JP4767000B2 - Vacuum deposition equipment - Google Patents

Vacuum deposition equipment Download PDF

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JP4767000B2
JP4767000B2 JP2005341304A JP2005341304A JP4767000B2 JP 4767000 B2 JP4767000 B2 JP 4767000B2 JP 2005341304 A JP2005341304 A JP 2005341304A JP 2005341304 A JP2005341304 A JP 2005341304A JP 4767000 B2 JP4767000 B2 JP 4767000B2
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JP2007146219A (en
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祐司 松本
和人 鈴木
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Hitachi Zosen Corp
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a vacuum vapor deposition apparatus capable of performing the vapor deposition of a plurality of dissimilar materials on a member for vapor deposition at a uniform component ratio by moving at least one of the member for vapor deposition and an evaporation source straight. <P>SOLUTION: The vacuum vapor deposition apparatus is provided with: an evaporation device 12 for heating and vaporizing first and second dissimilar vapor deposition materials; a glass substrate 13 for performing the vapor deposition of the first and second evaporation material vaporized from the evaporation device 12 in a vacuum vapor deposition container 11; and a substrate holding and moving device for moving the glass substrate 13 in the x direction. The evaporation device 12 has nozzle sets 25A, 25B arranging a first nozzle cylinder 25a and a second nozzle cylinder 25b close to each other which emit the first and second evaporation materials toward the glass substrate 13 after diffusing the first and second evaporation materials introduced from the evaporation units 21A, 21B by first and second diffusion containers 23A, 23B, and the nozzle sets 25A, 25B are arranged in line in the crossing direction orthogonal to the moving direction of the glass substrate 13. <P>COPYRIGHT: (C)2007,JPO&amp;INPIT

Description

本発明は、被蒸着部材と蒸発装置の少なくとも一方を直線方向に移動させつつ、蒸発装置で加熱されて気化された複数の異種材料を被蒸着部材に蒸着する真空蒸着装置に関する。   The present invention relates to a vacuum deposition apparatus that deposits a plurality of different materials heated and vaporized by an evaporation apparatus on the deposition member while moving at least one of the deposition target member and the evaporation apparatus in a linear direction.

従来、被蒸着部材である基板を直線方向に移動させつつ、移動方向と直交するライン方向に沿って配置された開口から材料を放出させて蒸着し、有機ELディスプレイを製造する成膜装置がたとえば特許文献1に開示されている。   2. Description of the Related Art Conventionally, a film forming apparatus that manufactures an organic EL display by moving a substrate, which is a member to be deposited, in a linear direction, discharging a material from an opening arranged along a line direction orthogonal to the moving direction, and depositing the material. It is disclosed in Patent Document 1.

上記有機ELディスプレイの基本構造は、ガラス基板上に配置された陽極(透明電極)上に、ホール輸送層、発光層、陰極が順次配置されたもので、少なくとも、上記発光層は有機材料が蒸着により形成されている。   The basic structure of the organic EL display is such that a hole transport layer, a light emitting layer, and a cathode are sequentially disposed on an anode (transparent electrode) disposed on a glass substrate, and at least the light emitting layer is formed by depositing an organic material. It is formed by.

一般的に、ガラス基板上に蒸着により薄膜を形成する場合、真空容器内に有機材料の蒸発源を配置しておき、真空状態で蒸発源を加熱し、その蒸気を同じく真空容器内に配置された基板の表面に付着させることにより薄膜が形成される。   Generally, when a thin film is formed on a glass substrate by vapor deposition, an organic material evaporation source is placed in a vacuum vessel, the evaporation source is heated in a vacuum state, and the vapor is also placed in the vacuum vessel. A thin film is formed by adhering to the surface of the substrate.

上記有機材料を蒸着させる際に、主成分であるホスト材料に微量添加成分であるドーパント材料を混合させる場合があり、この場合、2つの異なる材料を異なる割合で且つ均一な成分量比でガラス基板上に蒸着させる必要がある。   When the organic material is vapor-deposited, a dopant material that is a trace addition component may be mixed with a host material that is a main component. In this case, two different materials are mixed in different proportions and at a uniform component amount ratio. It needs to be deposited on top.

