 Download PDFInfo
- Publication number
- JP5561984B2 JP5561984B2 JP2009225452A JP2009225452A JP5561984B2 JP 5561984 B2 JP5561984 B2 JP 5561984B2 JP 2009225452 A JP2009225452 A JP 2009225452A JP 2009225452 A JP2009225452 A JP 2009225452A JP 5561984 B2 JP5561984 B2 JP 5561984B2
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- JP
- Japan
- Prior art keywords
- asperoside
- beverage
- tochu
- present
- asperroside
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 235000013361 beverage Nutrition 0.000 title claims description 45
- CCAIKWKFTGBEJQ-UHFFFAOYSA-N asperoside Natural products CC(CCC1(O)OC2C(CC3(C)CCC4C(CC=C5CC(CCC45C)OC6OC(CO)C(OC7OC(C)C(OC8OC(C)C(O)C(O)C8O)C(O)C7O)C(O)C6OC9OC(C)C(O)C(O)C9O)C23)C1C)COC%10OC(CO)C(O)C(O)C%10O CCAIKWKFTGBEJQ-UHFFFAOYSA-N 0.000 claims description 56
- YHKROSUJLZTZDS-IOLWVCCESA-N dichotomin Chemical compound O([C@H]1[C@H](C)O[C@H]([C@@H]([C@@H]1O)O)O[C@@H]1[C@@H](CO)O[C@H]([C@@H]([C@H]1O)O[C@H]1[C@@H]([C@H](O)[C@@H](O)[C@H](C)O1)O)OC1CC2=CCC3C4CC5O[C@]([C@H](C5C4(C)CCC3C2(C)CC1)C)(O)CCC(C)CO[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@@H](C)[C@H](O)[C@@H](O)[C@H]1O YHKROSUJLZTZDS-IOLWVCCESA-N 0.000 claims description 56
- 239000002253 acid Substances 0.000 claims description 42
- IBFYXTRXDNAPMM-BVTMAQQCSA-N Geniposide Chemical compound O([C@@H]1OC=C([C@@H]2[C@H]1C(=CC2)CO)C(=O)OC)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O IBFYXTRXDNAPMM-BVTMAQQCSA-N 0.000 claims description 41
- IBFYXTRXDNAPMM-FZEIBHLUSA-N Geniposide Natural products COC(=O)C1=CO[C@@H](O[C@H]2O[C@@H](CO)[C@H](O)[C@@H](O)[C@@H]2O)[C@H]2[C@@H]1CC=C2CO IBFYXTRXDNAPMM-FZEIBHLUSA-N 0.000 claims description 41
- VGLLGNISLBPZNL-RBUKDIBWSA-N arborescoside Natural products O=C(OC)C=1[C@@H]2C([C@H](O[C@H]3[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O3)OC=1)=C(CO)CC2 VGLLGNISLBPZNL-RBUKDIBWSA-N 0.000 claims description 41
- 241001122767 Theaceae Species 0.000 claims description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 229940092665 tea leaf extract Drugs 0.000 claims description 19
- 239000000284 extract Substances 0.000 claims description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 18
- 239000000203 mixture Substances 0.000 description 18
- 238000011156 evaluation Methods 0.000 description 17
- 238000000034 method Methods 0.000 description 13
- 229920003266 Leaf® Polymers 0.000 description 10
- 235000019640 taste Nutrition 0.000 description 10
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- 238000004128 high performance liquid chromatography Methods 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 8
- 239000000047 product Substances 0.000 description 8
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- 208000008589 Obesity Diseases 0.000 description 6
- 239000003463 adsorbent Substances 0.000 description 6
- IBIPGYWNOBGEMH-DILZHRMZSA-N asperuloside Chemical compound O([C@@H]1OC=C2C(=O)O[C@H]3C=C([C@@H]1[C@H]32)COC(=O)C)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O IBIPGYWNOBGEMH-DILZHRMZSA-N 0.000 description 6
- COUXBBBIXWWAEP-AGUBZPQCSA-N asperuloside Natural products CC(=O)OCC1=C[C@@H]2OC(=O)C3=CO[C@@H](OC[C@H]4O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]4O)[C@H]1[C@H]23 COUXBBBIXWWAEP-AGUBZPQCSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 235000020824 obesity Nutrition 0.000 description 6
