JP5199612B2 - Two-part cosmetic - Google Patents
Two-part cosmetic Download PDFInfo
- Publication number
- JP5199612B2 JP5199612B2 JP2007174987A JP2007174987A JP5199612B2 JP 5199612 B2 JP5199612 B2 JP 5199612B2 JP 2007174987 A JP2007174987 A JP 2007174987A JP 2007174987 A JP2007174987 A JP 2007174987A JP 5199612 B2 JP5199612 B2 JP 5199612B2
- Authority
- JP
- Japan
- Prior art keywords
- agent
- oil
- weight
- acid
- skin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
- QUEDXNHFTDJVIY-UHFFFAOYSA-N γ-tocopherol Chemical class OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-UHFFFAOYSA-N 0.000 description 1
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Description
本発明は、エステティックのマッサージの施術において、エステ効果が得られる2剤式化粧料に関する。 The present invention relates to a two-part cosmetic that provides an esthetic effect in an esthetic massage treatment.
エステティックにおいてマッサージは血行を促進させることにより皮膚の新陳代謝を向上させる重要な施術の一つである。しかし、施術者の熟練度によって付与される効果が大きく異なるという課題があった。これに対してマッサージで得られる効果を増大させる目的で施術時に使用するマッサージ用の化粧料が開発されてきた。そのようなマッサージ用の化粧料は皮膚の温度を高め、血流をよくすることが重要である。従来、皮膚温度を高める技術の多くは特定の無機物や有機化合物の溶解熱や水和熱を利用したものである。例えば無機物の場合では一〜三価金属イオンの硫酸塩、炭酸塩、塩化物、酸化物及びリン酸塩の他ゼオライト等を配合し、溶解熱を利用している。また、有機化合物の場合はポリエチレングリコール、グリセリン、1,3−ブチレングリコール等の多価アルコールやアルキルグリセリド等を配合し、水和熱を利用している。さらに、これらの発熱量をより増大させるために無機物と有機化合物の併用し、皮膚中の水との発熱反応により皮膚へ温感を付与する技術や(特許文献1)、無機塩・無機酸化物と油分を含む1剤と多価アルコールを含む2剤を使用時に混合する2剤式化粧料とすることで、発熱性を向上させる技術が開示されている(特許文献2)。 In aesthetics, massage is one of the important treatments to improve skin metabolism by promoting blood circulation. However, there is a problem that the effect imparted greatly depends on the skill level of the practitioner. On the other hand, massage cosmetics used during treatment have been developed for the purpose of increasing the effect obtained by massage. It is important for such massage cosmetics to increase skin temperature and improve blood flow. Conventionally, many techniques for increasing the skin temperature utilize the heat of dissolution and heat of hydration of specific inorganic substances and organic compounds. For example, in the case of inorganic substances, sulfates, carbonates, chlorides, oxides and phosphates of mono- to trivalent metal ions are blended with zeolite and the like, and the heat of dissolution is used. In the case of organic compounds, polyhydric alcohols such as polyethylene glycol, glycerin and 1,3-butylene glycol, alkyl glycerides and the like are blended and the heat of hydration is utilized. Furthermore, in order to further increase these calorific values, a technique of combining an inorganic substance and an organic compound and imparting a warm feeling to the skin by an exothermic reaction with water in the skin (Patent Document 1), an inorganic salt / inorganic oxide The technology which improves exothermic property is made by making it the 2 agent type cosmetics which mix 1 agent containing oil, and 2 agents containing a polyhydric alcohol at the time of use (patent document 2).
しかし、これらの化粧料においては、1剤式か2剤式かにかかわらず、皮膚中の水により発熱させるため、皮膚の水分が十分でない場合、皮膚温度の向上が望めず、エステ効果が不十分だった。また、皮膚の表面が垢や皮脂、ほこりなどで汚れていると、十分な発熱が得られず、皮膚の温度の向上や血流の促進がされなかった。 However, in these cosmetics, regardless of whether they are single-agent or double-agent, heat is generated by the water in the skin. Therefore, if the skin moisture is insufficient, the skin temperature cannot be improved and the esthetic effect is not satisfactory. It was enough. Further, when the skin surface was soiled with dirt, sebum, dust, etc., sufficient heat generation was not obtained, and skin temperature was not improved and blood flow was not promoted.
皮膚の温度を高め、血流を促進し、さらに肌水分を増加させ、使用時のマッサージ効果、エステ効果に優れた化粧料の提供を課題とする。特に、無機化合物の粉体を含有せずに、使用感のよい化粧料を提供することを課題とする。 The object is to provide cosmetics that increase skin temperature, promote blood flow, increase skin moisture, and have excellent massage and esthetic effects during use. In particular, it is an object of the present invention to provide a cosmetic material having a good feeling of use without containing powder of an inorganic compound.
発明者は、スクラブ剤を含有する化粧料用組成物を第1剤に、デカグリセリン脂肪酸エステルエイコサン二酸縮合物を1〜10重量%、多価アルコールを80〜99重量%、油分を0.5〜10重量%含有し、水の含有量が5重量%以下の化粧料用組成物を第2剤としてエステテティックのマッサージに使用することにより、皮膚の温度を高め、血流量が向上し、肌の水分量が増加するとともに、身体へ塗布するにもかかわらず顔の血行が上昇し、すぐれたエステ効果を得られることを見出し、本発明を完成させた。 The inventor uses a cosmetic composition containing a scrub agent as the first agent, 1 to 10% by weight of decaglycerin fatty acid ester eicosane diacid condensate, 80 to 99% by weight of polyhydric alcohol, and 0% of oil. Using a cosmetic composition containing 5 to 10% by weight and containing 5% by weight or less of water as a second agent for esthetic massage, increases skin temperature and improves blood flow As a result, the present inventors have found that the amount of moisture in the skin increases and the blood circulation of the face increases despite being applied to the body, and an excellent esthetic effect can be obtained.
本発明によれば、スクラブ剤を含有した第1剤によるマッサージにより皮膚が清浄され、適度に水分を付与した後、デカグリセリン脂肪酸エステルエイコサン二酸縮合物、多価アルコールおよび油分の含有した第2剤でマッサージすることにより、皮膚の温度を高め、血流を改善・促進し、皮膚水分量を増加することができ、すぐれたエステ効果を得ることができる。 According to the present invention, after the skin is cleaned by massaging with the first agent containing a scrubbing agent and moderately given water, the decaglycerin fatty acid ester eicosane diacid condensate, polyhydric alcohol, and oil containing oil are contained. By massaging with two agents, skin temperature can be increased, blood flow can be improved / promoted, skin moisture can be increased, and an excellent esthetic effect can be obtained.
さらに、第1剤として、マンナンをスクラブ剤に用いた乳化組成物を用いることにより皮膚清浄力が増加し、マッサージ効果を高めることができる。また、第2剤に、カルボキシビニルポリマー、キサンタンガム、又はヒドロキシエチルセルロースを含有することにより、粘度が向上し皮膚への滞留性を高めるため、温度上昇の持続性をより高めることができる。また、多価アルコールとしてグリセリン、1,3−ブチングリコール、油分としてスクワラン、スクワレン、オリーブ油、ホホバ油、スクワラン、スクワレン、シクロメチコン、ジメチルポリシロキサンを用いることにより、皮膚水分量を上げ、エステ効果をさらに向上させることができる。 Furthermore, by using an emulsified composition using mannan as a scrub agent as the first agent, the skin cleansing power can be increased and the massage effect can be enhanced. Further, by containing carboxyvinyl polymer, xanthan gum, or hydroxyethyl cellulose in the second agent, the viscosity is improved and the staying property on the skin is increased, so that the sustainability of the temperature rise can be further increased. In addition, by using glycerin, 1,3-butyne glycol as polyhydric alcohol, and squalane, squalene, olive oil, jojoba oil, squalane, squalene, cyclomethicone, and dimethylpolysiloxane as oil components, the skin moisture content is increased and the esthetic effect is enhanced. Further improvement can be achieved.
本発明を顔以外の上半身(例えば、胸元、首、肩、背中など)に塗布すると、血行が促進されることにより、顔の皮膚温度が上昇する。したがって、ホディに使用した場合でもフェイスケア効果が期待できる。 When the present invention is applied to the upper body other than the face (for example, the chest, neck, shoulders, back, etc.), blood circulation is promoted to increase the skin temperature of the face. Therefore, even when used as a body, a face care effect can be expected.
