JP5521036B2 - Cu−In−Ga−Se合金粉末の製造方法、Cu−In−Ga−Se合金焼結体の製造方法及びCu−In−Ga−Se合金粉末 - Google Patents
Cu−In−Ga−Se合金粉末の製造方法、Cu−In−Ga−Se合金焼結体の製造方法及びCu−In−Ga−Se合金粉末Info
- Publication number
- JP5521036B2 JP5521036B2 JP2012517125A JP2012517125A JP5521036B2 JP 5521036 B2 JP5521036 B2 JP 5521036B2 JP 2012517125 A JP2012517125 A JP 2012517125A JP 2012517125 A JP2012517125 A JP 2012517125A JP 5521036 B2 JP5521036 B2 JP 5521036B2
- Authority
- JP
- Japan
- Prior art keywords
- alloy
- powder
- mixed
- region
- alloy powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000843 powder Substances 0.000 title claims description 74
- 229910001370 Se alloy Inorganic materials 0.000 title claims description 68
- 238000004519 manufacturing process Methods 0.000 title claims description 28
- 229910000807 Ga alloy Inorganic materials 0.000 claims description 115
- 238000000034 method Methods 0.000 claims description 30
- 238000010304 firing Methods 0.000 claims description 28
- 239000011812 mixed powder Substances 0.000 claims description 27
- 239000002184 metal Substances 0.000 claims description 16
- 229910052751 metal Inorganic materials 0.000 claims description 16
- 239000002245 particle Substances 0.000 claims description 15
- 238000005245 sintering Methods 0.000 claims description 7
- 239000011669 selenium Substances 0.000 description 74
- 238000006243 chemical reaction Methods 0.000 description 32
- 229910052738 indium Inorganic materials 0.000 description 32
- 229910052711 selenium Inorganic materials 0.000 description 32
- 239000010949 copper Substances 0.000 description 20
- 229910052802 copper Inorganic materials 0.000 description 13
- 239000002360 explosive Substances 0.000 description 11
- 238000005266 casting Methods 0.000 description 9
- 238000005275 alloying Methods 0.000 description 8
- 238000004455 differential thermal analysis Methods 0.000 description 8
- 229910052733 gallium Inorganic materials 0.000 description 8
- 239000010410 layer Substances 0.000 description 7
- 238000001878 scanning electron micrograph Methods 0.000 description 7
- 229910001128 Sn alloy Inorganic materials 0.000 description 6
- 239000010408 film Substances 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 238000002149 energy-dispersive X-ray emission spectroscopy Methods 0.000 description 4
- 230000020169 heat generation Effects 0.000 description 4
- 238000005477 sputtering target Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 3
- 238000010298 pulverizing process Methods 0.000 description 3
- 238000004544 sputter deposition Methods 0.000 description 3
- 238000002411 thermogravimetry Methods 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000002238 attenuated effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000003292 diminished effect Effects 0.000 description 1
- 238000010894 electron beam technology Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 238000004451 qualitative analysis Methods 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 238000002490 spark plasma sintering Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C9/00—Alloys based on copper
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/04—Making non-ferrous alloys by powder metallurgy
- C22C1/0425—Copper-based alloys
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C28/00—Alloys based on a metal not provided for in groups C22C5/00 - C22C27/00
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
- C23C14/3407—Cathode assembly for sputtering apparatus, e.g. Target
- C23C14/3414—Metallurgical or chemical aspects of target preparation, e.g. casting, powder metallurgy