このように、複数の異種材料を蒸着させる装置、方法等として、特許文献2に示すように、真空チャンバー内の被蒸着部材に対向する下部位置に2個のセルを配置し、各セルの放出孔から異種材料をそれぞれ放出するようにしたものがある。また特許文献3,4に示すように、別個に設けられた蒸発源で発生した材料を混合室で混合して放出させるものがある。
特開2004−269948 特開2003−297565 特開2002−30418 特開2003−155555
As described above, as an apparatus and method for depositing a plurality of different materials, as shown in Patent Document 2, two cells are arranged at a lower position facing a member to be deposited in a vacuum chamber, and each cell is discharged. There is one in which different materials are discharged from the holes. Further, as shown in Patent Documents 3 and 4, there are materials in which materials generated by separately provided evaporation sources are mixed and discharged in a mixing chamber.
JP2004-269948 JP 2003-297565 A JP2002-30418 JP2003-155555A

ところで、被蒸着部材に蒸着される蒸着膜厚は、所謂コサイン則による分布を示すことが知られているが、特許文献2に示すように、異種材料を別のセル室に入れて同時に蒸着させようとする場合、離れた位置の放出孔から放出された材料のコサイン則による膜厚分布では、部位によって成分量比が一定にならないため、品質が一定であるとはいえない。   By the way, it is known that the deposited film thickness deposited on the member to be deposited shows a distribution according to a so-called cosine law. However, as shown in Patent Document 2, different materials are placed in different cell chambers and deposited simultaneously. In such a case, in the film thickness distribution according to the cosine law of the material released from the discharge holes at the distant positions, the component amount ratio does not become constant depending on the part, so the quality cannot be said to be constant.

すなわち、図12に示すように、特許文献2の構成を特許文献1に適用して直線移動する基板3に蒸着する場合、基板3の移動方向の前部にホスト材料用の蒸発装置1を配置し、基板3の移動方向の後部にドーパント材料用の蒸発装置2を配置して蒸着すると、基板3に形成される蒸着膜全体における異種材料の成分量比が等しくなっても、膜厚方向において、最初に蒸着されるホスト材料の成分量比が膜厚の基板側で大きく、また次いで蒸着されるドーパント材料の成分量比が膜厚の表面側で大きくなり、膜厚方向において成分比率が不均一になるという問題がある。なお、図12において蒸発装置1,2の放出範囲を示す直線間に示された曲線は、蒸発流分布曲線である。   That is, as shown in FIG. 12, when the structure of Patent Document 2 is applied to Patent Document 1 and vapor deposition is performed on the substrate 3 that moves linearly, the evaporation apparatus 1 for the host material is arranged at the front in the moving direction of the substrate 3. If the evaporation apparatus 2 for dopant material is disposed at the rear of the movement direction of the substrate 3 and vapor deposition is performed, even if the component amount ratios of different materials in the entire vapor deposition film formed on the substrate 3 are equal, The component ratio of the host material deposited first is large on the substrate side of the film thickness, and the component ratio of the dopant material deposited next is large on the surface side of the film thickness. There is a problem that it becomes uniform. In addition, the curve shown between the straight lines which show the discharge | release range of the evaporators 1 and 2 in FIG. 12 is an evaporation flow distribution curve.

またこれを解消するために、図13に示すように、複数の防着板4を配置して材料を蒸着制御することも行われているが、各材料の蒸発流分布自体を変えるものではなく、防着板4により遮られた部分の材料が基板3に付着しないため、材料の利用効率が低下するという問題が生じる。   In order to solve this problem, as shown in FIG. 13, a plurality of deposition prevention plates 4 are arranged to control the evaporation of the material, but this does not change the evaporation flow distribution itself of each material. Since the material of the portion blocked by the deposition preventing plate 4 does not adhere to the substrate 3, there arises a problem that the utilization efficiency of the material is lowered.

