JP5068561B2 - 潤滑油組成物 - Google Patents
潤滑油組成物 Download PDFInfo
- Publication number
- JP5068561B2 JP5068561B2 JP2007070414A JP2007070414A JP5068561B2 JP 5068561 B2 JP5068561 B2 JP 5068561B2 JP 2007070414 A JP2007070414 A JP 2007070414A JP 2007070414 A JP2007070414 A JP 2007070414A JP 5068561 B2 JP5068561 B2 JP 5068561B2
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- JP
- Japan
- Prior art keywords
- acid
- mass
- lubricating oil
- molybdenum
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- Prior art date
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- 239000000203 mixture Substances 0.000 title claims description 135
- 239000010687 lubricating oil Substances 0.000 title claims description 112
- 239000002199 base oil Substances 0.000 claims description 138
- 125000004432 carbon atom Chemical group C* 0.000 claims description 117
- 229910052751 metal Inorganic materials 0.000 claims description 105
- 239000002184 metal Substances 0.000 claims description 105
- 125000000217 alkyl group Chemical group 0.000 claims description 100
- 150000003839 salts Chemical class 0.000 claims description 71
- 229910052717 sulfur Inorganic materials 0.000 claims description 62
- 239000003599 detergent Substances 0.000 claims description 59
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 57
- 239000011593 sulfur Substances 0.000 claims description 56
- 229910052799 carbon Inorganic materials 0.000 claims description 48
- 150000002752 molybdenum compounds Chemical class 0.000 claims description 42
- 150000001875 compounds Chemical class 0.000 claims description 41
- 239000005078 molybdenum compound Substances 0.000 claims description 37
- 239000011574 phosphorus Substances 0.000 claims description 32
- 229910052698 phosphorus Inorganic materials 0.000 claims description 32
- 230000001050 lubricating effect Effects 0.000 claims description 26
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 25
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 24
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 22
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 21
- 239000003607 modifier Substances 0.000 claims description 20
- 239000002270 dispersing agent Substances 0.000 claims description 19
- 229910052750 molybdenum Inorganic materials 0.000 claims description 19
- 239000011733 molybdenum Substances 0.000 claims description 19
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 15
- KHYKFSXXGRUKRE-UHFFFAOYSA-J molybdenum(4+) tetracarbamodithioate Chemical compound C(N)([S-])=S.[Mo+4].C(N)([S-])=S.C(N)([S-])=S.C(N)([S-])=S KHYKFSXXGRUKRE-UHFFFAOYSA-J 0.000 claims description 15
- 229910052757 nitrogen Inorganic materials 0.000 claims description 15
- 229910052760 oxygen Inorganic materials 0.000 claims description 15
- 239000001301 oxygen Substances 0.000 claims description 15
- XYRMLECORMNZEY-UHFFFAOYSA-B [Mo+4].[Mo+4].[Mo+4].[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S Chemical compound [Mo+4].[Mo+4].[Mo+4].[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S XYRMLECORMNZEY-UHFFFAOYSA-B 0.000 claims description 12
- 239000003502 gasoline Substances 0.000 claims description 11
- 239000003112 inhibitor Substances 0.000 claims description 11
- 238000002347 injection Methods 0.000 claims description 11
- 239000007924 injection Substances 0.000 claims description 11
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 9
- 125000004429 atom Chemical group 0.000 claims description 9
- 229910052796 boron Inorganic materials 0.000 claims description 9
