JP5079230B2 - ウィスカー状の金属酸化物及びその複合体 - Google Patents
ウィスカー状の金属酸化物及びその複合体 Download PDFInfo
- Publication number
- JP5079230B2 JP5079230B2 JP2005329815A JP2005329815A JP5079230B2 JP 5079230 B2 JP5079230 B2 JP 5079230B2 JP 2005329815 A JP2005329815 A JP 2005329815A JP 2005329815 A JP2005329815 A JP 2005329815A JP 5079230 B2 JP5079230 B2 JP 5079230B2
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- JP
- Japan
- Prior art keywords
- hydroxide
- zinc oxide
- water
- whisker
- metal oxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 239000002131 composite material Substances 0.000 title claims description 31
- 150000004706 metal oxides Chemical class 0.000 title abstract description 28
- 229910044991 metal oxide Inorganic materials 0.000 title abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims abstract description 39
- 239000002537 cosmetic Substances 0.000 claims abstract description 35
- 229920003169 water-soluble polymer Polymers 0.000 claims abstract description 28
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 27
- 150000003839 salts Chemical class 0.000 claims abstract description 23
- 229920000642 polymer Polymers 0.000 claims abstract description 21
- 238000004519 manufacturing process Methods 0.000 claims abstract description 13
- 238000000034 method Methods 0.000 claims abstract description 10
- 229920002125 Sokalan® Polymers 0.000 claims abstract description 6
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- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 4
- 239000003513 alkali Substances 0.000 claims abstract description 4
- 238000001035 drying Methods 0.000 claims abstract description 4
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 4
- 229920002845 Poly(methacrylic acid) Polymers 0.000 claims abstract description 3
- 238000005406 washing Methods 0.000 claims abstract description 3
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 65
- 239000011787 zinc oxide Substances 0.000 claims description 32
- 239000010419 fine particle Substances 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 238000002360 preparation method Methods 0.000 claims description 16
- 229910021511 zinc hydroxide Inorganic materials 0.000 claims description 14
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- 239000002552 dosage form Substances 0.000 claims description 11
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 7
- 229910052725 zinc Inorganic materials 0.000 claims description 7
- 239000011701 zinc Substances 0.000 claims description 7
- 239000012298 atmosphere Substances 0.000 claims description 3
- 230000001590 oxidative effect Effects 0.000 claims description 3
- 238000010304 firing Methods 0.000 claims description 2
- 150000003751 zinc Chemical class 0.000 claims description 2
- 229910000000 metal hydroxide Inorganic materials 0.000 abstract description 20
- 229910052751 metal Inorganic materials 0.000 abstract description 14
- 239000002184 metal Substances 0.000 abstract description 14
- -1 foodstuffs Substances 0.000 description 29
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- 230000000052 comparative effect Effects 0.000 description 14
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 12
- 235000014113 dietary fatty acids Nutrition 0.000 description 10
- 239000000194 fatty acid Substances 0.000 description 10
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- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 9
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- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 7
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- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 5
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- 239000000203 mixture Substances 0.000 description 5
- 235000011121 sodium hydroxide Nutrition 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 description 4
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 4
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- 239000002585 base Substances 0.000 description 4
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- 238000010586 diagram Methods 0.000 description 4
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- 235000019388 lanolin Nutrition 0.000 description 4
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- 239000012046 mixed solvent Substances 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
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- 239000000049 pigment Substances 0.000 description 4
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- 238000010992 reflux Methods 0.000 description 4
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 4
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- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
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- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
- GHOKWGTUZJEAQD-ZETCQYMHSA-N (D)-(+)-Pantothenic acid Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCC(O)=O GHOKWGTUZJEAQD-ZETCQYMHSA-N 0.000 description 2
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- XIOUDVJTOYVRTB-UHFFFAOYSA-N 1-(1-adamantyl)-3-aminothiourea Chemical compound C1C(C2)CC3CC2CC1(NC(=S)NN)C3 XIOUDVJTOYVRTB-UHFFFAOYSA-N 0.000 description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 2
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 description 2
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 2
- ALYNCZNDIQEVRV-UHFFFAOYSA-N 4-aminobenzoic acid Chemical compound NC1=CC=C(C(O)=O)C=C1 ALYNCZNDIQEVRV-UHFFFAOYSA-N 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- 239000004386 Erythritol Substances 0.000 description 2
- UNXHWFMMPAWVPI-UHFFFAOYSA-N Erythritol Natural products OCC(O)C(O)CO UNXHWFMMPAWVPI-UHFFFAOYSA-N 0.000 description 2
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| JP2005329815A JP5079230B2 (ja) | 2005-11-15 | 2005-11-15 | ウィスカー状の金属酸化物及びその複合体 |
| HK09103784.5A HK1125398B (en) | 2005-11-15 | 2006-06-15 | Organic inorganic composite powder, method of producing the same, and composition containing the powder |
| CN200680050959XA CN101356243B (zh) | 2005-11-15 | 2006-06-15 | 有机无机复合粉末及其制备方法和含有上述粉末的组合物 |
| US12/093,680 US20090162302A1 (en) | 2005-11-15 | 2006-06-15 | Organic inorganic composite powder, method of producing the same, and composition containing the powder |
| PCT/JP2006/312035 WO2007057997A1 (ja) | 2005-11-15 | 2006-06-15 | 有機無機複合粉体、その製造方法、及び前記粉体を含有する組成物 |
| KR1020087014406A KR101243466B1 (ko) | 2005-11-15 | 2006-06-15 | 무기 분체 복합체를 제조하는 방법 |
| EP06766769A EP1950258A4 (en) | 2005-11-15 | 2006-06-15 | ORGANIC-INORGANIC COMPOUND POWDER, METHOD OF MANUFACTURING THEREOF AND COMPOSITION COMPRISING THE POWDER |
| AU2006314025A AU2006314025B2 (en) | 2005-11-15 | 2006-06-15 | Organic inorganic composite powder, method of producing the same and composition containing the powder |
| CA2629646A CA2629646C (en) | 2005-11-15 | 2006-06-15 | Organic inorganic composite powder, method of producing the same, and composition containing the powder |
| TW095122601A TWI357821B (en) | 2005-11-15 | 2006-06-23 | Method of producing organic inorganic composite po |
| US12/701,943 US20100137489A1 (en) | 2005-11-15 | 2010-02-08 | Organic inorganic composite powder, method of producing the same, and composition containing the powder |
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| CN101641077B (zh) * | 2007-03-23 | 2013-01-16 | 巴斯夫欧洲公司 | 生产表面改性的纳米颗粒状金属氧化物、金属氢氧化物和/或金属氧化物氢氧化物的方法 |
| JP5392817B2 (ja) * | 2008-12-24 | 2014-01-22 | ポーラ化成工業株式会社 | 乳化剤形の皮膚外用剤 |
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| JP2821357B2 (ja) * | 1994-02-22 | 1998-11-05 | 株式会社日本触媒 | 酸化亜鉛微粒子の製法 |
| JP3554369B2 (ja) * | 1994-08-19 | 2004-08-18 | 株式会社日本触媒 | 酸化亜鉛−ポリマー複合体微粒子、その製造方法およびその用途 |
| JP3923206B2 (ja) * | 1999-01-29 | 2007-05-30 | 花王株式会社 | 化粧料 |
| JP4045707B2 (ja) * | 1999-12-06 | 2008-02-13 | 日亜化学工業株式会社 | 金属酸化物微粒子の製造方法 |
| US6946513B2 (en) * | 2000-05-09 | 2005-09-20 | Daikin Industries, Ltd. | Polymer composition containing clean filler incorporated therein |
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