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- 239000002904 solvent Substances 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- 239000000706 filtrate Substances 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- 230000003579 anti-obesity Effects 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 235000019606 astringent taste Nutrition 0.000 description 3
- 235000019658 bitter taste Nutrition 0.000 description 3
- 230000002265 prevention Effects 0.000 description 3
- 238000010025 steaming Methods 0.000 description 3
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- 101100313763 Arabidopsis thaliana TIM22-2 gene Proteins 0.000 description 2
- 206010003210 Arteriosclerosis Diseases 0.000 description 2
- 208000031226 Hyperlipidaemia Diseases 0.000 description 2
- 206010020772 Hypertension Diseases 0.000 description 2
- 208000001145 Metabolic Syndrome Diseases 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 239000004793 Polystyrene Substances 0.000 description 2
- 201000000690 abdominal obesity-metabolic syndrome Diseases 0.000 description 2
- 208000011775 arteriosclerosis disease Diseases 0.000 description 2
- 238000004587 chromatography analysis Methods 0.000 description 2
- 206010012601 diabetes mellitus Diseases 0.000 description 2
- 238000007865 diluting Methods 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- -1 fluidizers Substances 0.000 description 2
- 229930014626 natural product Natural products 0.000 description 2
- 229920002223 polystyrene Polymers 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 201000002859 sleep apnea Diseases 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000006228 supernatant Substances 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 244000302899 Cassia mimosoides Species 0.000 description 1
- 235000014112 Cassia mimosoides Nutrition 0.000 description 1
- 240000004670 Glycyrrhiza echinata Species 0.000 description 1
- 235000001453 Glycyrrhiza echinata Nutrition 0.000 description 1
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 description 1
- 235000017382 Glycyrrhiza lepidota Nutrition 0.000 description 1
- ZUKLFFYDSALIQW-MSUKCBDUSA-N Iridoid glycoside Chemical compound [H][C@]12CC[C@H](C(O)=O)[C@@]1([H])[C@H](OC1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O)OC=C2 ZUKLFFYDSALIQW-MSUKCBDUSA-N 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 244000082204 Phyllostachys viridis Species 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000006286 aqueous extract Substances 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 230000037237 body shape Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000011088 calibration curve Methods 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000004440 column chromatography Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000007884 disintegrant Substances 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- MYRTYDVEIRVNKP-UHFFFAOYSA-N divinylbenzene Substances C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 1
- 235000006694 eating habits Nutrition 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 230000002068 genetic effect Effects 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 210000001596 intra-abdominal fat Anatomy 0.000 description 1
- 238000004255 ion exchange chromatography Methods 0.000 description 1
- 229930182489 iridoid glycoside Natural products 0.000 description 1
- 229940010454 licorice Drugs 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
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- 238000004810 partition chromatography Methods 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 239000000546 pharmaceutical excipient Substances 0.000 description 1