本発明は、第1剤としてのスクラブ剤の含有した化粧料用組成物、ならびに第2剤としてのデカグリセリン脂肪酸エステルエイコサン二酸縮合物、多価アルコールおよび油分を所望量含有した化粧料用組成物からなる。 The present invention relates to a cosmetic composition containing a scrub agent as a first agent, and a cosmetic containing a desired amount of a decaglycerin fatty acid ester eicosane diacid condensate, a polyhydric alcohol and an oil as a second agent. It consists of a composition.
第1剤に用いるスクラブ剤は特に限定されないが、肌を清浄する際に適度なマッサージ効果を与えるものが望ましい。具体的には、天然系スクラブの例としては、マンナン、カンテン、アルギン酸塩、キチン、キトサン等の多糖類粒子、クルミ殻、モモ種等の核種粉砕物、落花生、ゴマ等の外皮粉末、カゼイン等のタンパク質粉末が挙げられる。また、合成高分子系スクラブの例としては、ポリエチレン、ポリプロピレン、ポリエステル、ポリスチレン、ポリウレタン、シリコンパウダー等の合成樹脂の粒子が挙げられる。これらは1種又は2種以上を組み合わせて使用することができる。中でも、第1剤中のスクラブ剤として特に好ましいものは、マンナン、カンテン、アルギン酸塩である。マンナン、カンテン、アルギン酸塩は、水分を含んだゲル状であるため、柔らかい感触を有し、皮膚の血行促進等のマッサージ効果が高い。 The scrub agent used for the first agent is not particularly limited, but it is desirable to provide an appropriate massage effect when cleaning the skin. Specifically, examples of natural scrubs include polysaccharide particles such as mannan, agar, alginate, chitin, chitosan, ground nuclides such as walnut shells and peach species, peanut powder such as peanuts and sesame seeds, and casein. Of protein powder. Examples of the synthetic polymer scrub include particles of synthetic resin such as polyethylene, polypropylene, polyester, polystyrene, polyurethane, and silicon powder. These can be used alone or in combination of two or more. Among these, mannan, agarite, and alginates are particularly preferable as the scrub agent in the first agent. Mannan, agar, and alginates are gels containing moisture, so they have a soft feel and a high massage effect such as promoting blood circulation in the skin.
特にマンナンは皮膚のマッサージ効果が高いので、より好ましい。マンナンは、コンニャク芋などから精製して得られるものであり、グルコマンナンともいう。好ましくはマンナンがゲル化したマンナンゲル化物である。マンナンは第1剤中に顆粒状に均一に配合され、使用時も溶解又は破砕することなく粒状を保ち、スクラブ効果を与えることができる。マンナンの市販品としては、プロポールISLB、ホワイトプロポールISLB(清水化学社)等が挙げられる。 In particular, mannan is more preferable because it has a high skin massage effect. Mannan is obtained by refining from konjac koji and is also called glucomannan. Preferably, it is a mannan gel product obtained by gelling mannan. Mannan is uniformly blended into the first agent in a granular form, and can maintain a granular shape without being dissolved or crushed during use, and can provide a scrub effect. Commercial products of Mannan include Propol ISLB, White Propol ISLB (Shimizu Chemical Co., Ltd.) and the like.
スクラブ剤は、第1剤中に好ましくは0.1〜10重量%、より好ましくは0.5〜5重量%、さらに好ましくは1〜3重量%配合する。0.1重量%より少ないとスクラブ力が十分でなく、10重量%を超えると使用感が悪くなる。 The scrub agent is preferably added to the first agent in an amount of 0.1 to 10% by weight, more preferably 0.5 to 5% by weight, and still more preferably 1 to 3% by weight. If it is less than 0.1% by weight, the scrubbing force is not sufficient, and if it exceeds 10% by weight, the feeling of use becomes worse.
第1剤の水の含有量は10〜50重量%が好ましく、20〜40重量%がより好ましい。第1剤中の水を適切な量にすることにより、第2剤による発熱効果を高めることができる。水の含有量が10重量%より少ないと皮膚への水分補給が少なくなり、第2剤の使用時に発熱のための水が不足し発熱性が低下する。また、水の含有量が50重量%より多いと水の量が多すぎるため第2剤の使用時の発熱性が低下する。いずれにしても皮膚温度の上昇効果が低下してしまう。 The content of water in the first agent is preferably 10 to 50% by weight, and more preferably 20 to 40% by weight. By setting the amount of water in the first agent to an appropriate amount, the heat generation effect of the second agent can be enhanced. If the water content is less than 10% by weight, water supply to the skin is reduced, and water for heat generation is insufficient when the second agent is used, resulting in a decrease in heat generation. On the other hand, if the content of water is more than 50% by weight, the amount of water is too large, and the exothermicity when using the second agent is lowered. In any case, the effect of increasing the skin temperature is reduced.
第1剤の化粧料用組成物は、清浄用組成物が好ましく、剤型としてはクレンジングおよび水分を付与する作用をもつ乳化組成物又は水性組成物(水を基材とした可溶化組成物)が好ましい。その中でも乳化組成物は、肌をクレンジングし、水分を十分に与えることにより、第2剤によるエステ効果を向上させるためにより好ましい。 The cosmetic composition for the first agent is preferably a cleaning composition, and the dosage form is an emulsified composition or an aqueous composition (solubilized composition based on water) having the effect of imparting cleansing and moisture. Is preferred. Among these, the emulsified composition is more preferable because it cleanses the skin and gives sufficient moisture to improve the esthetic effect of the second agent.
第1剤が乳化組成物の場合に用いる油分は、特に限定されないが、スクワラン、スクワレン、セレシン、オレフィンオリゴマー、流動パラフィン等の炭化水素類、オリーブ油、ホホバ油、アボカド油、アルモンド油、グレープシード油、月見草油、トウモロコシ油、ツバキ油、サザンカ油、マカデミアナッツ油、メドフォーム油、シアバター、ゴマ油、コメヌカ油、卵黄油等の油脂類、イソステアリルアルコール、オクチルドデカノール、ラノリンアルコール、フィトステロール、オレイルアルコール等の高級アルコール類、トリ2−エチルヘキサン酸グリセリル、ミリスチン酸イソプロピル、オレイン酸エチル、ステアリン酸オクチル、2−エチルヘキサン酸セチル、イソノナン酸イソノニル、パルミチン酸オクチル、ジオレイン酸エチレングリコール、トリイソステアリン酸グリセリル、乳酸セチル、アジピン酸ジイソプロピル、イソステアリン酸イソステアリル等のエステル油類、ジメチルポリシロキサン、メチルフェニルポリシロキサン、ポリエ−テル変性ポリシロキサン、アミノ変性ポリシロキサン、エポキシ変性ポリシロキサン、フッ素変性ポリシロキサン、アルコ−ル変性ポリシロキサン、アルキル変性ポリシロキサン、高分子シリコーン等のシリコーン類、ラウリン酸、ミリスチン酸、パルミチン酸、ステアリン酸、ベヘン(ベヘニン)酸、オレイン酸、12−ヒドロキシステアリン酸、ウンデシレン酸、トール酸、イソステアリン酸、リノール酸、リノレイン酸、エイコサペンタエン酸(EPA)、ドコサヘキサエン酸(DHA)等の高級脂肪酸等が挙げらる。これらから選ばれる1種又は2種以上を組み合わせて使用することができる。油分の配合量は、好ましくは30〜90重量%、より好ましくは40〜80重量%、さらに好ましくは50〜70重量%である。30重量%未満では発熱の持続性が十分に発揮せず、10重量%を超えて配合すると、製剤の安定性が悪くなる。 The oil component used when the first agent is an emulsified composition is not particularly limited, but hydrocarbons such as squalane, squalene, ceresin, olefin oligomer, liquid paraffin, olive oil, jojoba oil, avocado oil, almond oil, grape seed oil , Evening primrose oil, corn oil, camellia oil, sasanqua oil, macadamia nut oil, medfoam oil, shea butter, sesame oil, rice bran oil, egg yolk oil and other oils, isostearyl alcohol, octyldodecanol, lanolin alcohol, phytosterol, oleyl alcohol Higher alcohols such as glyceryl tri-2-ethylhexanoate, isopropyl myristate, ethyl oleate, octyl stearate, cetyl 2-ethylhexanoate, isononyl isononanoate, octyl palmitate, ethyl dioleate Ester oils such as glycol, glyceryl triisostearate, cetyl lactate, diisopropyl adipate, isostearyl isostearate, dimethylpolysiloxane, methylphenylpolysiloxane, polyether-modified polysiloxane, amino-modified polysiloxane, epoxy-modified polysiloxane, Fluorine-modified polysiloxane, alcohol-modified polysiloxane, alkyl-modified polysiloxane, silicones such as polymer silicone, lauric acid, myristic acid, palmitic acid, stearic acid, behen (behenine) acid, oleic acid, 12-hydroxystearin And higher fatty acids such as acid, undecylenic acid, toluic acid, isostearic acid, linoleic acid, linolenic acid, eicosapentaenoic acid (EPA), and docosahexaenoic acid (DHA). One or two or more selected from these can be used in combination. The amount of oil is preferably 30 to 90% by weight, more preferably 40 to 80% by weight, and still more preferably 50 to 70% by weight. If it is less than 30% by weight, the sustainability of heat generation cannot be sufficiently exhibited, and if it exceeds 10% by weight, the stability of the preparation is deteriorated.
