JP5106127B2 - 第四オニウム塩を精製するための方法 - Google Patents

第四オニウム塩を精製するための方法 Download PDF

Info

Publication number
JP5106127B2
JP5106127B2 JP2007558303A JP2007558303A JP5106127B2 JP 5106127 B2 JP5106127 B2 JP 5106127B2 JP 2007558303 A JP2007558303 A JP 2007558303A JP 2007558303 A JP2007558303 A JP 2007558303A JP 5106127 B2 JP5106127 B2 JP 5106127B2
Authority
JP
Japan
Prior art keywords
resin
anion
concentration
solution
group
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2007558303A
Other languages
English (en)
Japanese (ja)
Other versions
JP2008536809A5 (enExample
JP2008536809A (ja
Inventor
ズィゲル,アルフレッド
テイッセン,ミヒャエル
カンシック−コンラドセン,アンドレアス
デメル,ソンジャ
ネレンズ,フランク
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Honeywell International Inc
Original Assignee
Honeywell International Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Honeywell International Inc filed Critical Honeywell International Inc
Publication of JP2008536809A publication Critical patent/JP2008536809A/ja
Publication of JP2008536809A5 publication Critical patent/JP2008536809A5/ja
Application granted granted Critical
Publication of JP5106127B2 publication Critical patent/JP5106127B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82Purification; Separation; Stabilisation; Use of additives
    • C07C209/84Purification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82Purification; Separation; Stabilisation; Use of additives
    • C07C209/86Separation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00Compounds containing amino groups bound to a carbon skeleton
    • C07C211/62Quaternary ammonium compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00Compounds containing amino groups bound to a carbon skeleton
    • C07C211/62Quaternary ammonium compounds
    • C07C211/63Quaternary ammonium compounds having quaternised nitrogen atoms bound to acyclic carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/025Purification; Separation; Stabilisation; Desodorisation of organo-phosphorus compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/54Quaternary phosphonium compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/54Quaternary phosphonium compounds
    • C07F9/5407Acyclic saturated phosphonium compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/6564Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
    • C07F9/6568Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus atoms as the only ring hetero atoms
    • C07F9/65688Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus atoms as the only ring hetero atoms the ring phosphorus atom being part of a phosphonium compound

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Electric Double-Layer Capacitors Or The Like (AREA)
  • Pyridine Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pyrrole Compounds (AREA)
JP2007558303A 2005-03-04 2006-03-03 第四オニウム塩を精製するための方法 Expired - Fee Related JP5106127B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US65854505P 2005-03-04 2005-03-04
US60/658,545 2005-03-04
PCT/US2006/007784 WO2006096578A1 (en) 2005-03-04 2006-03-03 Method for purifying quaternary onium salts

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2012156737A Division JP5501411B2 (ja) 2005-03-04 2012-07-12 第四オニウム塩を精製するための方法

Publications (3)

Publication Number Publication Date
JP2008536809A JP2008536809A (ja) 2008-09-11
JP2008536809A5 JP2008536809A5 (enExample) 2008-12-25
JP5106127B2 true JP5106127B2 (ja) 2012-12-26

Family

ID=36646213

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2007558303A Expired - Fee Related JP5106127B2 (ja) 2005-03-04 2006-03-03 第四オニウム塩を精製するための方法
JP2012156737A Expired - Fee Related JP5501411B2 (ja) 2005-03-04 2012-07-12 第四オニウム塩を精製するための方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2012156737A Expired - Fee Related JP5501411B2 (ja) 2005-03-04 2012-07-12 第四オニウム塩を精製するための方法

Country Status (6)

Country Link
US (1) US7601871B2 (enExample)
EP (1) EP1856027B1 (enExample)
JP (2) JP5106127B2 (enExample)
KR (1) KR20070114381A (enExample)
CN (1) CN101163661B (enExample)
WO (1) WO2006096578A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012232993A (ja) * 2005-03-04 2012-11-29 Honeywell Internatl Inc 第四オニウム塩を精製するための方法