- 229910019142 PO4 Inorganic materials 0.000 claims description 4
- 239000010452 phosphate Substances 0.000 claims description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 2
- -1 alkali metal borate hydrate Chemical class 0.000 description 162
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 61
- 239000004071 soot Substances 0.000 description 52
- 150000002430 hydrocarbons Chemical group 0.000 description 50
- 239000002253 acid Substances 0.000 description 47
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 43
- 229960004889 salicylic acid Drugs 0.000 description 43
- 238000002156 mixing Methods 0.000 description 42
- 239000002585 base Substances 0.000 description 37
- 239000003921 oil Substances 0.000 description 35
- KZNICNPSHKQLFF-UHFFFAOYSA-N succinimide Chemical class O=C1CCC(=O)N1 KZNICNPSHKQLFF-UHFFFAOYSA-N 0.000 description 30
- 230000003749 cleanliness Effects 0.000 description 29
- 125000003342 alkenyl group Chemical group 0.000 description 28
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 27
- 238000000034 method Methods 0.000 description 27
- 230000000694 effects Effects 0.000 description 24
- 239000000446 fuel Substances 0.000 description 23
- 239000003054 catalyst Substances 0.000 description 22
- 239000007789 gas Substances 0.000 description 22
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 21
- 229910052783 alkali metal Inorganic materials 0.000 description 21
- 125000003118 aryl group Chemical group 0.000 description 20
- 239000003795 chemical substances by application Substances 0.000 description 20
- 229910052739 hydrogen Inorganic materials 0.000 description 19
- 239000001257 hydrogen Substances 0.000 description 19
- 239000001993 wax Substances 0.000 description 19
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 18
- 238000012360 testing method Methods 0.000 description 18
- 239000000470 constituent Substances 0.000 description 16
- 230000003647 oxidation Effects 0.000 description 16
- 238000007254 oxidation reaction Methods 0.000 description 16
- 230000009467 reduction Effects 0.000 description 16
- 229960001860 salicylate Drugs 0.000 description 16
- YGSDEFSMJLZEOE-UHFFFAOYSA-M salicylate Chemical compound OC1=CC=CC=C1C([O-])=O YGSDEFSMJLZEOE-UHFFFAOYSA-M 0.000 description 15
- 239000002904 solvent Substances 0.000 description 15
- 150000005846 sugar alcohols Polymers 0.000 description 15
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 14
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 14
- 150000001340 alkali metals Chemical class 0.000 description 14
- 239000003963 antioxidant agent Substances 0.000 description 14
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 13
- 150000001336 alkenes Chemical class 0.000 description 13
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 13
- 235000010338 boric acid Nutrition 0.000 description 13
- 229960002645 boric acid Drugs 0.000 description 13
- 235000014113 dietary fatty acids Nutrition 0.000 description 13
- 229930195729 fatty acid Natural products 0.000 description 13
- 239000000194 fatty acid Substances 0.000 description 13
- 238000012423 maintenance Methods 0.000 description 13
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 13
- 150000002894 organic compounds Chemical class 0.000 description 13
- 229910052725 zinc Inorganic materials 0.000 description 13
- 239000011701 zinc Substances 0.000 description 13
- 239000004327 boric acid Substances 0.000 description 12
- 238000004517 catalytic hydrocracking Methods 0.000 description 12