第1剤中の油分としては、上記の中でも、トリ2−エチルヘキサン酸グリセリルとオレフィンオリゴマーのいずれか1種以上が好ましい。トリ2−エチルヘキサン酸グリセリルは極性のある液状油分であり、第1剤中のクレンジング力を高めることができる。別名をトリオクタノインという。市販品としては、T.I.O(日清オイリオ社)等が挙げられる。トリ2−エチルヘキサン酸グリセリルは第1剤中に好ましくは1〜80重量%、より好ましくは5〜50重量%、さらに好ましくは10〜30重量%配合する。1重量%より少ないとクレンジング力が十分でなく、80重量%を超えると使用感が悪くなる。 Among the above, the oil component in the first agent is preferably at least one of glyceryl tri-2-ethylhexanoate and an olefin oligomer. Glyceryl tri-2-ethylhexanoate is a polar liquid oil, and can increase the cleansing power in the first agent. Another name is trioctanoin. As a commercial item, T.I.O (Nisshin Oillio Co., Ltd.) etc. are mentioned. Glyceryl tri-2-ethylhexanoate is preferably blended in the first agent in an amount of 1 to 80% by weight, more preferably 5 to 50% by weight, and even more preferably 10 to 30% by weight. If it is less than 1% by weight, the cleansing power is not sufficient, and if it exceeds 80% by weight, the feeling of use becomes worse.
オレフィンオリゴマーは常温で液体の油分であり、第1剤のクレンジング力を高めることができる。オレフィンオリゴマーとしては、α−オレフィンオリゴマーが好ましい。また、好ましくは平均分子量500〜5000である。オレフィンオリゴマーの市販品としては、Puresyn40、Puresyn100、Puresyn150、Puresyn300、Puresyn1000(エクソンモービル社)やシンセラン4(日光ケミカルズ社)等が挙げられる。オレフィンオリゴマーは第1剤中に好ましくは1〜80重量%、より好ましくは5〜50重量%、さらに好ましくは10〜30重量%配合する。1重量%より少ないとクレンジング力が十分でなく、50重量%を超えると使用感が悪くなる。第1剤の油分にトリ2−エチルヘキサン酸グリセリルとオレフィンオリゴマーのいずれも含有する場合、好ましくは重量比で1:5〜5:1である。この重量比にすることにより、クレンジング力を高めることができる。 The olefin oligomer is an oil that is liquid at room temperature, and can increase the cleansing power of the first agent. As the olefin oligomer, an α-olefin oligomer is preferable. The average molecular weight is preferably 500 to 5,000. Examples of commercially available olefin oligomers include Puresyn 40, Puresyn 100, Puresyn 150, Puresyn 300, Puresyn 1000 (Exxon Mobil) and Synthelan 4 (Nikko Chemicals). The olefin oligomer is preferably blended in the first agent in an amount of 1 to 80% by weight, more preferably 5 to 50% by weight, and still more preferably 10 to 30% by weight. If it is less than 1% by weight, the cleansing power is not sufficient, and if it exceeds 50% by weight, the feeling of use becomes worse. When the oil component of the first agent contains both glyceryl tri-2-ethylhexanoate and an olefin oligomer, the weight ratio is preferably 1: 5 to 5: 1. By using this weight ratio, the cleansing force can be increased.
また、界面活性剤は、ポリオキシエチレンヤシ油脂肪酸グリセリン、ポリオキシエチレン硬化ヒマシ油、ポリグリセリン脂肪酸エステルなどが挙げられる。 Examples of the surfactant include polyoxyethylene coconut oil fatty acid glycerin, polyoxyethylene hydrogenated castor oil, and polyglycerin fatty acid ester.
第1剤が水性組成物の場合においては、好ましくは油分を可溶化したものである。可溶化に用いる界面活性剤は特に限定はされないが、ポリオキシエチレンヤシ油脂肪酸グリセリン、ポリオキシエチレン硬化ヒマシ油、ポリグリセリン脂肪酸エステルなどが挙げられる。また、油分は特に限定はされないが、スクワラン、スクワレン、オレフィンオリゴマー、流動パラフィン、オリーブ油、ホホバ油マカデミアナッツ油等の液状油等が挙げられる。 When the first agent is an aqueous composition, the oil is preferably solubilized. The surfactant used for solubilization is not particularly limited, and examples thereof include polyoxyethylene coconut oil fatty acid glycerin, polyoxyethylene hydrogenated castor oil, and polyglycerin fatty acid ester. The oil content is not particularly limited, and examples thereof include liquid oils such as squalane, squalene, olefin oligomer, liquid paraffin, olive oil, jojoba oil and macadamia nut oil.
本発明の第2剤に用いるデカグリセリン脂肪酸エステルエイコサン二酸縮合物は、平均重合度2以上のグリセリンの縮合物と、炭素数18〜28の直鎖状飽和脂肪酸と、炭素数20〜28の脂肪族飽和二塩基酸とのエステル化生成物である。英語名:POLYGLYCERYL−10 BEHENATE/EICOSADIOATE、別名:(ベヘン酸/エイコサン二酸)ポリグリセリル−10である。具体的に入手可能な市販品してはノムコートHK−P(日清オイリオ社製)が例示される。デカグリセリン脂肪酸エステルエイコサン二酸縮合物の配合量としては1〜10重量%が好ましく、2〜8重量%がより好ましく、3〜5重量%がさらに好ましい。1重量%未満では発熱の持続性が十分に発揮せず、10重量%を超えて配合すると、化粧料としての使用感が悪くなる。 The decaglycerin fatty acid ester eicosane diacid condensate used in the second agent of the present invention is a condensate of glycerin having an average polymerization degree of 2 or more, a linear saturated fatty acid having 18 to 28 carbon atoms, and 20 to 28 carbon atoms. The esterification product of an aliphatic saturated dibasic acid. English name: POLYGLYCERYL-10 BEHENATE / EICOSADIOATE, also known as: (behenic acid / eicosanedioic acid) polyglyceryl-10. Specific examples of commercially available products include NOMCOAT HK-P (Nisshin Oilio Co., Ltd.). The amount of decaglycerin fatty acid ester eicosane diacid condensate is preferably 1 to 10% by weight, more preferably 2 to 8% by weight, and even more preferably 3 to 5% by weight. If it is less than 1% by weight, the sustainability of heat generation is not sufficiently exhibited, and if it exceeds 10% by weight, the usability as a cosmetic becomes worse.
第2剤に用いる多価アルコールは基剤として使用するだけでなく、水と混和した時に発熱する効果を与える。多価アルコールは水との接触により発熱することが知られているが、本発明においては、デカグリセリン脂肪酸エステルエイコサン二酸縮合物および油分と併用することにより発熱性が向上する。多価アルコールの種類としては、特に限定されないが、例えばグリセリン、1,3−ブチングリコール、1,2−ペンタンジオール、ポリエチレングリコール、プロピレングリコール、ジプロピレングリコール、ポリプロピレングリコール、ヘキシレングリコール、グリセリン、ジグリセリン等が挙げられる。好ましくは、グリセリン、1,3−ブチングリコール、ポリエチレングリコール、プロピレングリコール、ジプロピレングリコールが挙げられ、さらに好ましくはグリセリン、1,3−ブチングリコールが挙げられる。これらから選ばれる1種又は2種以上を組み合わせて使用することができる。 The polyhydric alcohol used for the second agent is not only used as a base, but also has an effect of generating heat when mixed with water. Polyhydric alcohols are known to generate heat upon contact with water, but in the present invention, exothermic properties are improved by the combined use with decaglycerin fatty acid ester eicosane diacid condensate and oil. The type of polyhydric alcohol is not particularly limited. For example, glycerin, 1,3-butyne glycol, 1,2-pentanediol, polyethylene glycol, propylene glycol, dipropylene glycol, polypropylene glycol, hexylene glycol, glycerin, diester Examples include glycerin. Preferred are glycerin, 1,3-butyne glycol, polyethylene glycol, propylene glycol, and dipropylene glycol, and more preferred are glycerin and 1,3-butyne glycol. One or two or more selected from these can be used in combination.
第2剤において多価アルコールの配合量は80〜99重量%であり、好ましくは85〜98重量%、より好ましくは90〜96重量%である。80重量%より少ないと発熱効果が十分でなく、99重量%より多いと化粧料の使用感を損ねる。 In the second agent, the blending amount of the polyhydric alcohol is 80 to 99% by weight, preferably 85 to 98% by weight, and more preferably 90 to 96% by weight. If it is less than 80% by weight, the heat generation effect is not sufficient, and if it exceeds 99% by weight, the feeling of use of the cosmetic is impaired.
第2剤に用いる油分としては、特に限定しないが、スクワラン、スクワレン、セレシン、オレフィンオリゴマー、流動パラフィン等の炭化水素類、オリーブ油、ホホバ油、アボカド油、アルモンド油、グレープシード油、月見草油、トウモロコシ油、ツバキ油、サザンカ油、マカデミアナッツ油、メドフォーム油、シアバター、ゴマ油、コメヌカ油、卵黄油等の油脂類、イソステアリルアルコール、オクチルドデカノール、ラノリンアルコール、フィトステロール、オレイルアルコール等の高級アルコール類、トリ2−エチルヘキサン酸グリセリル、ミリスチン酸イソプロピル、オレイン酸エチル、ステアリン酸オクチル、2−エチルヘキサン酸セチル、イソノナン酸イソノニル、パルミチン酸オクチル、ジオレイン酸エチレングリコール、トリイソステアリン酸グリセリル、乳酸セチル、アジピン酸ジイソプロピル、イソステアリン酸イソステアリル等のエステル油類、シクロメチコン、ジメチルポリシロキサン、メチルフェニルポリシロキサン、ポリエ−テル変性ポリシロキサン、アミノ変性ポリシロキサン、エポキシ変性ポリシロキサン、フッ素変性ポリシロキサン、アルコ−ル変性ポリシロキサン、アルキル変性ポリシロキサン、高分子シリコーン等のシリコーン類、ラウリン酸、ミリスチン酸、パルミチン酸、ステアリン酸、ベヘン(ベヘニン)酸、オレイン酸、12−ヒドロキシステアリン酸、ウンデシレン酸、トール酸、イソステアリン酸、リノール酸、リノレイン酸、エイコサペンタエン酸(EPA)、ドコサヘキサエン酸(DHA)等の高級脂肪酸等が挙げられる。好ましくは、スクワラン、スクワレン、オリーブ油、ホホバ油、シクロメチコン、ジメチルポリシロキサンが挙げられる。これらから選ばれる1種又は2種以上を組み合わせて使用することができる。油分の配合量としては0.5〜10重量%が好ましく、0.7〜5重量%がより好ましく、1〜3重量%がさらに好ましい。0.5重量%未満では発熱の持続性が十分に発揮せず、10重量%を超えて配合すると、製剤の安定性が悪くなる。 The oil component used in the second agent is not particularly limited, but hydrocarbons such as squalane, squalene, ceresin, olefin oligomer, liquid paraffin, olive oil, jojoba oil, avocado oil, almond oil, grape seed oil, evening primrose oil, corn Oil, camellia oil, sasanqua oil, macadamia nut oil, medofoam oil, shea butter, sesame oil, rice bran oil, egg yolk oil and other fats, isostearyl alcohol, octyldodecanol, lanolin alcohol, phytosterol, oleyl alcohol and other higher alcohols Glyceryl tri-2-ethylhexanoate, isopropyl myristate, ethyl oleate, octyl stearate, cetyl 2-ethylhexanoate, isononyl isononanoate, octyl palmitate, ethylene glycol dioleate, Ester oils such as glyceryl lyisostearate, cetyl lactate, diisopropyl adipate, isostearyl isostearate, cyclomethicone, dimethylpolysiloxane, methylphenylpolysiloxane, polyether-modified polysiloxane, amino-modified polysiloxane, epoxy-modified polysiloxane , Fluorine-modified polysiloxane, alcohol-modified polysiloxane, alkyl-modified polysiloxane, silicones such as high molecular silicone, lauric acid, myristic acid, palmitic acid, stearic acid, behenic acid, oleic acid, 12-hydroxy Higher fatty acids such as stearic acid, undecylenic acid, toluic acid, isostearic acid, linoleic acid, linolenic acid, eicosapentaenoic acid (EPA), docosahexaenoic acid (DHA), etc. . Preferably, squalane, squalene, olive oil, jojoba oil, cyclomethicone, and dimethylpolysiloxane are used. One or two or more selected from these can be used in combination. The blending amount of oil is preferably 0.5 to 10% by weight, more preferably 0.7 to 5% by weight, and further preferably 1 to 3% by weight. If the amount is less than 0.5% by weight, the persistence of heat generation cannot be sufficiently exhibited, and if the amount exceeds 10% by weight, the stability of the preparation is deteriorated.
第2剤における水の含有量は5重量%以下であり、好ましくは3重量%以下、より好ましくは2重量%以下である。5重量%より多いと発熱性が十分でない。水の含有量は発熱効果に影響を与え、少ない方が発熱性および発熱の持続性がよくなるため好ましい。そのため、水の含有量は実質的に0重量%、すなわち非水系の化粧料用組成物にすることがさらに好ましい。ここで、実質的に0重量%とは、液体の多価アルコール等の化粧料原料の中には、水分が含まれているものがあるため、水の含有量を完全に0重量%にはできないが、原料中に含まれている水以外の水を配合しないという意味である。 The content of water in the second agent is 5% by weight or less, preferably 3% by weight or less, more preferably 2% by weight or less. If it exceeds 5% by weight, the exothermicity is not sufficient. The water content affects the heat generation effect, and a smaller content is preferable because heat generation and heat generation persistence are improved. Therefore, it is more preferable that the water content is substantially 0% by weight, that is, a non-aqueous cosmetic composition is used. Here, “substantially 0% by weight” means that some cosmetic raw materials such as liquid polyhydric alcohols contain moisture, so that the water content is completely 0% by weight. Although it cannot, it means that water other than the water contained in the raw material is not blended.
第2剤には、さらに、カルボキシビニルポリマー、キサンタンガム、ヒドロキシエチルセルロースから選ばれる少なくとも1種以上を含有することにより発熱の持続性を高めることができる。カルボキシビニルポリマー、キサンタンガム、ヒドロキシエチルセルロースから選ばれる少なくとも1種以上の配合量は0.1〜1重量%が好ましく、0.2〜0.5重量%がより好ましい。0.1重量%未満では発熱の持続性が十分に発揮せず、1重量%を超えて配合すると、製剤の粘度が高くなり、化粧料の使用感が悪くなる。 The second agent can further increase the sustainability of heat generation by containing at least one selected from carboxyvinyl polymer, xanthan gum, and hydroxyethyl cellulose. The blending amount of at least one selected from carboxyvinyl polymer, xanthan gum and hydroxyethyl cellulose is preferably 0.1 to 1% by weight, more preferably 0.2 to 0.5% by weight. If it is less than 0.1% by weight, the sustainability of heat generation cannot be sufficiently exhibited, and if it exceeds 1% by weight, the viscosity of the preparation becomes high and the feeling of use of the cosmetics is deteriorated.
第2剤は、好ましくはゲル状の化粧料用組成物である。ゲル状にすることにより、皮膚に塗布しやすく、塗布した化粧料用組成物が皮膚上に長時間保持されるため、発熱効果の持続性をより高めることができる。皮膚への適度な発熱は、エステ効果およびマッサージ効果を付与することができ、特に胸元(デコルテ)、首および背中のケアに最適な化粧料にすることができる。 The second agent is preferably a gel cosmetic composition. By making it into a gel, it is easy to apply to the skin, and the applied cosmetic composition is held on the skin for a long time, so the durability of the heat generation effect can be further enhanced. Moderate fever on the skin can impart an esthetic effect and a massage effect, and can be a cosmetic that is particularly suitable for caring for the chest (decorte), neck and back.