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- 238000000746 purification Methods 0.000 description 1
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- 235000009566 rice Nutrition 0.000 description 1
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- 239000013589 supplement Substances 0.000 description 1
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- 208000024891 symptom Diseases 0.000 description 1
- 239000003826 tablet Substances 0.000 description 1
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Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Non-Alcoholic Beverages (AREA)
- Medicines Containing Plant Substances (AREA)
Description
本発明の飲料および組成物は、杜仲茶葉由来のゲニポシド酸を成分として含有するが、その他の添加物由来のゲニポシド酸を含んでもよい。本発明におけるアスペルロシドおよびゲニポシド酸の重量比は、杜仲茶葉由来のゲニポシド酸に基づいて算出される。
[アスペルロシドの調製]
以下に示す手法により、アスペルロシドを杜仲葉より抽出・精製した。原料として使用した杜仲葉粉末は、特開2005−287469号公報の実施例5の記載に基づいて製造した。
[HPLC測定条件]
HPLC装置:LC−6(島津製作所);
カラム:YMC−Pack ODS A−312、φ6.0mm×150mm(YMC製);
移動相:水/メタノール/リン酸=870/130/1;
カラム温度:40℃;
検出器:UV検出器(測定波長:215nm);
流速:1mL/分。
[杜仲茶葉抽出物の製造]
杜仲葉抽出物の製造は、特開2005−289950号公報の実施例1の記載に基づいて行った。杜仲生葉(5kg)を、日本茶製造用の送帯蒸機により110℃で90秒間蒸熱した。生葉を送帯蒸し機の投入口から機内に投入し、コンベヤ上を移動する間に上下スチーム供給装置からスチームを当て、110℃で90秒間蒸熱した。ネットコンベア上に杜仲生葉を広げ、ボイラーから供給される無圧蒸気を充満させた処理室を通過させることにより、杜仲生葉を蒸熱処理した。宮村鉄工株式会社製、給葉機、地上型1500及びネットコンベア、送帯式1000を用いた。
[官能評価試験]
上記のアスペルロシドおよび杜仲茶葉抽出物を使用して、アスペルロシド濃度が50mg/L、80mg/L、200mg/Lおよび500mg/Lであり、アスペルロシドおよびゲニポシド酸の重量比が表1〜表4に示したとおりである試料を調製した。
5点:異味を感じない。
4点:異味をやや感じる。
3点:異味を感じる。
2点:異味を強く感じる。
1点:異味を非常に強く感じる。
Claims (4)
- 杜仲茶葉抽出物およびアスペルロシドを含む飲料であって、飲料中に含まれるアスペルロシドの濃度が30〜1000mg/Lであり、飲料中に含まれるアスペルロシドおよび杜仲茶葉由来のゲニポシド酸の重量比(アスペルロシド/ゲニポシド酸)が0.2〜100である前記飲料。
- アスペルロシドの濃度が50〜500mg/Lである、請求項1に記載の飲料。
- 飲料中に含まれるアスペルロシドおよび杜仲茶葉由来のゲニポシド酸の重量比(アスペルロシド/ゲニポシド酸)が1〜20である、請求項1または2に記載の飲料。
- 杜仲茶葉抽出物が杜仲茶葉の水抽出物である、請求項1〜3のいずれか1項に記載の飲料。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2009225452A JP5561984B2 (ja) | 2009-09-29 | 2009-09-29 | 新規飲料 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2009225452A JP5561984B2 (ja) | 2009-09-29 | 2009-09-29 | 新規飲料 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2011072227A JP2011072227A (ja) | 2011-04-14 |
JP5561984B2 true JP5561984B2 (ja) | 2014-07-30 |
Family
ID=44016916
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2009225452A Active JP5561984B2 (ja) | 2009-09-29 | 2009-09-29 | 新規飲料 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JP5561984B2 (ja) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107668453A (zh) * | 2017-09-28 | 2018-02-09 | 郑州轻工业学院 | 一种杜仲雄花发酵型饮料制备的方法 |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102204601B (zh) * | 2011-05-18 | 2012-09-26 | 徐杏昌 | 一种降血糖保健茶及其制备方法 |
JP6789613B2 (ja) * | 2015-02-25 | 2020-11-25 | 小林製薬株式会社 | 経口組成物 |
CN106668050A (zh) * | 2017-01-22 | 2017-05-17 | 新乡医学院 | 治疗动脉粥样硬化的药物组合物及应用 |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5088846B2 (ja) * | 2006-03-03 | 2012-12-05 | 小林製薬株式会社 | 杜仲葉水抽出物の分画物、および当該分画物を含む抗肥満剤 |
JP2007238456A (ja) * | 2006-03-03 | 2007-09-20 | Kobayashi Pharmaceut Co Ltd | 杜仲葉水抽出物の分画物、およびそれを含む経口摂取用組成物 |
JP5394644B2 (ja) * | 2008-03-04 | 2014-01-22 | 小林製薬株式会社 | アスペルロシドまたはその類縁体を含む筋肉増強剤 |
JP5014320B2 (ja) * | 2008-12-10 | 2012-08-29 | 有限会社 碧山園 | 杜仲葉緑色乾燥粉末 |
-
2009
- 2009-09-29 JP JP2009225452A patent/JP5561984B2/ja active Active
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107668453A (zh) * | 2017-09-28 | 2018-02-09 | 郑州轻工业学院 | 一种杜仲雄花发酵型饮料制备的方法 |
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