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
- B22F2998/10—Processes characterised by the sequence of their steps
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Powder Metallurgy (AREA)
- Physical Vapour Deposition (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2012517125A JP5521036B2 (ja) | 2010-05-24 | 2011-05-20 | Cu−In−Ga−Se合金粉末の製造方法、Cu−In−Ga−Se合金焼結体の製造方法及びCu−In−Ga−Se合金粉末 |
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2010118679 | 2010-05-24 | ||
JP2010118679 | 2010-05-24 | ||
PCT/JP2011/002813 WO2011148600A1 (fr) | 2010-05-24 | 2011-05-20 | Procédé pour la production d'une poudre d'alliage de cu-in-ga, procédé pour la production d'une poudre d'alliage de cu-in-ga-se, procédé pour la production d'un alliage de cu-in-ga-se fritté, poudre d'alliage de cu-in-ga, et poudre d'alliage de cu-in-ga-se |
JP2012517125A JP5521036B2 (ja) | 2010-05-24 | 2011-05-20 | Cu−In−Ga−Se合金粉末の製造方法、Cu−In−Ga−Se合金焼結体の製造方法及びCu−In−Ga−Se合金粉末 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPWO2011148600A1 JPWO2011148600A1 (ja) | 2013-07-25 |
JP5521036B2 true JP5521036B2 (ja) | 2014-06-11 |
Family
ID=45003600
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2012517125A Expired - Fee Related JP5521036B2 (ja) | 2010-05-24 | 2011-05-20 | Cu−In−Ga−Se合金粉末の製造方法、Cu−In−Ga−Se合金焼結体の製造方法及びCu−In−Ga−Se合金粉末 |
Country Status (3)
Country | Link |
---|---|
JP (1) | JP5521036B2 (fr) |
TW (1) | TW201200270A (fr) |
WO (1) | WO2011148600A1 (fr) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5588757B2 (ja) * | 2010-06-21 | 2014-09-10 | 株式会社アルバック | In−Se合金粉末、In−Se合金焼結体、Ga−Se合金粉末、Ga−Se合金焼結体、In−Ga−Se合金粉末、In−Ga−Se合金焼結体、Cu−In−Ga−Se合金粉末及びCu−In−Ga−Se合金焼結体の製造方法 |
JP5767447B2 (ja) * | 2010-06-29 | 2015-08-19 | 株式会社コベルコ科研 | Cu、In、GaおよびSeの元素を含有する粉末の製造方法、及びCu、In、GaおよびSeの元素を含有するスパッタリングターゲット |
JP5533607B2 (ja) * | 2010-11-30 | 2014-06-25 | 三菱マテリアル株式会社 | スパッタリングターゲット及びその製造方法 |
WO2013089630A1 (fr) * | 2011-12-15 | 2013-06-20 | Midsummer Ab | Recyclage de diséléniure de cuivre, d'indium et de gallium |
WO2013129044A1 (fr) * | 2012-02-27 | 2013-09-06 | 株式会社日本マイクロニクス | Procédé de fabrication d'alliage pour cellule solaire à base de cigs |
JP5993945B2 (ja) * | 2012-05-15 | 2016-09-21 | 株式会社日本マイクロニクス | n型光吸収層用合金とその製造方法及び太陽電池 |
WO2013172252A1 (fr) * | 2012-05-15 | 2013-11-21 | 株式会社 日本マイクロニクス | ALLIAGE POUR UNE COUCHE ABSORBANT LA LUMIÈRE AJOUTÉE AU SODIUM (Na), PROCÉDÉ PERMETTANT DE PRODUIRE CE DERNIER ET CELLULE SOLAIRE |
JP2013253308A (ja) * | 2012-06-08 | 2013-12-19 | Futek Furnace Inc | Cigsスパッタリングターゲットの製造方法 |
KR101483254B1 (ko) | 2013-07-15 | 2015-01-15 | 한국생산기술연구원 | 스퍼터링 타겟용 4성분계 셀렌화합물 소결체 및 그 제조방법 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2009120862A (ja) * | 2007-11-12 | 2009-06-04 | Mitsubishi Materials Corp | Cu−In−Ga三元系焼結合金スパッタリングターゲットおよびその製造方法 |
JP2009287092A (ja) * | 2008-05-30 | 2009-12-10 | Mitsubishi Materials Corp | カルコパイライト型半導体膜成膜用スパッタリングターゲットの製造方法 |
-
2011
- 2011-05-20 WO PCT/JP2011/002813 patent/WO2011148600A1/fr active Application Filing
- 2011-05-20 JP JP2012517125A patent/JP5521036B2/ja not_active Expired - Fee Related
- 2011-05-23 TW TW100117936A patent/TW201200270A/zh unknown
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2009120862A (ja) * | 2007-11-12 | 2009-06-04 | Mitsubishi Materials Corp | Cu−In−Ga三元系焼結合金スパッタリングターゲットおよびその製造方法 |
JP2009287092A (ja) * | 2008-05-30 | 2009-12-10 | Mitsubishi Materials Corp | カルコパイライト型半導体膜成膜用スパッタリングターゲットの製造方法 |
Also Published As
Publication number | Publication date |
---|---|
TW201200270A (en) | 2012-01-01 |
JPWO2011148600A1 (ja) | 2013-07-25 |
WO2011148600A1 (fr) | 2011-12-01 |
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