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5121248B2 (ja) * 2007-02-23 2013-01-16 日本カーリット株式会社 スピロ型第四級アンモニウム化合物の製造方法及び該スピロ型第四級アンモニウム化合物並びにその用途
US8000084B2 (en) * 2007-07-25 2011-08-16 Honeywell International, Inc. High voltage electrolytes
CN102448431A (zh) * 2009-05-28 2012-05-09 默克专利股份有限公司 抗头屑试剂
CN101993380B (zh) * 2009-08-11 2013-05-01 兆联实业股份有限公司 氢氧化四甲基铵的回收设备及其方法
US8493713B2 (en) 2010-12-14 2013-07-23 Avx Corporation Conductive coating for use in electrolytic capacitors
US8576543B2 (en) 2010-12-14 2013-11-05 Avx Corporation Solid electrolytic capacitor containing a poly(3,4-ethylenedioxythiophene) quaternary onium salt
US8451588B2 (en) 2011-03-11 2013-05-28 Avx Corporation Solid electrolytic capacitor containing a conductive coating formed from a colloidal dispersion
JP5724042B2 (ja) * 2011-08-24 2015-05-27 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 電気化学または光電子デバイスのための硫黄含有添加剤
US8636916B2 (en) 2011-08-30 2014-01-28 Corning Incorporated Electrolyte synthesis for ultracapacitors
US8971019B2 (en) 2012-03-16 2015-03-03 Avx Corporation Wet capacitor cathode containing an alkyl-substituted poly(3,4-ethylenedioxythiophene)
CN106565499B (zh) * 2016-09-30 2018-10-23 多氟多化工股份有限公司 一种利用微通道反应器合成四乙基四氟硼酸铵的方法
CN106674232A (zh) * 2017-01-04 2017-05-17 湖南省正源储能材料与器件研究所 一种用离子交换净化法制备高纯螺环季铵盐的方法
KR101830636B1 (ko) 2017-01-04 2018-02-21 삼화페인트공업주식회사 스피로 4차 암모늄 염의 제조 방법
JP2023035836A (ja) * 2021-08-31 2023-03-13 富士フイルム株式会社 感活性光線性又は感放射線性樹脂組成物の製造方法、パターン形成方法、電子デバイスの製造方法、及びオニウム塩の製造方法
CN115477926B (zh) * 2022-09-15 2024-06-25 江苏科技大学 一种相变材料及其制备方法

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01246386A (ja) * 1987-11-25 1989-10-02 Asahi Glass Co Ltd オニウム塩の製造方法
FR2639888B1 (fr) * 1988-12-07 1993-08-13 Valeo Vision Projecteur de vehicule automobile, comportant un reflecteur a surface complexe a zones intermediaires modifiees
US5086374A (en) 1989-05-24 1992-02-04 Specialised Conductives Pty. Limited Aprotic electrolyte capacitors and methods of making the same
JPH03167160A (ja) * 1989-11-22 1991-07-19 Sumitomo Chem Co Ltd 水酸化第四級アンモニウム水溶液の精製方法
US5965054A (en) * 1997-08-12 1999-10-12 Covalent Associates, Inc. Nonaqueous electrolyte for electrical storage devices
US5968338A (en) * 1998-01-20 1999-10-19 Sachem, Inc. Process for recovering onium hydroxides from solutions containing onium compounds
US6207039B1 (en) * 1998-04-07 2001-03-27 Sachem, Inc. Process for recovering onium hydroxides or onium salts from solutions containing onium compounds using electrochemical ion exchange
JP3324502B2 (ja) * 1998-05-14 2002-09-17 日本メクトロン株式会社 アクリルエラストマー組成物
JP2002053532A (ja) * 2000-08-07 2002-02-19 Tonen Chem Corp 四級アンモニウム塩の精製方法
CN1177804C (zh) * 2001-12-28 2004-12-01 中国石油化工股份有限公司 一种由季铵盐制备季铵碱的方法
US6787021B2 (en) * 2002-01-03 2004-09-07 Sachem, Inc. Purification of onium hydroxides by electrodialysis
JP4194296B2 (ja) * 2002-05-14 2008-12-10 ステラケミファ株式会社 四級アルキルアンモニウム塩の精製方法及び四級アルキルアンモニウム塩の製造方法
DE10250808B3 (de) 2002-10-31 2004-04-08 Honeywell Specialty Chemicals Seelze Gmbh Tetraalkylammoniumtetrafluoroborat-haltige Elektrolytzusammensetzung, Verfahren zur Herstellung dieser Tetraalkylammoniumtetrafluoroborathaltiger Elektrolytzusammensetzungen sowie deren Verwendung
KR20070114381A (ko) * 2005-03-04 2007-12-03 허니웰 인터내셔널 인코포레이티드 4급 오니움염의 정제방법