本発明の第1剤および第2剤には、上記成分の他、通常、化粧料として使用できる成分を適宜配合することができる。例えば、紫外線吸収剤、粉体、酸化防止剤、界面活性剤、防腐剤、増粘剤、保湿剤、pH調整剤、着色料、植物エキス、香料などが挙げられる。具体的には次のものが例示される。 In addition to the above components, the first agent and the second agent of the present invention can be appropriately mixed with components that can usually be used as cosmetics. Examples include ultraviolet absorbers, powders, antioxidants, surfactants, preservatives, thickeners, humectants, pH adjusters, colorants, plant extracts, and fragrances. Specifically, the following are exemplified.
紫外線吸収剤として、パラアミノ安息香酸などの安息香酸系紫外線吸収剤、ホモメンチル−N−アセチルアントラニレート等のアントラニル酸系紫外線吸収剤、メンチルサリシレート等のサリチル酸系紫外線吸収剤、オクチルシンナメート等の桂皮酸系紫外線吸収剤、2,4−ジヒドロキシベンゾフェノン等のベンゾフェノン系紫外線吸収剤が挙げられる。 As UV absorbers, benzoic acid UV absorbers such as paraaminobenzoic acid, anthranilic acid UV absorbers such as homomenthyl-N-acetylanthranilate, salicylic acid UV absorbers such as menthyl salicylate, and cinnamon such as octylcinnamate Examples include acid ultraviolet absorbers and benzophenone ultraviolet absorbers such as 2,4-dihydroxybenzophenone.
粉体として、カオリン、無水ケイ酸、ケイ酸アルミニウムマグネシウム、セリサイト、タルク、窒化ホウ素、マイカ、セルロース末、シルク末、デンプン、ポリエチレン末、ナイロン末、架橋ポリスチレン等が挙げられる。酸化防止剤として、トコフェロール類、ジブチルヒドロキシトルエン、ブチルヒドロキシアニソール、没食子酸エステル類、アスコルビン酸等が挙げられる。金属封鎖剤としてフィチン酸、グルコン酸、エチレンジアミン四酢酸等が挙げられる。 Examples of the powder include kaolin, anhydrous silicic acid, magnesium aluminum silicate, sericite, talc, boron nitride, mica, cellulose powder, silk powder, starch, polyethylene powder, nylon powder, and crosslinked polystyrene. Examples of the antioxidant include tocopherols, dibutylhydroxytoluene, butylhydroxyanisole, gallic acid esters, ascorbic acid and the like. Examples of the metal sequestering agent include phytic acid, gluconic acid, and ethylenediaminetetraacetic acid.
界面活性剤として、アルキル硫酸エステル塩、ポリオキシエチレンアルキルエーテル硫酸エステル塩、N−アシルグルタミン酸塩、アルキロイルサルコシン塩、アルキロイルメチル−β−アラニン塩、アルキルスルホコハク酸塩、ポリオキシエチレンアルキルエーテルスルホコハク酸塩、アルキロイルメチルタウリン塩、アルカンスルホン酸塩、α−オレフィンスルホン酸塩、アルキルエーテル酢酸塩、ポリオキシエチレンアルキルエーテル酢酸塩、高級脂肪酸塩、アルキル燐酸塩、ポリオキシエチレンアルキルエーテル燐酸塩、イセチオネート系界面活性剤、アシル化ポリペプチドに代表されるアニオン性界面活性剤、アルキルベタイン型界面活性剤、アミドプロピルベタイン型界面活性剤、イミダゾリニウムベタイン型界面活性剤、スルホベタイン型界面活性剤、ホスホベタイン型界面活性剤に代表される両性界面活性剤、脂肪酸グリセリンエステル類、ソルビタン脂肪酸エステル類、ショ糖脂肪酸エステル類、ポリグリセリン脂肪酸エステル類、プロピレングリコール脂肪酸エステル類、ペンタエリトリトール脂肪酸エステル類、アルカノールアミド、アルキルアミンオキシド、ポリオキシエチレンアルキルエーテル、ポリオキシエチレンアルキルアリルエーテル、ポリオキシエチレンラノリンアルコール、アルキルフェノールホルマリン縮合物の酸化エチレン誘導体、プルロニック型界面活性剤、ポリオキシエチレンアルキルチオエーテル、ポリオキシエチレン脂肪酸エステル、ポリオキシエチレンソルビタン脂肪酸エステル、ポリオキシエチレングリセリンモノ脂肪酸エステル、ポリオキシエチレンプロピレングリコールモノ脂肪酸エステル、ポリオキシエチレンソルビトール脂肪酸エステル、ポリオキシエチレンヒマシ油、ポリオキシエチレンラノリン誘導体、ポリオキシエチレン脂肪酸アミド、ポリオキシエチレンアルキルアミン、アルキルポリグルコシドに代表されるノニオン性界面活性剤、塩化アルキルトリメチルアンモニウム、塩化ジアルキルジメチルアンモニウム、脂肪酸アミドアミン塩、エチル硫酸ラノリン脂肪酸アミノプロピルエチルジメチルアンモニウム、ジココイルエチルヒドロキシエチルモニウムメトサルフェートに代表されるカチオン性界面活性剤が挙げられる。 As surfactant, alkyl sulfate ester salt, polyoxyethylene alkyl ether sulfate ester salt, N-acyl glutamate salt, alkyloyl sarcosine salt, alkyloyl methyl-β-alanine salt, alkyl sulfosuccinate, polyoxyethylene alkyl ether sulfosuccinate Acid salt, alkyloylmethyl taurate, alkane sulfonate, α-olefin sulfonate, alkyl ether acetate, polyoxyethylene alkyl ether acetate, higher fatty acid salt, alkyl phosphate, polyoxyethylene alkyl ether phosphate, Isethionate surfactants, anionic surfactants typified by acylated polypeptides, alkyl betaine surfactants, amidopropyl betaine surfactants, imidazolinium betaine surfactants, sulfo Betaine surfactants, amphoteric surfactants typified by phosphobetaine surfactants, fatty acid glycerin esters, sorbitan fatty acid esters, sucrose fatty acid esters, polyglycerin fatty acid esters, propylene glycol fatty acid esters, penta Erythritol fatty acid esters, alkanolamides, alkylamine oxides, polyoxyethylene alkyl ethers, polyoxyethylene alkyl allyl ethers, polyoxyethylene lanolin alcohols, ethylene oxide derivatives of alkylphenol formalin condensates, pluronic surfactants, polyoxyethylene alkylthios Ether, polyoxyethylene fatty acid ester, polyoxyethylene sorbitan fatty acid ester, polyoxyethylene glycerol mono fatty acid ester Polyoxyethylene propylene glycol mono fatty acid ester, polyoxyethylene sorbitol fatty acid ester, polyoxyethylene castor oil, polyoxyethylene lanolin derivative, polyoxyethylene fatty acid amide, polyoxyethylene alkylamine, nonion represented by alkylpolyglucoside And cationic surfactants represented by alkyltrimethylammonium chloride, dialkyldimethylammonium chloride, fatty acid amidoamine salt, ethyl lanolin sulfate fatty acid aminopropylethyldimethylammonium, and dicocoylethylhydroxyethylmonium methosulfate.
防腐剤として、フェノキシエタノール、安息香酸塩、パラオキシ安息香酸エステル、1,2−ジブロモ−2,4−ジシアノブタン、イソチアゾロン誘導体、1,2−ヘキサンジオール、1,2−ペンタンジオール、ウンデシレン酸、ソルビン酸等が挙げられる。 As preservatives, phenoxyethanol, benzoate, paraoxybenzoate, 1,2-dibromo-2,4-dicyanobutane, isothiazolone derivatives, 1,2-hexanediol, 1,2-pentanediol, undecylenic acid, sorbic acid Etc.
増粘剤として、グアガム、デンプン、アラアビアガム、トラガカントガム、ガラクタン、カラヤガム、カラギーナン、ペクチン、カンテン、クインスシード(マルメロ)、アルゲコロイド(カッソウエキス)、デンプン(コメ、トウモロコシ、バレイショ、コムギ)、デキストラン、サクシノグルカン、プルラン、コラーゲン、カゼイン、アルブミン、ゼラチン等の天然高分子及びその誘導体、ヒドロキシプロピルメチルセルロース、ヒドロキシエチルセルロース、メチルセルロース、ニトロセルロース、エチルセルロース、メチルヒドロキシプロピルセルロース、セルロース硫酸ナトリウム、ヒドロキシプロピルセルロース、カルボキシメチルセルロースナトリウム(CMC)、結晶セルロース、セルロース末等のセルロース系高分子、アルギン酸ナトリウム、アルギン酸プロピレングリコールエステル等のアルギン酸系高分子、ポリビニルアルコール、ポリビニルメチルエーテル、ポリビニルピロリドン、カルボキシビニルポリマー(カーボポール)等のビニル系高分子、ポリエチレングリコール20,000、40,000、60,000等のポリオキシエチレン系高分子、ポリオキシエチレンポリオキシプロピレン共重合体共重合系高分子、ポリアクリル酸ナトリウム、ポリエチルアクリレート、ポリアクリルアミド等のアクリル系高分子、ポリエチレンイミン、カチオンポリマー等が挙げられる。 Thickeners include guar gum, starch, arabia gum, tragacanth gum, galactan, karaya gum, carrageenan, pectin, agar, quince seed (malmello), algae colloid (gypsum extract), starch (rice, corn, potato, wheat), dextran, saxino Natural polymers such as glucan, pullulan, collagen, casein, albumin, gelatin and derivatives thereof, hydroxypropylmethylcellulose, hydroxyethylcellulose, methylcellulose, nitrocellulose, ethylcellulose, methylhydroxypropylcellulose, sodium cellulose sulfate, hydroxypropylcellulose, sodium carboxymethylcellulose (CMC), cellulose-based polymers such as crystalline cellulose and cellulose powder, Alginic acid polymers such as sodium formate and propylene glycol alginate, vinyl polymers such as polyvinyl alcohol, polyvinyl methyl ether, polyvinylpyrrolidone and carboxyvinyl polymer (Carbopol), polyethylene glycol 20,000, 40,000, 60 , 000, etc., polyoxyethylene polymer, polyoxyethylene polyoxypropylene copolymer copolymer polymer, acrylic polymer such as sodium polyacrylate, polyethyl acrylate, polyacrylamide, polyethyleneimine, cationic polymer, etc. Is mentioned.
保湿剤として、プロピレングリコール、ジプロピレングリコール、ポリプロピレングリコール、ポリエチレングリコール、グリセリン、ジグリセリン、イソプレングリコール、1,3−ブチレングリコール、エチルアルコール、イソプロパノール等の多価アルコール類、キシリトール、ソルビトール、マルチトール等の糖アルコール類、コンドロイチン硫酸、ヒアルロン酸、ムコイチン硫酸、アテロコラーゲン、コレステリル−12−ヒドロキシステアレート、海洋深層水、キトサン誘導体、ピロリドンカルボン酸ナトリウム等が挙げられる。 As humectants, polyhydric alcohols such as propylene glycol, dipropylene glycol, polypropylene glycol, polyethylene glycol, glycerin, diglycerin, isoprene glycol, 1,3-butylene glycol, ethyl alcohol, isopropanol, xylitol, sorbitol, maltitol, etc. Sugar alcohols, chondroitin sulfate, hyaluronic acid, mucoitin sulfate, atelocollagen, cholesteryl-12-hydroxystearate, deep sea water, chitosan derivatives, sodium pyrrolidone carboxylate and the like.
pH調整剤として、乳酸、乳酸ナトリウム、クエン酸、クエン酸ナトリウム、水酸化ナトリウム、水酸化カリウム、リン酸等が挙げられる。その他適宜必要に応じて法定色素、天然色素などの着色料や香料を選択できる。 Examples of the pH adjuster include lactic acid, sodium lactate, citric acid, sodium citrate, sodium hydroxide, potassium hydroxide, and phosphoric acid. In addition, colorants and fragrances such as legal pigments and natural pigments can be selected as appropriate.
植物エキス等の天然成分として、アシタバ、アボガド、アマチャ、アルテア、アルニカ、アロエ、アンズ、イチョウ、ウイキョウ、ウコン、ウーロン茶、エイジツ、エチナシ葉、オウゴン、オウバク、オウレン、オオムギ、オトギリソウ、オドリコソウ、オランダカラシ、オレンジ、海藻、カモミラ、カロット、カワラヨモギ、甘草、カルカデ、カキョク、キウイ、キナ、キューカンバー、グアノシン、クチナシ、クマザサ、クララ、クルミ、グレープフルーツ、クレマティス、クロレラ、クワ、ゲンチアナ、紅茶、ゴボウ、コメヌカ、コメ胚芽油、コンフリー、コケモモ、サイシン、サイコ、サイタイ、サルビア、サボンソウ、ササ、サンザシ、サンショウ、シイタケ、ジオウ、シコン、シソ、シナノキ、シモツケソウ、シャクヤク、ショウブ根、シラカバ、スギナ、セイヨウキズタ、セイヨウサンザシ、セイヨウニワトコ、セイヨウノコギリソウ、セイヨウハッカ、セージ、ゼニアオイ、センキュウ、センブリ、ダイズ、タイソウ、タイム、茶、緑茶、チョウジ、チガヤ、チンピ、トウキ、トウキンセンカ、トウニン、トウヒ、ドクダミ、トマト、納豆、ニンジン、ニンニク、ノバラ、ハイビスカス、バクモンドウ、ハス、パセリ、ハマメリス、パリエタリア、ヒキオコシ、ビサボロール、ビワ、フキタンポポ、フキノトウ、ブクリョウ、ブッチャーブルーム、ブドウ、ヘチマ、ベニバナ、ペパーミント、ボダイジュ、ボタン、ホップ、マツ、マロニエ、ミズバショウ、ムクロジ、メリッサ、モモ、ヤグルマギク、ユーカリ、ユキノシタ、ユズ、ヨクイニン、ヨモギ、ラベンダー、リンゴ、レタス、レモン、レンゲソウ、ローズ、ローズマリー、ローマカミツレ等のエキスや、シルク、酵母、蜂蜜、プロポリス、ローヤルゼリー、コラーゲン、エラスチン等をあげることができる。 As natural ingredients such as plant extracts, Ashitaba, Avocado, Achacha, Altea, Arnica, Aloe, Apricot, Ginkgo, Fennel, Turmeric, Oolong Tea, Ages, Echinacea leaf, Ogon, Oubak, Ouren, Barley, Hypericum, Odori Orange, seaweed, camomile, carrot, sagebrush, licorice, calcade, oyster, kiwi, kina, cucumber, guanosine, gardenia, kumazasa, clara, walnut, grapefruit, clematis, chlorella, mulberry, gentian, tea, burdock, rice bran, rice germ Oil, Comfrey, Cowberry, Saishin, Psycho, Saitai, Salvia, Salamander, Sasa, Hawthorn, Salamander, Shiitake, Giant, Shikon, Perilla, Linden, Periwinkle, Peonies, Sho Bush root, birch, horsetail, horseshoe, hawthorn, elderberry, achillea millefolium, mint sage, sage, mallow, senbu, assembly, soybeans, tiso, thyme, tea, green tea, clove, chigaya, chimpi, toki, tokisenka , Tonin, spruce, dokudami, tomato, natto, carrot, garlic, wild rose, hibiscus, buckwheat, lotus, parsley, sea cucumber, parietalia, toad, bisabolol, loquat, dandelion, burdock, butcher bloom, beech maize Peppermint, Bodaige, Button, Hop, Pine, Marronnier, Mizubasho, Mukuroji, Melissa, Peach, Cornflower, Eucalyptus, Yukinoshita, Yuzu, Yokuinin, Mugwort, Ravenda , Mention may be made of apples, lettuce, lemon, Rengesou, rose, rosemary, and extracts such as chamomile, silk, yeast, honey, propolis, royal jelly, collagen, elastin and the like.
香料として、ペパーミント油、スペアミント油、ラベンダー油、ジャスミン油、ローズ油、レモン油、オレンジ油、ハッカ油、タイム油、ショウブ油、ウイキョウ油、スギ油、ヒバ油、ラズベリー油、ヒノキ油、バラ油、ユーカリ油、カンファー、ゲラニオール、ミカン油、トウヒ、シトロネロール、テルペン類、コーヒー油、茶油、椿油、ラズベリーケトン等の天然及び合成香料等が挙げられる。 As perfumes, peppermint oil, spearmint oil, lavender oil, jasmine oil, rose oil, lemon oil, orange oil, peppermint oil, thyme oil, ginger oil, fennel oil, cedar oil, hiba oil, raspberry oil, cypress oil, rose oil Natural and synthetic fragrances such as eucalyptus oil, camphor, geraniol, mandarin oil, spruce, citronellol, terpenes, coffee oil, tea oil, coconut oil, and raspberry ketone.
本発明の2剤式化粧料はマッサージ施術時において第1剤と第2剤を適宜組合せて使用するものであるが、第1剤を皮膚に塗布した後に、第2剤を皮膚に塗布するのが好ましい。より好ましくは、第1剤を塗布し、マッサージを行った後、ガーゼや布、タオルなどで拭き取り、すぐに第2剤を塗布しマッサージする。第1剤と第2剤の量は、適宜選択できるが、重量比で2:1〜1:3であるのが好ましい。2:1より第1剤が多いと第2剤を塗布した際に皮膚上の水分が多すぎるので発熱が十分でなく、1:3より第2剤が多いと第2剤を塗布した際に皮膚上の水分が十分でなく十分な発熱が得られない。このように2剤式化粧料とすることで1剤式の場合よりも皮膚温度の上昇効果、血流の促進効果、皮膚水分量の増加効果が期待できる。 The two-component cosmetic of the present invention is used by appropriately combining the first agent and the second agent during massage treatment. After the first agent is applied to the skin, the second agent is applied to the skin. Is preferred. More preferably, after the first agent is applied and massaged, it is wiped off with gauze, cloth, towels, etc., and the second agent is immediately applied and massaged. The amount of the first agent and the second agent can be appropriately selected, but is preferably 2: 1 to 1: 3 by weight ratio. When there is more 1st agent than 2: 1, there is too much moisture on the skin when applying 2nd agent, so heat is not enough, and when there is more 2nd agent than 1: 3, when 2nd agent is applied There is not enough moisture on the skin and sufficient fever cannot be obtained. Thus, by setting it as 2 agent type cosmetics, the raise effect of skin temperature, the blood flow promotion effect, and the increase effect of skin moisture content can be anticipated rather than the case of 1 agent type.
本発明は、上記2剤式化粧料を用いた2剤式化粧料を用いることを特徴とする美容方法を包含する。上記2剤式の化粧料を用い、マッサージをすることによりエステ効果を向上させることができる。好ましい美容方法として、第1剤を肌に塗布しマッサージを30秒〜10分程度、好ましくは1〜5分程度行い、肌の上に残存する第1剤を布又はガーゼなどを用いて拭き取り、第2剤を塗布して30秒〜20分、好ましくは1分〜10分程度マッサージを行う。マッサージは通常の美容マッサージでよい。このように2剤式による2ステップでマッサージを行うことにより、1剤式では不十分であった皮膚温度を向上させる効果、血流を促進させる効果、および肌の水分を増加させる効果(保湿効果)をより発揮することができる。
The present invention includes a cosmetic method characterized by using a two-component cosmetic using the two-component cosmetic. The esthetic effect can be improved by massage using the two-component cosmetic. As a preferred cosmetic method, the first agent is applied to the skin and massaged for about 30 seconds to 10 minutes, preferably about 1 to 5 minutes, and the first agent remaining on the skin is wiped off using a cloth or gauze, The second agent is applied and massaged for 30 seconds to 20 minutes, preferably about 1 minute to 10 minutes. The massage can be a normal beauty massage. Thus, by performing massage in two steps by the two-agent type, the effect of improving the skin temperature, the effect of promoting blood flow, and the effect of increasing the moisture of the skin (moisturizing effect) ).
以下、実施例を挙げて本発明をさらに詳しく説明するが、本発明はこれら実施例に限定されるものではない。特に断りのない限り%は重量%を表す。 EXAMPLES Hereinafter, although an Example is given and this invention is demonstrated in more detail, this invention is not limited to these Examples. Unless otherwise indicated, “%” represents “% by weight”.
[試験例1]
以下の成分からなる第1剤例1(クレンジング)を常法により製造した。
オレフィンオリゴマー 30
トリ2−エチルヘキサン酸グリセリル 20
グリセリン 10
ラウリン酸ポリグリセリル−10 3
1,3−ブチレングリコール 1.5
マンナン 1
カルボキシビニルポリマー 0.4
パラベン 0.3
水酸化カリウム 0.2
香料 0.2
水 残部
(合計) 100 重量%
[Test Example 1]
The 1st agent example 1 (cleansing) which consists of the following components was manufactured by the conventional method.
Glyceryl tri-2-
Polyglyceryl laurate-10 3
1,3-butylene glycol 1.5
Carboxyvinyl polymer 0.4
Paraben 0.3
Potassium hydroxide 0.2
Fragrance 0.2
Water balance (total) 100% by weight
表1に記載する第2剤(ジェル)を常法により製造した。
第1剤例1を適量とり、成人女性3名の下腕内側に約2×2cmで6ヶ所(左右3ヶ所)試験部位にそれぞれ0.5g塗布した。30秒後、第1剤をガーゼで拭き取った。その後すぐに、第2剤例1〜6を適量とり、同一部位に塗布した。第1剤の塗布前、第2剤の塗布直後、塗布3分後、塗布6分後、塗布9分後の皮膚温度を赤外線サーモグラフィ(Handy Thermo TVS-200EX、Avio社製)で測定し、画像解析により温度変化を算出した。
The 2nd agent (gel) described in Table 1 was manufactured by the conventional method.
Appropriate amount of the first agent example 1 was taken, and 0.5 g each was applied to the test sites of 6 adults (3 sites on the left and right sides) at about 2 × 2 cm inside the lower arm of 3 adult women. After 30 seconds, the first agent was wiped off with gauze. Immediately thereafter, an appropriate amount of the second agent example 1-6 was taken and applied to the same site. Before applying the first agent, immediately after applying the second agent, 3 minutes after application, 6 minutes after application, and 9 minutes after application, the skin temperature was measured by infrared thermography (Handy Thermo TVS-200EX, manufactured by Avio). The temperature change was calculated by analysis.
皮膚温度の結果は図1に示す。図1は時間を横軸に皮膚温度の塗布直前の温度からの変化量を縦軸にしたものである。第2剤例1(水0%)及び例2(水1%)は皮膚の温度上昇がきわめて大きく、第2剤例3(水3%)及び例4(水5%)は皮膚の温度が高くなっている。一方、第2剤例5及び例6は温度がかえって低くなっている。
The skin temperature results are shown in FIG. FIG. 1 shows time on the horizontal axis and the amount of change from the temperature immediately before application of the skin temperature on the vertical axis. The second agent example 1 (
[試験例2]
化粧料用組成物は試験例1の第1剤例1と第2剤例2を用いた。
第1剤を適量とり、成人女性1名の肩部に塗布し1分間クレンジングおよびスクラブマッサージを行った後、第1剤をガーゼで拭き取った。その後すぐに、第2剤を適量とり、同一部位(肩部)に塗布し3分間マッサージを行った。試験は24℃、湿度50%の恒温恒湿下で行った。塗布部位の水分量を水分量測定器SKICON-200で測定した。塗布部位および顔面の皮膚温度を赤外線サーモグラフィ(Handy
Thermo TVS-200EX、Avio社製)で測定し、画像解析で温度変化量を算出した。顔の血流量をレーザードップラー血流画像化装置PeriScanPIM3で測定し、第1剤塗布前の血流量を1としたときの比を求めた。
[Test Example 2]
As the cosmetic composition, Example 1 and Example 2 of Test Example 1 were used.
An appropriate amount of the first agent was taken and applied to the shoulder of one adult woman, and after 1 minute cleansing and scrub massage, the first agent was wiped with gauze. Immediately thereafter, an appropriate amount of the second agent was taken, applied to the same site (shoulder), and massaged for 3 minutes. The test was performed under constant temperature and humidity of 24 ° C. and a humidity of 50%. The moisture content at the application site was measured with a moisture meter SKICON-200. Infrared thermography (Handy)
Thermo TVS-200EX, manufactured by Avio), and the amount of temperature change was calculated by image analysis. The blood flow volume of the face was measured with a laser Doppler blood flow imaging device PeriScanPIM3, and the ratio when the blood flow volume before application of the first agent was set to 1 was determined.
図2に示すように、第1剤でグレンジングした後に第2剤でマッサージを行うことにより水分量の増加がみられた。また、図3および図4で示すように、塗布部位および顔面の皮膚温度が上昇した。図5で示すように、顔の血流量が増加した。 As shown in FIG. 2, an increase in the amount of water was observed by performing a massage with the second agent after the cleansing with the first agent. Moreover, as shown in FIG. 3 and FIG. 4, the skin temperature of the application site and the face increased. As shown in FIG. 5, facial blood flow increased.
以下、本発明の処方例をさらに示す。
[処方例1]
以下の成分からなる第1剤例1を常法により製造した。
オレフィンオリゴマー 20
トリ2−エチルヘキサン酸グリセリル 25
スクワラン 5
オリーブ油 5
グリセリン 8
ラウリン酸ポリグリセリル−10 3
1,3−ブチレングリコール 3
マンナン 1
カルボキシビニルポリマー 0.3
パラベン 0.2
プルーン分解物 0.2
ビルベリー葉エキス 0.01
アセチル化ヒアルロン酸ナトリウム 0.01
水酸化カリウム 0.2
香料 0.2
水 残部
(合計) 100 重量%
Hereinafter, the formulation example of this invention is further shown.
[Prescription Example 1]
A first example 1 consisting of the following components was produced by a conventional method.
Glyceryl tri-2-ethylhexanoate 25
Squalane 5
Olive oil 5
Glycerin 8
Polyglyceryl laurate-10 3
1,3-
Carboxyvinyl polymer 0.3
Paraben 0.2
Prune degradation product 0.2
Bilberry leaf extract 0.01
Acetylated sodium hyaluronate 0.01
Potassium hydroxide 0.2
Fragrance 0.2
Water balance (total) 100% by weight
[処方例2]
以下の成分からなる第2剤例7を常法により製造した。
濃グリセリン 90
ポリエチレングリコール(分子量400) 2
1,3-ブチレングリコール 1
デカグリセリン脂肪酸エステルエイコサン二酸縮合物 3.5
スクワラン 1
カルボキシビニルポリマー 0.3
ヒドロキシエチルセルロース 0.1
パラベン 0.2
トリエタノールアミン 0.1
ビルベリー葉エキス 0.02
ラッカセイ種皮エキス 0.03
水 1.75
香料 0.1
(合計) 100 重量%
[Prescription Example 2]
A second example 7 comprising the following components was prepared by a conventional method.
Concentrated glycerin 90
Polyethylene glycol (molecular weight 400) 2
1,3-
Decaglycerin fatty acid ester eicosane diacid condensate 3.5
Carboxyvinyl polymer 0.3
Hydroxyethyl cellulose 0.1
Paraben 0.2
Triethanolamine 0.1
Bilberry leaf extract 0.02
Peanut seed coat extract 0.03
Water 1.75
Fragrance 0.1
(Total) 100 wt%
[処方例3]
以下の成分からなる発熱性のある第2剤例8を常法により製造した。
濃グリセリン 93
デカグリセリン脂肪酸エステルエイコサン二酸縮合物 3
オリーブ油 0.3
シクロペンタシロキサン 0.6
カルボキシビニルポリマー 0.5
キサンタンガム 0.1
パラベン 0.2
トリエタノールアミン 0.2
ヒアルロン酸 0.01
ビタミンE 0.01
水 1.88
香料 0.2
(合計) 100 重量%
[Prescription Example 3]
A second exothermic agent example 8 comprising the following components was produced by a conventional method.
Concentrated glycerin 93
Decaglycerin fatty acid ester
Olive oil 0.3
Cyclopentasiloxane 0.6
Carboxyvinyl polymer 0.5
Xanthan gum 0.1
Paraben 0.2
Triethanolamine 0.2
Hyaluronic acid 0.01
Vitamin E 0.01
Water 1.88
Fragrance 0.2
(Total) 100 wt%
第1剤例1、2および第2剤例1〜4、7、8を適宜組み合わせて、本発明の2剤式化粧料を得た。さらに、第1剤例2を塗布しマッサージした後、第2剤例1〜4、7、8を塗布しマッサージすることにより皮膚温度が向上した。
First agent examples 1 and 2 and second agent examples 1 to 4, 7, and 8 were appropriately combined to obtain a two-component cosmetic of the present invention. Furthermore, after apply | coating and massaging the 1st agent example 2, the skin temperature improved by apply | coating and massaging the 2nd agent examples 1-4, 7, and 8.
Claims (4)
第1剤:水を20〜40重量%、油分を40〜80重量%およびスクラブ剤を含有する化粧料用組成物
第2剤:デカグリセリン脂肪酸エステルエイコサン二酸縮合物を1〜10重量%、グリセリン、1,3−ブチングリコール、ポリエチレングリコール、プロピレングリコール、ジプロピレングリコールから選ばれる少なくとも1種以上からなる多価アルコールを90〜96重量%、及びスクワラン、スクワレン、オリーブ油、ホホバ油、シクロメチコン、ジメチルポリシロキサンから選ばれる少なくとも1種以上からなる油分を0.5〜10重量%含有し、水の含有量が5重量%以下で、無機化合物の粉体を含有しない化粧料用組成物。 A two-component cosmetic comprising the following first and second agents.
First agent: Cosmetic composition containing 20 to 40% by weight of water, 40 to 80% by weight of oil and scrub agent Second agent: 1 to 10% by weight of decaglycerin fatty acid ester eicosane diacid condensate , 90 to 96 % by weight of polyhydric alcohol consisting of at least one selected from glycerin, 1,3-butyne glycol, polyethylene glycol, propylene glycol and dipropylene glycol , and squalane, squalene, olive oil, jojoba oil, cyclomethicone A cosmetic composition containing 0.5 to 10% by weight of an oil composed of at least one selected from dimethylpolysiloxane , having a water content of 5% by weight or less and containing no inorganic compound powder .
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JP2007174987A JP5199612B2 (en) | 2007-07-03 | 2007-07-03 | Two-part cosmetic |
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Families Citing this family (4)
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CA2751304C (en) | 2009-02-03 | 2016-08-02 | Sunstar Inc. | Hesperidin-containing composition |
WO2010140319A1 (en) * | 2009-06-01 | 2010-12-09 | 花王株式会社 | Cleansing method |
JP6589237B2 (en) * | 2015-07-24 | 2019-10-16 | ポーラ化成工業株式会社 | Gel-like face wash containing agar |
JP6086462B1 (en) * | 2016-10-26 | 2017-03-01 | 株式会社 サティス製薬 | Paste cleansing cosmetic |
Family Cites Families (11)
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JPS6210009A (en) * | 1985-07-06 | 1987-01-19 | Nonogawa Shoji:Kk | Cosmetic containing hydrogenated jojoba oil as scrubbing agent |
JPH03106809A (en) * | 1989-09-19 | 1991-05-07 | Asahi Chem Ind Co Ltd | Cellulosic scrubbing material |
JPH05221822A (en) * | 1991-10-01 | 1993-08-31 | Shiseido Co Ltd | Cosmetic |
JPH07304647A (en) * | 1994-05-09 | 1995-11-21 | Kao Corp | Composition for massage |
JP2001048745A (en) * | 1999-08-10 | 2001-02-20 | Kanebo Ltd | Beauty care |
JP2001058936A (en) * | 1999-08-19 | 2001-03-06 | Shiseido Co Ltd | Cosmetic comprising granule formulated therein |
JP2001131054A (en) * | 1999-10-29 | 2001-05-15 | Nishikawa Rubber Co Ltd | Scrubbing agent and its production |
WO2003015741A1 (en) * | 2001-08-13 | 2003-02-27 | The Nisshin Oillio, Ltd. | Humectant and cosmetics and external preparations containing the same |
JP2003300826A (en) * | 2002-02-06 | 2003-10-21 | Pola Chem Ind Inc | Warmth-feeling cosmetic |
JP4090384B2 (en) * | 2003-05-08 | 2008-05-28 | 株式会社ノエビア | Solid polyhydric alcohol base |
JP2006219465A (en) * | 2005-02-08 | 2006-08-24 | Estate Chemical Kk | Cosmetic |
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