さらにまた特許文献3,4に示すように、混合した後の材料を、多数の放出孔から放出することで、被蒸着部材と放出孔との間の距離を短くして材料の利用効率の低下を改善し、成分量比も均一にしやすくなるが、異種材料を混合した後で放出する場合は、温度差の異なる異種材料を取り扱うことが困難になる。   Furthermore, as shown in Patent Documents 3 and 4, the material after mixing is discharged from a large number of discharge holes, thereby shortening the distance between the deposition target member and the discharge holes and reducing the utilization efficiency of the material. Although it is easy to make the component amount ratio uniform, when different materials are released after mixing, it becomes difficult to handle different materials having different temperature differences.

これは、有機ELディスプレイの表示部を製造する有機材料は、安定性が低く、また異種材料間で蒸発温度が異なるとともに分解してその性能を失う分解温度(蒸発温度より高い)も異なることに起因する。すなわち、異種材料をそれぞれ独立して坩堝で加熱する場合には、蒸発温度以上で、分解温度未満に設定するだけでよく比較的制約が小さいが、異種材料を混合する場合には、混合する部分で混合される材料の全ての蒸発温度以上で、かつ分解温度未満に保持して、蒸着と分解とによる材料の劣化を防ぐ必要が生じるため、坩堝により個別に加熱する場合に比べて制約が大きくなる。   This is because the organic material for manufacturing the display part of the organic EL display has low stability, and the dissociation temperature (higher than the evaporation temperature) at which the dissociation material loses its performance due to the dissimilar evaporation temperature differs. to cause. That is, when different materials are heated independently in the crucible, it is only necessary to set the temperature to be equal to or higher than the evaporation temperature and lower than the decomposition temperature, but there are relatively few restrictions. It is necessary to prevent the material from being deteriorated due to vapor deposition and decomposition by maintaining it at a temperature equal to or higher than all the evaporation temperatures of the materials mixed in the process, and there are more restrictions than when individually heating with a crucible. Become.

有機ELディスプレイなどは一部製品が出回っているが、確立された分野とはいえず、特に、その材料においてはこれからどのようなものが出てくるかも知れず、蒸発温度と分解温度による制約を装置が大きく受ける構成は望ましいとはいえない。   Some products such as organic EL displays are on the market, but it is not an established field. Especially, what kind of materials may appear in the future, and there are restrictions due to evaporation temperature and decomposition temperature. A configuration in which the apparatus receives a large amount is not desirable.

本発明は上記問題点を解決して、被蒸着部材と蒸発源とを相対移動させて異種材料を蒸着させる場合、被蒸着部材に均一な異種材料の成分量比で蒸着することができる真空蒸着装置を提供することを目的とする。   The present invention solves the above-described problems, and when vapor deposition is performed on a member to be vapor-deposited by relatively moving the member to be vapor-deposited and the evaporation source, vacuum deposition can be performed on the member to be vapor-deposited at a uniform component amount ratio. An object is to provide an apparatus.

請求項1記載の発明は、異種の蒸着材料をそれぞれ加熱して気化させる複数の蒸発装置と、真空蒸着容器内で前記蒸発装置から気化された複数の蒸発材料を蒸着させる被蒸着部材と、前記蒸発装置と被蒸着部材の少なくとも一方を直線方向に移動させる移動装置とを具備し、
前記蒸発装置に、異種の蒸着材料をそれぞれ加熱して気化する複数の蒸発部と、前記移動装置による移動方向を横断する方向で、かつ上下段に配置されて前記各蒸発部から導入された蒸発材料をそれぞれ拡散する複数の拡散容器と、上段の前記拡散容器の上面に開口されたノズル口、および下段側の前記拡散容器から上方に突設されたノズル筒が上段側の前記拡散容器を貫通して上段の前記拡散容器の上面に開口されたノズル口からそれぞれ被蒸着部材に向かって蒸発材料を放出するノズル群とを設け、
前記ノズル群は、異種の蒸着材料をそれぞれ放出するノズル口が移動装置による移動方向の前後位置に近接配置されたノズル組を有し、当該ノズル組は、移動装置による移動方向を横断する方向に所定間隔でライン状に配置され、さらに隣接するノズル組で同種の蒸着材料を放出するノズル口が移動装置による移動方向の前後位置に配置されたものである。
The invention according to claim 1 is a plurality of evaporation devices for heating and vaporizing different kinds of vapor deposition materials, a member to be vapor deposited for vaporizing a plurality of evaporation materials vaporized from the evaporation device in a vacuum vapor deposition container, A moving device that moves at least one of the evaporation device and the deposition target member in a linear direction;
A plurality of evaporation units that heat and vaporize different kinds of vapor deposition materials in the evaporation device, and evaporation introduced from the evaporation units arranged in the upper and lower stages in a direction crossing the moving direction by the moving device. A plurality of diffusion containers for diffusing the material, a nozzle opening opened on the upper surface of the upper diffusion container, and a nozzle cylinder protruding upward from the lower diffusion container penetrate the upper diffusion container And a nozzle group that discharges the evaporation material from the nozzle opening opened on the upper surface of the upper diffusion container toward the deposition target member,
The nozzle group has a nozzle set in which nozzle ports for discharging different kinds of vapor deposition materials are arranged close to front and rear positions in the moving direction by the moving device , and the nozzle set is in a direction crossing the moving direction by the moving device. Nozzle ports that are arranged in a line at predetermined intervals and that discharge the same kind of vapor deposition material from adjacent nozzle groups are arranged in front and rear positions in the movement direction by the moving device .

請求項2記載の発明は、異種の蒸着材料をそれぞれ加熱して気化させる複数の蒸発装置と、真空蒸着容器内で前記蒸発装置から気化された複数の蒸発材料を蒸着させる被蒸着部材と、前記蒸発装置と被蒸着部材の少なくとも一方を直線方向に移動させる移動装置とを具備し、
前記蒸発装置に、異種の蒸着材料をそれぞれ加熱して気化する複数の蒸発部と、前記移動装置による移動方向を横断する方向で、かつ上下段に配置されて前記各蒸発部から導入された蒸発材料をそれぞれ拡散する複数の拡散容器と、上段の前記拡散容器の上面に開口されたノズル口、および下段側の前記拡散容器から上方に突設されたノズル筒が上段側の前記拡散容器を貫通して上段の前記拡散容器の上面に開口されたノズル口からそれぞれ被蒸着部材に向かって蒸発材料を放出するノズル群とを設け、
前記ノズル群は、異種の蒸着材料をそれぞれ放出するノズル口が、移動装置による移動方向でかつ移動方向を横断する方向に近接配置された複数のノズル組を有し、当該ノズル組が移動装置による移動方向を横断する方向に所定間隔でライン状に配置され、さらに隣接するノズル組で同種の蒸着材料を放出するノズル口が移動装置による移動方向の前後位置に配置されたものである。
The invention according to claim 2 is a plurality of evaporation devices for heating and vaporizing different kinds of vapor deposition materials, a member to be vapor deposited for vaporizing a plurality of evaporation materials vaporized from the evaporation device in a vacuum evaporation container, A moving device that moves at least one of the evaporation device and the deposition target member in a linear direction;
A plurality of evaporation units that heat and vaporize different kinds of vapor deposition materials in the evaporation device, and evaporation introduced from the evaporation units arranged in the upper and lower stages in a direction crossing the moving direction by the moving device. A plurality of diffusion containers for diffusing the material, a nozzle opening opened on the upper surface of the upper diffusion container, and a nozzle cylinder protruding upward from the lower diffusion container penetrate the upper diffusion container And a nozzle group that discharges the evaporation material from the nozzle opening opened on the upper surface of the upper diffusion container toward the deposition target member,
The nozzle group has a plurality of nozzle sets in which nozzle openings for discharging different kinds of vapor deposition materials are arranged close to each other in the direction of movement by the moving device and in the direction crossing the moving direction. The nozzle ports are arranged in a line at predetermined intervals in the direction crossing the moving direction, and the nozzle ports for discharging the same kind of vapor deposition material by the adjacent nozzle groups are arranged at the front and rear positions in the moving direction by the moving device .