- 238000002485 combustion reaction Methods 0.000 description 12
- 150000002148 esters Chemical class 0.000 description 12
- 238000004519 manufacturing process Methods 0.000 description 12
- 229920001083 polybutene Polymers 0.000 description 12
- 229960002317 succinimide Drugs 0.000 description 12
- 239000000654 additive Substances 0.000 description 11
- 230000003078 antioxidant effect Effects 0.000 description 11
- 238000006243 chemical reaction Methods 0.000 description 11
- 239000000460 chlorine Substances 0.000 description 11
- 125000004430 oxygen atom Chemical group O* 0.000 description 11
- 230000002265 prevention Effects 0.000 description 11
- 239000000047 product Substances 0.000 description 11
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 11
- 238000011282 treatment Methods 0.000 description 11
- 150000001342 alkaline earth metals Chemical class 0.000 description 10
- 150000004665 fatty acids Chemical class 0.000 description 10
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 10
- 239000010802 sludge Substances 0.000 description 10
- 125000004434 sulfur atom Chemical group 0.000 description 10
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 9
- 150000001412 amines Chemical class 0.000 description 9
- 229910052801 chlorine Inorganic materials 0.000 description 9
- 238000001704 evaporation Methods 0.000 description 9
- 230000008020 evaporation Effects 0.000 description 9
- 229920000768 polyamine Polymers 0.000 description 9
- 230000001603 reducing effect Effects 0.000 description 9
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 8
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 8
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 8
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 8
- 239000011575 calcium Substances 0.000 description 8
- 229910052791 calcium Inorganic materials 0.000 description 8
- 150000002751 molybdenum Chemical class 0.000 description 8
- VLAPMBHFAWRUQP-UHFFFAOYSA-L molybdic acid Chemical compound O[Mo](O)(=O)=O VLAPMBHFAWRUQP-UHFFFAOYSA-L 0.000 description 8
- 239000010705 motor oil Substances 0.000 description 8
- 230000007935 neutral effect Effects 0.000 description 8
- 125000004433 nitrogen atom Chemical group N* 0.000 description 8
- 150000007519 polyprotic acids Polymers 0.000 description 8
- 239000000126 substance Substances 0.000 description 8
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 7
- VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical group CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 description 7
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 7
- 230000000996 additive effect Effects 0.000 description 7
- 150000001298 alcohols Chemical class 0.000 description 7
- 238000009835 boiling Methods 0.000 description 7
- 239000006229 carbon black Substances 0.000 description 7
- 230000003197 catalytic effect Effects 0.000 description 7
- 238000004821 distillation Methods 0.000 description 7
- 150000004678 hydrides Chemical class 0.000 description 7
- 239000011630 iodine Substances 0.000 description 7
- 229910052740 iodine Inorganic materials 0.000 description 7
- 150000007524 organic acids Chemical class 0.000 description 7
- 150000003568 thioethers Chemical class 0.000 description 7
- 239000004711 α-olefin Substances 0.000 description 7
- VXNZUUAINFGPBY-UHFFFAOYSA-N 1-Butene Chemical compound CCC=C VXNZUUAINFGPBY-UHFFFAOYSA-N 0.000 description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 6
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 239000002202 Polyethylene glycol Substances 0.000 description 6
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 6
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 6
- 125000001931 aliphatic group Chemical group 0.000 description 6
- WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical compound FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 description 6
- 150000005690 diesters Chemical class 0.000 description 6
- 150000002431 hydrogen Chemical class 0.000 description 6
- 239000011777 magnesium Substances 0.000 description 6
- 229910052749 magnesium Inorganic materials 0.000 description 6
- JKQOBWVOAYFWKG-UHFFFAOYSA-N molybdenum trioxide Chemical compound O=[Mo](=O)=O JKQOBWVOAYFWKG-UHFFFAOYSA-N 0.000 description 6
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 6
- 229910017464 nitrogen compound Inorganic materials 0.000 description 6
- 150000002830 nitrogen compounds Chemical class 0.000 description 6
- 229920001223 polyethylene glycol Polymers 0.000 description 6
- 238000000746 purification Methods 0.000 description 6
- KWKAKUADMBZCLK-UHFFFAOYSA-N 1-octene Chemical compound CCCCCCC=C KWKAKUADMBZCLK-UHFFFAOYSA-N 0.000 description 5
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 5
- 150000007513 acids Chemical class 0.000 description 5
- 239000002518 antifoaming agent Substances 0.000 description 5
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 5
- 150000001639 boron compounds Chemical class 0.000 description 5
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 5
- 229920001577 copolymer Polymers 0.000 description 5
- 239000010779 crude oil Substances 0.000 description 5
- 239000002480 mineral oil Substances 0.000 description 5
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 5
- 125000005702 oxyalkylene group Chemical group 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- 229960005137 succinic acid Drugs 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 229910001868 water Inorganic materials 0.000 description 5
- AFFLGGQVNFXPEV-UHFFFAOYSA-N 1-decene Chemical compound CCCCCCCCC=C AFFLGGQVNFXPEV-UHFFFAOYSA-N 0.000 description 4
- CRSBERNSMYQZNG-UHFFFAOYSA-N 1-dodecene Chemical compound CCCCCCCCCCC=C CRSBERNSMYQZNG-UHFFFAOYSA-N 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- 229910015900 BF3 Inorganic materials 0.000 description 4
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 description 4
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 4
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 4
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 4
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 4
- REYJJPSVUYRZGE-UHFFFAOYSA-N Octadecylamine Chemical compound CCCCCCCCCCCCCCCCCCN REYJJPSVUYRZGE-UHFFFAOYSA-N 0.000 description 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 4
- 229920002367 Polyisobutene Polymers 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 4
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 description 4
- 125000005037 alkyl phenyl group Chemical group 0.000 description 4
- 125000002947 alkylene group Chemical group 0.000 description 4
- 125000003277 amino group Chemical group 0.000 description 4
- 239000004202 carbamide Substances 0.000 description 4
- 239000001569 carbon dioxide Substances 0.000 description 4
- 229910002092 carbon dioxide Inorganic materials 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 4
- 238000005260 corrosion Methods 0.000 description 4
- 239000010710 diesel engine oil Substances 0.000 description 4
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 4
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 4
- NAGJZTKCGNOGPW-UHFFFAOYSA-N dithiophosphoric acid Chemical compound OP(O)(S)=S NAGJZTKCGNOGPW-UHFFFAOYSA-N 0.000 description 4
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 239000011737 fluorine Substances 0.000 description 4
- 229910052731 fluorine Inorganic materials 0.000 description 4
- 235000011187 glycerol Nutrition 0.000 description 4
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 4
- 125000001183 hydrocarbyl group Chemical group 0.000 description 4
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 4
- 125000004356 hydroxy functional group Chemical group O* 0.000 description 4
- 229910052500 inorganic mineral Inorganic materials 0.000 description 4
- 239000011707 mineral Substances 0.000 description 4
- 235000010755 mineral Nutrition 0.000 description 4
- 235000010446 mineral oil Nutrition 0.000 description 4
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 description 4
- ISYWECDDZWTKFF-UHFFFAOYSA-N nonadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCCC(O)=O ISYWECDDZWTKFF-UHFFFAOYSA-N 0.000 description 4
- FBUKVWPVBMHYJY-UHFFFAOYSA-N nonanoic acid Chemical compound CCCCCCCCC(O)=O FBUKVWPVBMHYJY-UHFFFAOYSA-N 0.000 description 4
- 125000002524 organometallic group Chemical group 0.000 description 4
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 4
- 150000003018 phosphorus compounds Chemical class 0.000 description 4
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 4
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- 230000008569 process Effects 0.000 description 4
- CYIDZMCFTVVTJO-UHFFFAOYSA-N pyromellitic acid Chemical compound OC(=O)C1=CC(C(O)=O)=C(C(O)=O)C=C1C(O)=O CYIDZMCFTVVTJO-UHFFFAOYSA-N 0.000 description 4
- 238000007670 refining Methods 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
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- PTISTKLWEJDJID-UHFFFAOYSA-N sulfanylidenemolybdenum Chemical class [Mo]=S PTISTKLWEJDJID-UHFFFAOYSA-N 0.000 description 4
- SZHOJFHSIKHZHA-UHFFFAOYSA-N tridecanoic acid Chemical compound CCCCCCCCCCCCC(O)=O SZHOJFHSIKHZHA-UHFFFAOYSA-N 0.000 description 4
- ARCGXLSVLAOJQL-UHFFFAOYSA-N trimellitic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1 ARCGXLSVLAOJQL-UHFFFAOYSA-N 0.000 description 4
- ZDPHROOEEOARMN-UHFFFAOYSA-N undecanoic acid Chemical compound CCCCCCCCCCC(O)=O ZDPHROOEEOARMN-UHFFFAOYSA-N 0.000 description 4
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N valeric acid Chemical compound CCCCC(O)=O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 description 4
- JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical compound OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 description 3
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 3
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 3
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
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- 239000004332 silver Substances 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- NVIFVTYDZMXWGX-UHFFFAOYSA-N sodium metaborate Chemical compound [Na+].[O-]B=O NVIFVTYDZMXWGX-UHFFFAOYSA-N 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000004328 sodium tetraborate Substances 0.000 description 1
- 239000001593 sorbitan monooleate Substances 0.000 description 1
- 235000011069 sorbitan monooleate Nutrition 0.000 description 1
- 229940035049 sorbitan monooleate Drugs 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 235000000346 sugar Nutrition 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 150000003463 sulfur Chemical class 0.000 description 1
- XTQHKBHJIVJGKJ-UHFFFAOYSA-N sulfur monoxide Chemical compound S=O XTQHKBHJIVJGKJ-UHFFFAOYSA-N 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- HIFJUMGIHIZEPX-UHFFFAOYSA-N sulfuric acid;sulfur trioxide Chemical compound O=S(=O)=O.OS(O)(=O)=O HIFJUMGIHIZEPX-UHFFFAOYSA-N 0.000 description 1
- 229910052714 tellurium Inorganic materials 0.000 description 1
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 description 1
- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 description 1
- QZZGJDVWLFXDLK-UHFFFAOYSA-N tetracosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCCCC(O)=O QZZGJDVWLFXDLK-UHFFFAOYSA-N 0.000 description 1
- KXTZPAQXYKUVLD-UHFFFAOYSA-N tetradecanehydrazide Chemical compound CCCCCCCCCCCCCC(=O)NN KXTZPAQXYKUVLD-UHFFFAOYSA-N 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- IBYFOBGPNPINBU-UHFFFAOYSA-N tetradecenoic acid Natural products CCCCCCCCCCCC=CC(O)=O IBYFOBGPNPINBU-UHFFFAOYSA-N 0.000 description 1
- IPOBMWQSKXACEW-UHFFFAOYSA-N tetradecylurea Chemical compound CCCCCCCCCCCCCCNC(N)=O IPOBMWQSKXACEW-UHFFFAOYSA-N 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- DPUZPWAFXJXHBN-UHFFFAOYSA-N tetrasodium dioxidoboranyloxy(dioxido)borane Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]B([O-])OB([O-])[O-] DPUZPWAFXJXHBN-UHFFFAOYSA-N 0.000 description 1
- JJJPTTANZGDADF-UHFFFAOYSA-N thiadiazole-4-thiol Chemical compound SC1=CSN=N1 JJJPTTANZGDADF-UHFFFAOYSA-N 0.000 description 1
- YUKQRDCYNOVPGJ-UHFFFAOYSA-N thioacetamide Chemical compound CC(N)=S YUKQRDCYNOVPGJ-UHFFFAOYSA-N 0.000 description 1
- DLFVBJFMPXGRIB-UHFFFAOYSA-N thioacetamide Natural products CC(N)=O DLFVBJFMPXGRIB-UHFFFAOYSA-N 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
- WXBXVVIUZANZAU-CMDGGOBGSA-N trans-2-decenoic acid Chemical compound CCCCCCC\C=C\C(O)=O WXBXVVIUZANZAU-CMDGGOBGSA-N 0.000 description 1
- HSBSUGYTMJWPAX-HNQUOIGGSA-N trans-2-hexenedioic acid Chemical compound OC(=O)CC\C=C\C(O)=O HSBSUGYTMJWPAX-HNQUOIGGSA-N 0.000 description 1
- HOGWBMWOBRRKCD-BUHFOSPRSA-N trans-2-pentadecenoic acid Chemical compound CCCCCCCCCCCC\C=C\C(O)=O HOGWBMWOBRRKCD-BUHFOSPRSA-N 0.000 description 1
- IBYFOBGPNPINBU-OUKQBFOZSA-N trans-2-tetradecenoic acid Chemical compound CCCCCCCCCCC\C=C\C(O)=O IBYFOBGPNPINBU-OUKQBFOZSA-N 0.000 description 1
- HSBSUGYTMJWPAX-UHFFFAOYSA-N trans-Deltaalpha-Dihydromuconsaeure Natural products OC(=O)CCC=CC(O)=O HSBSUGYTMJWPAX-UHFFFAOYSA-N 0.000 description 1
- LKOVPWSSZFDYPG-WUKNDPDISA-N trans-octadec-2-enoic acid Chemical compound CCCCCCCCCCCCCCC\C=C\C(O)=O LKOVPWSSZFDYPG-WUKNDPDISA-N 0.000 description 1
- YIYBQIKDCADOSF-ONEGZZNKSA-N trans-pent-2-enoic acid Chemical compound CC\C=C\C(O)=O YIYBQIKDCADOSF-ONEGZZNKSA-N 0.000 description 1
- LGQXXHMEBUOXRP-UHFFFAOYSA-N tributyl borate Chemical compound CCCCOB(OCCCC)OCCCC LGQXXHMEBUOXRP-UHFFFAOYSA-N 0.000 description 1
- ZCLIWYZDWIIUSS-UHFFFAOYSA-N tricalcium boric acid diborate Chemical compound B([O-])([O-])[O-].B(O)(O)O.B(O)(O)O.B([O-])([O-])[O-].[Ca+2].[Ca+2].[Ca+2] ZCLIWYZDWIIUSS-UHFFFAOYSA-N 0.000 description 1
- VLCLHFYFMCKBRP-UHFFFAOYSA-N tricalcium;diborate Chemical class [Ca+2].[Ca+2].[Ca+2].[O-]B([O-])[O-].[O-]B([O-])[O-] VLCLHFYFMCKBRP-UHFFFAOYSA-N 0.000 description 1
- 150000003628 tricarboxylic acids Chemical class 0.000 description 1
- 125000002469 tricosyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- DXNCZXXFRKPEPY-UHFFFAOYSA-N tridecanedioic acid Chemical compound OC(=O)CCCCCCCCCCCC(O)=O DXNCZXXFRKPEPY-UHFFFAOYSA-N 0.000 description 1
- MCSPQTFLIAPWRZ-UHFFFAOYSA-N tridecanehydrazide Chemical compound CCCCCCCCCCCCC(=O)NN MCSPQTFLIAPWRZ-UHFFFAOYSA-N 0.000 description 1
- VIFASLUWVPBABR-UHFFFAOYSA-N tridecylurea Chemical compound CCCCCCCCCCCCCNC(N)=O VIFASLUWVPBABR-UHFFFAOYSA-N 0.000 description 1
- AJSTXXYNEIHPMD-UHFFFAOYSA-N triethyl borate Chemical compound CCOB(OCC)OCC AJSTXXYNEIHPMD-UHFFFAOYSA-N 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- RIUWBIIVUYSTCN-UHFFFAOYSA-N trilithium borate Chemical compound [Li+].[Li+].[Li+].[O-]B([O-])[O-] RIUWBIIVUYSTCN-UHFFFAOYSA-N 0.000 description 1
- UKUWOJWHPCYQDY-UHFFFAOYSA-N trimagnesium boric acid diborate Chemical compound [Mg+2].[Mg+2].[Mg+2].OB(O)O.OB(O)O.[O-]B([O-])[O-].[O-]B([O-])[O-] UKUWOJWHPCYQDY-UHFFFAOYSA-N 0.000 description 1
- NFMWFGXCDDYTEG-UHFFFAOYSA-N trimagnesium;diborate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]B([O-])[O-].[O-]B([O-])[O-] NFMWFGXCDDYTEG-UHFFFAOYSA-N 0.000 description 1
- WRECIMRULFAWHA-UHFFFAOYSA-N trimethyl borate Chemical compound COB(OC)OC WRECIMRULFAWHA-UHFFFAOYSA-N 0.000 description 1
- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- WUUHFRRPHJEEKV-UHFFFAOYSA-N tripotassium borate Chemical class [K+].[K+].[K+].[O-]B([O-])[O-] WUUHFRRPHJEEKV-UHFFFAOYSA-N 0.000 description 1
- LTEHWCSSIHAVOQ-UHFFFAOYSA-N tripropyl borate Chemical compound CCCOB(OCCC)OCCC LTEHWCSSIHAVOQ-UHFFFAOYSA-N 0.000 description 1
- WMYJOZQKDZZHAC-UHFFFAOYSA-H trizinc;dioxido-sulfanylidene-sulfido-$l^{5}-phosphane Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([S-])=S.[O-]P([O-])([S-])=S WMYJOZQKDZZHAC-UHFFFAOYSA-H 0.000 description 1
- 239000010723 turbine oil Substances 0.000 description 1
- QFKMMXYLAPZKIB-UHFFFAOYSA-N undecan-1-amine Chemical compound CCCCCCCCCCCN QFKMMXYLAPZKIB-UHFFFAOYSA-N 0.000 description 1
- KJIOQYGWTQBHNH-UHFFFAOYSA-N undecanol Chemical compound CCCCCCCCCCCO KJIOQYGWTQBHNH-UHFFFAOYSA-N 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000003672 ureas Chemical class 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
- 229940005605 valeric acid Drugs 0.000 description 1
- 239000003981 vehicle Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 239000012991 xanthate Substances 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
- JQBWIGPYQPOAJZ-UHFFFAOYSA-L zinc;2-ethylhexyl phosphate Chemical compound [Zn+2].CCCCC(CC)COP([O-])([O-])=O JQBWIGPYQPOAJZ-UHFFFAOYSA-L 0.000 description 1
- JLQRJCDABIESLT-UHFFFAOYSA-L zinc;dibutyl phosphate Chemical compound [Zn+2].CCCCOP([O-])(=O)OCCCC.CCCCOP([O-])(=O)OCCCC JLQRJCDABIESLT-UHFFFAOYSA-L 0.000 description 1
- MBBWTVUFIXOUBE-UHFFFAOYSA-L zinc;dicarbamodithioate Chemical class [Zn+2].NC([S-])=S.NC([S-])=S MBBWTVUFIXOUBE-UHFFFAOYSA-L 0.000 description 1
Landscapes
- Lubricants (AREA)
Description
本発明の潤滑油組成物(以下、本発明の組成物ともいう。)における潤滑油基油には、%CPが70以上、%CAが1以下、粘度指数115以上、−35℃におけるCCS粘度が3000mPa・s以下である基油(X)が含有される。このような基油(X)としては、上記数値範囲内にあれば、鉱油系基油及び合成系基油のいずれも使用することができる。
(1)パラフィン基系原油及び/又は混合基系原油の常圧蒸留による留出油
(2)パラフィン基系原油及び/又は混合基系原油の常圧蒸留残渣油の減圧蒸留による留出油(WVGO)
(3)潤滑油脱ろう工程により得られるワックス(スラックワックス、スラックワックスをさらに脱油・精製したワックス等)及び/又はガストゥリキッド(GTL)プロセス等により得られる合成ワックス(フィッシャートロプシュワックス、GTLワックス等)
(4)基油(1)〜(3)から選ばれる1種又は2種以上の混合油及び/又は当該混合油のマイルドハイドロクラッキング処理油
(5)基油(1)〜(4)から選ばれる2種以上の混合油
(6)基油(1)、(2)、(3)、(4)又は(5)の脱れき油(DAO)
(7)基油(6)のマイルドハイドロクラッキング処理油(MHC)
(8)基油(1)〜(7)から選ばれる2種以上の混合油
(9)上記基油(1)〜(8)から選ばれる基油又は当該基油から回収された潤滑油留分を水素化分解し、その生成物又はその生成物から蒸留等により回収される潤滑油留分について溶剤脱ろうや接触脱ろうなどの脱ろう処理を行い、又は当該脱ろう処理をした後に蒸留することによって得られる水素化分解鉱油
(10)上記基油(1)〜(8)から選ばれる基油又は当該基油から回収された潤滑油留分を水素化異性化し、その生成物又はその生成物から蒸留等により回収される潤滑油留分について溶剤脱ろうや接触脱ろうなどの脱ろう処理を行い、又は、当該脱ろう処理をしたあとに蒸留することによって得られる水素化異性化鉱油
(Y1)−35℃におけるCCS粘度が3000mPa・sを超える基油(例えば、−35℃におけるCCS粘度が3000mPa・sを超える基油、好ましくは100000mPa・s以下、より好ましくは3500〜15000mPa・sの基油)
(Y2)%CPが70未満の基油(例えば、%CPが50〜70未満、好ましくは60〜70未満の基油)、
(Y3)%CAが1を越える基油(例えば、%CAが1を越え20以下、好ましくは10以下、さらに好ましくは3以下の基油)、
(Y4)粘度指数120未満の基油(例えば、粘度指数が好ましくは80〜120未満の基油)、及び
(Y5)基油(X)の規定のいずれか2つ以上の規定を満たさない基油、
から選ばれる。
(B1)炭素数3〜8から選ばれる2級アルキル基を有するジアルキルジチオリン酸亜鉛
(B2)炭素数3〜8から選ばれる1級アルキル基を有するジアルキルジチオリン酸亜鉛
(B3)硫黄を含有しないリン含有酸の金属塩
すす混入油を模擬的に調製するために、試験油にカーボンブラックを1.5質量%分散させ、JPI−5S−32−90に準拠して以下の試験条件で四球摩耗試験を行い、試験後の摩耗痕径を測定した。本試験においては、摩耗痕径が小さいものほど耐摩耗性に優れていることを意味する。
(試験条件)
回転数:1500rpm
荷重:294N
試験油温:110℃
試験時間:1時間
新油及びカーボンブラックを1.5質量%分散させた油を試験油とし、HFRR摩擦試験機を用いて以下の条件にて摩擦係数を測定した。得られた結果を表1に記載した。本試験においては、摩擦係数が小さいものほど省燃費性に優れていることを意味し、カーボンブラック添加後の摩擦係数が小さいものほど摩擦低減効果の維持性に優れることを意味する。
(試験条件)
錘:200g
試験油温:100℃
振幅:1mm
振動数:50Hz
試験時間:1時間
摩擦係数測定:試験開始後50分〜60分後までの摩擦係数を平均した。
JPI−5S−5599に準拠し、ホットチューブ試験を行った。評点は無色透明(汚れ無)を10点、黒色不透明を0点とし、この間をあらかじめ1刻みで作成した標準チューブを参照して評価した。
Claims (10)
- %CPが70以上、%CAが1以下、粘度指数115以上、−35℃におけるCCS粘度が3000mPa・s以下である基油(X)を含有する潤滑油基油に、組成物全量基準で、
(A)無灰摩擦調整剤を0.01〜10質量%、
(B)リン含有摩耗防止剤をリン量として0.01〜0.2質量%、
(C)金属系清浄剤を金属量として0.01〜1質量%、及び
(D)ホウ素含有量と窒素含有量とのB/N質量比が0.1〜0.4である、重量平均分子量が3000〜20000の無灰分散剤を窒素量として0.01〜0.4質量%
含有することを特徴とする潤滑油組成物。 - 前記基油(X)が、100℃における動粘度が3.5mm2/s以上、−35℃におけるCCS粘度が2000mPa・s以下であることを特徴とする請求項1に記載の潤滑油組成物。
- 前記潤滑油基油が、さらに、−35℃におけるCCS粘度が3000mPa・sを超え、粘度指数が80以上、%CPが60以上、%CAが10以下、100℃動粘度が5mm2/s以上である基油(Ya)を含有することを特徴とする請求項1又は2に記載の潤滑油組成物。
- 前記(A)成分が、窒素、酸素、硫黄から選ばれる1種又は2種以上の元素を少なくとも3原子以上含有する化合物であることを特徴とする請求項1〜3のいずれかの項に記載の潤滑油組成物。
- 前記(D)成分が、(D1)重量平均分子量が6500以上の無灰分散剤及び/又は(D2)重量平均分子量が3000以上でありホウ素を含有する無灰分散剤を含有することを特徴とする請求項1〜4のいずれかの項に記載の潤滑油組成物。
- モリブデンジチオカーバメート及びモリブデンジチオホスフェート以外の有機モリブデン化合物(E2)を、組成物全量基準で、モリブデン量として0.001〜0.2質量%含有する請求項1〜5のいずれかの項に記載の潤滑油組成物。
- ディーゼルエンジン用又は直噴ガソリンエンジン用であることを特徴とする請求項1〜6のいずれかの項に記載の潤滑油組成物。
- 前記(C)金属系清浄剤として、金属比が6以上のスルホネート系金属系清浄剤を含有する、請求項1〜7のいずれかの項に記載の潤滑油組成物。
- 前記(A)無灰摩擦調整剤が、アミド結合を有する化合物である、請求項1〜8のいずれかの項に記載の潤滑油組成物。
- 前記(B)リン含有摩耗防止剤として、
炭素数6〜8のアルキル基を1つ又は2つ有するモノ及び/又はジアルキルリン酸エステル金属塩
を含有する、請求項1〜9のいずれかの項に記載の潤滑油組成物。
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JP5483662B2 (ja) | 2008-01-15 | 2014-05-07 | Jx日鉱日石エネルギー株式会社 | 潤滑油組成物 |
JP2010090251A (ja) | 2008-10-07 | 2010-04-22 | Nippon Oil Corp | 潤滑油基油及びその製造方法、潤滑油組成物 |
JP5806796B2 (ja) * | 2008-10-07 | 2015-11-10 | Jx日鉱日石エネルギー株式会社 | 内燃機関用潤滑油組成物及びその製造方法 |
EP2497819B1 (en) | 2008-10-07 | 2017-01-04 | JX Nippon Oil & Energy Corporation | Lubricant composition |
EP2581437B2 (en) | 2008-10-07 | 2019-05-01 | JX Nippon Oil & Energy Corporation | Process for producing lubricant base oil and lubricating oil composition |
JP5502356B2 (ja) * | 2009-03-27 | 2014-05-28 | 出光興産株式会社 | ギヤ油組成物 |
CN105695045A (zh) | 2009-06-04 | 2016-06-22 | 吉坤日矿日石能源株式会社 | 润滑油组合物 |
CN103275800B (zh) | 2009-06-04 | 2016-06-22 | 吉坤日矿日石能源株式会社 | 润滑油组合物 |
EP2439257A4 (en) | 2009-06-04 | 2012-11-28 | Jx Nippon Oil & Energy Corp | LUBRICATING OIL COMPOSITION AND MANUFACTURING METHOD THEREFOR |
JP5689592B2 (ja) | 2009-09-01 | 2015-03-25 | Jx日鉱日石エネルギー株式会社 | 潤滑油組成物 |
JP6151914B2 (ja) * | 2010-04-02 | 2017-06-21 | 出光興産株式会社 | 内燃機関用潤滑油組成物 |
KR101771764B1 (ko) | 2010-04-02 | 2017-08-25 | 이데미쓰 고산 가부시키가이샤 | 내연 기관용 윤활유 조성물 |
KR20130103652A (ko) * | 2010-04-02 | 2013-09-24 | 이데미쓰 고산 가부시키가이샤 | 내연 기관용 윤활유 조성물 |
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JPWO2017188087A1 (ja) * | 2016-04-25 | 2019-02-28 | コスモ石油ルブリカンツ株式会社 | 内燃機関用潤滑油組成物 |
JP6864461B2 (ja) * | 2016-11-04 | 2021-04-28 | Emgルブリカンツ合同会社 | 潤滑油組成物 |
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