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012232993A (ja) * 2005-03-04 2012-11-29 Honeywell Internatl Inc 第四オニウム塩を精製するための方法

Also Published As

Publication number Publication date
EP1856027A1 (en) 2007-11-21
CN101163661A (zh) 2008-04-16
KR20070114381A (ko) 2007-12-03
CN101163661B (zh) 2015-08-19
JP2012232993A (ja) 2012-11-29
JP2008536809A (ja) 2008-09-11
US7601871B2 (en) 2009-10-13
US20060247472A1 (en) 2006-11-02
WO2006096578A1 (en) 2006-09-14
EP1856027B1 (en) 2016-04-20
JP5501411B2 (ja) 2014-05-21

Similar Documents

Publication Publication Date Title
JP5501411B2 (ja) 第四オニウム塩を精製するための方法
US8029689B2 (en) Method for producing high-purity quaternary ammonium salt
EP1919922A1 (en) Method for synthesizing spiro quaternary ammonium systems
KR20060105452A (ko) 초고순도 이온성 액체
JP4430818B2 (ja) オニウム化合物を含有する溶液から水酸化オニウムを回収するプロセス
JP2005139100A (ja) 常温溶融塩
CN104292114A (zh) 一种鎓氢氧化物的制备方法
EP0028430B1 (en) A process for the electroreductive preparation of organic compounds
CN1293231C (zh) 通过电渗析纯化氢氧化鎓
CN101851526A (zh) 以离子液体为氟磺酸的促进剂生产烷基化汽油的方法
JP2004221557A (ja) 電解液
CN108047137A (zh) 一种含有醚基功能基团氨基酸咪唑盐离子液体及其制备方法
CN103992275A (zh) 一种氟化盐离子液体的合成方法
JP2005089313A (ja) イオン性液体の精製方法
CN106674232A (zh) 一种用离子交换净化法制备高纯螺环季铵盐的方法
CN102199096A (zh) 一种合成有机离子化合物的方法
JP4732704B2 (ja) イオン性液体およびその製造方法
CN1521163A (zh) 室温离子液体的制备方法
CN102276439B (zh) 一种脂肪酸根类离子液体的制备方法
Li et al. Redox Reaction: A New Route for the Synthesis of Water-Miscible Imidazolium Ionic Liquids
CN101068791B (zh) 卤化物含量减少的、带四氟硼酸盐阴离子的鎓盐的制备方法
D'Aprano et al. The conductance of lithium-7 fluoride in dioxane-water mixtures at 25° C
Wendt et al. Halogen Bonding in N‐Alkyl‐Bromo‐/Lodo‐Pyridinium Salts and its Application in Chromatography
CN115724805B (zh) N,n-二甲基吡咯烷鎓二氟草酸硼酸盐及应用和制备
Merli et al. A detailed study of the (electro) chemical behavior of bis (trifluoromethanesulfonyl) imide based ionic liquids at different purification steps

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20081029

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20081029

RD04 Notification of resignation of power of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7424

Effective date: 20110909

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20111124

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20111129

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20120223

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20120315

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20120712

A911 Transfer to examiner for re-examination before appeal (zenchi)

Free format text: JAPANESE INTERMEDIATE CODE: A911

Effective date: 20120723

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20120903

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20121002

R150 Certificate of patent or registration of utility model

Ref document number: 5106127

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20151012

Year of fee payment: 3

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees