JP5002418B2 - リーク監視装置 - Google Patents
リーク監視装置 Download PDFInfo
- Publication number
- JP5002418B2 JP5002418B2 JP2007285961A JP2007285961A JP5002418B2 JP 5002418 B2 JP5002418 B2 JP 5002418B2 JP 2007285961 A JP2007285961 A JP 2007285961A JP 2007285961 A JP2007285961 A JP 2007285961A JP 5002418 B2 JP5002418 B2 JP 5002418B2
- Authority
- JP
- Japan
- Prior art keywords
- exchange resin
- cation exchange
- hardness
- leak monitoring
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000012806 monitoring device Methods 0.000 title claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 53
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 47
- 239000003729 cation exchange resin Substances 0.000 claims description 47
- 239000003795 chemical substances by application Substances 0.000 claims description 30
- 239000003513 alkali Substances 0.000 claims description 21
- 238000012544 monitoring process Methods 0.000 claims description 20
- 239000010419 fine particle Substances 0.000 claims description 4
- 150000001768 cations Chemical class 0.000 claims description 3
- 230000001376 precipitating effect Effects 0.000 claims description 2
- 238000011144 upstream manufacturing Methods 0.000 claims 1
- 239000012528 membrane Substances 0.000 description 39
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 30
- 238000002242 deionisation method Methods 0.000 description 12
- 238000001223 reverse osmosis Methods 0.000 description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
- 230000002378 acidificating effect Effects 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 150000002500 ions Chemical class 0.000 description 5
- 238000012423 maintenance Methods 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000003957 anion exchange resin Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 238000010979 pH adjustment Methods 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 230000001172 regenerating effect Effects 0.000 description 3
- 230000008929 regeneration Effects 0.000 description 3
- 238000011069 regeneration method Methods 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 239000003011 anion exchange membrane Substances 0.000 description 2
- 238000005341 cation exchange Methods 0.000 description 2
- 238000007872 degassing Methods 0.000 description 2
- 238000005115 demineralization Methods 0.000 description 2
- 230000002328 demineralizing effect Effects 0.000 description 2
- 239000008235 industrial water Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- -1 polypropylene Polymers 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000002349 well water Substances 0.000 description 2
- 235000020681 well water Nutrition 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 239000004695 Polyether sulfone Substances 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000004760 aramid Substances 0.000 description 1
- 229920003235 aromatic polyamide Polymers 0.000 description 1
- RQPZNWPYLFFXCP-UHFFFAOYSA-L barium dihydroxide Chemical compound [OH-].[OH-].[Ba+2] RQPZNWPYLFFXCP-UHFFFAOYSA-L 0.000 description 1
- 229910001863 barium hydroxide Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229920002301 cellulose acetate Polymers 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000010612 desalination reaction Methods 0.000 description 1
- 238000011033 desalting Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012510 hollow fiber Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 239000003014 ion exchange membrane Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000001471 micro-filtration Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920000515 polycarbonate Polymers 0.000 description 1
- 239000004417 polycarbonate Substances 0.000 description 1
- 229920006393 polyether sulfone Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 1
- 238000000108 ultra-filtration Methods 0.000 description 1
Images
Landscapes
- Separation Using Semi-Permeable Membranes (AREA)
- Treatment Of Water By Ion Exchange (AREA)
Description
Ca2++HCO3 −⇔H++CaCO3↓・・・(1)
図4の経路Aに示すように、この実施例の装置は、被処理水の流れに沿って順に、カチオン交換樹脂装置と、リーク監視装置として膜式除濁手段、アルカリ剤添加手段及び計測手段を備えている。アルカリ剤添加手段で用いたアルカリ剤は、NaOHである。アルカリ剤添加手段で膜式除濁手段の処理水のpHを11〜11.5に調整し、各機器のメンテナンス時を除く20時間の連続運転を行った。
カチオン交換樹脂装置で使用したカチオン交換樹脂:デュオライトC−20(Na型強酸性カチオン交換樹脂、ローム&ハース社製),充填樹脂量7L,通水流量200L/hr、
膜式除濁手段で使用した除濁フィルター:QTEC0.1μm 20IN−NPC BUNA(Graver Technologies社製)、
計測手段:低濃度濁度計(1720E、HACH社製),通水流量0.2L/min、
実施例1においてアルカリ剤としてNaOHを添加せずに、図4の経路Bに示す通水経路で連続運転を行う以外は、実施例1と同様にして行った。結果を表1に示す。
Claims (2)
- カチオン交換樹脂装置の後段に配置して該装置からの硬度成分のリークを監視するリーク監視装置であって、
前記カチオン交換樹脂装置の処理水に、2価以上のカチオンを実質的に含まないアルカリ剤を添加し、該処理水のpHを9以上、13以下に調整して前記処理水に含まれる硬度成分を硬度スケールとして析出させるアルカリ剤添加手段と、
前記硬度スケールの濃度を計測する濁度計もしくは微粒子カウンターからなる計測手段と、
を備えることを特徴とするリーク監視装置。 - 前記アルカリ剤添加手段の前段に、膜式除濁手段をさらに備えることを特徴とする請求項1に記載のリーク監視装置。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2007285961A JP5002418B2 (ja) | 2007-11-02 | 2007-11-02 | リーク監視装置 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2007285961A JP5002418B2 (ja) | 2007-11-02 | 2007-11-02 | リーク監視装置 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2009112894A JP2009112894A (ja) | 2009-05-28 |
JP5002418B2 true JP5002418B2 (ja) | 2012-08-15 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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JP2007285961A Active JP5002418B2 (ja) | 2007-11-02 | 2007-11-02 | リーク監視装置 |
Country Status (1)
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JP (1) | JP5002418B2 (ja) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5862167B2 (ja) * | 2011-09-30 | 2016-02-16 | 栗田工業株式会社 | 閉鎖系空間用の水回収装置 |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH01218680A (ja) * | 1988-02-25 | 1989-08-31 | Nomura Micro Sci Kk | イオン交換装置のブレーク監視方法 |
JP2696533B2 (ja) * | 1988-09-19 | 1998-01-14 | 三浦工業株式会社 | 硬度指示薬 |
JPH0592198A (ja) * | 1991-06-18 | 1993-04-16 | Naizu Saat:Kk | 硬水の軟化処理方法 |
JPH10216718A (ja) * | 1997-02-12 | 1998-08-18 | Kurita Water Ind Ltd | 復水脱塩方法 |
JPH10244266A (ja) * | 1997-03-05 | 1998-09-14 | Kinousui Kenkyusho:Kk | 配管内液体の電場処理装置 |
JPH1128482A (ja) * | 1997-07-11 | 1999-02-02 | Kurita Water Ind Ltd | 純水製造方法 |
JP2000126764A (ja) * | 1998-10-28 | 2000-05-09 | Samson Co Ltd | 硬度リークの予知検出を行う硬水軟化装置 |
JP2001340850A (ja) * | 2000-05-31 | 2001-12-11 | Miura Co Ltd | 軟水装置並びに軟水装置におけるイオン交換樹脂の劣化度合判定方法および軟水装置の制御方法 |
JP2002192152A (ja) * | 2000-12-25 | 2002-07-10 | Nomura Micro Sci Co Ltd | 水処理方法および水処理装置 |
JP4120606B2 (ja) * | 2004-03-30 | 2008-07-16 | 三浦工業株式会社 | 硬度測定用試薬 |
JP4222327B2 (ja) * | 2004-03-30 | 2009-02-12 | 三浦工業株式会社 | 硬度測定用試薬 |
JP2007155371A (ja) * | 2005-12-01 | 2007-06-21 | Miura Co Ltd | 光学計測装置 |
JP2007155372A (ja) * | 2005-12-01 | 2007-06-21 | Miura Co Ltd | 光学計測装置 |
JP5224041B2 (ja) * | 2007-06-27 | 2013-07-03 | ダイキン工業株式会社 | ヒートポンプ式給湯装置 |
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- 2007-11-02 JP JP2007285961A patent/JP5002418B2/ja active Active
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