請求項3記載の発明は、異種の蒸着材料をそれぞれ加熱して気化させる複数の蒸発装置と、真空蒸着容器内で前記蒸発装置から気化された複数の蒸発材料を蒸着させる被蒸着部材と、前記蒸発装置と被蒸着部材の少なくとも一方を直線方向に移動させる移動装置とを具備し、
前記蒸発装置に、異種の蒸着材料をそれぞれ加熱して気化する複数の蒸発部と、前記移動装置による移動方向を横断する方向で、かつ上下段に配置されて前記各蒸発部から導入された蒸発材料をそれぞれ拡散する複数の拡散容器と、上段の前記拡散容器の上面に開口されたノズル口、および下段側の前記拡散容器から上方に突設されたノズル筒が上段側の前記拡散容器を貫通して上段の前記拡散容器の上面に開口されたノズル口からそれぞれ被蒸着部材に向かって蒸発材料を放出するノズル群とを設け、
前記ノズル群は、異種の蒸着材料をそれぞれ放出する複数のノズル口が、移動装置による移動方向を横断する方向に近接配置されたノズル組を有し、当該ノズル組は、移動装置による移動方向を横断する方向に所定間隔でライン状に配置され、異種の蒸着材料を放出するノズル口が移動装置による移動方向を横断する方向に沿って交互に配置されたものである。
The invention according to claim 3 is a plurality of evaporation devices for heating and vaporizing different kinds of vapor deposition materials, a member to be vapor deposited for vaporizing a plurality of evaporation materials vaporized from the evaporation device in a vacuum vapor deposition container, A moving device that moves at least one of the evaporation device and the deposition target member in a linear direction;
A plurality of evaporation units that heat and vaporize different kinds of vapor deposition materials in the evaporation device, and evaporation introduced from the evaporation units arranged in the upper and lower stages in a direction crossing the moving direction by the moving device. A plurality of diffusion containers for diffusing the material, a nozzle opening opened on the upper surface of the upper diffusion container, and a nozzle cylinder protruding upward from the lower diffusion container penetrate the upper diffusion container And a nozzle group that discharges the evaporation material from the nozzle opening opened on the upper surface of the upper diffusion container toward the deposition target member,
The nozzle group has a nozzle set in which a plurality of nozzle openings for discharging different kinds of vapor deposition materials are arranged close to each other in a direction crossing the moving direction by the moving device, and the nozzle set has a moving direction by the moving device. The nozzle ports are arranged in a line at predetermined intervals in the crossing direction, and nozzle ports for discharging different kinds of vapor deposition materials are alternately arranged along the direction crossing the moving direction by the moving device .

請求項1乃至3記載の発明によれば、異種の蒸発材料を放出するノズル口が、移動装置による移動方向、または同移動方向および同移動方向を横断する方向、あるいは同移動方向を横断する方向に近接配置されたノズル組を、移動装置による移動方向を横断する方向にライン状に配置したので、ノズル口から放出される異種の蒸発材料の蒸発流分布がほぼ重なり、被蒸着部材に均一な成分量比で異種の蒸発材料を蒸着することができる。また異種の蒸発材料は、蒸発源から拡散部を介して複数のノズルに導入されるので、均一な放出が可能となり、均一な厚みの蒸着膜を形成することができる。 According to the first to third aspects of the present invention, the nozzle port that discharges the different kinds of evaporating materials has a moving direction by the moving device, a direction crossing the moving direction and the moving direction, or a direction crossing the moving direction. in a closely spaced nozzle sets, so arranged in a direction transverse to the moving direction by the moving device linearly, evaporative flow distribution of the evaporation of different materials discharged from the nozzle opening substantially overlap, uniform in the deposition member Different kinds of evaporation materials can be vapor-deposited in a component amount ratio. In addition, since different kinds of evaporation materials are introduced from the evaporation source to the plurality of nozzles via the diffusing portion, it is possible to discharge uniformly and form a vapor deposition film having a uniform thickness.

以下、本発明の実施の形態を図面に基づいて説明する。
[実施の形態1]
真空蒸発装置の実施の形態1を図1〜図5を参照して説明する。
Hereinafter, embodiments of the present invention will be described with reference to the drawings.
[Embodiment 1]
A first embodiment of a vacuum evaporation apparatus will be described with reference to FIGS.

この真空蒸着装置は、図1〜図3に示すように、たとえば有機ELディスプレイの表示部を製造するもので、真空蒸着容器11の蒸着室11a内で、たとえば2種類の蒸着材料をガラス基板(被蒸着部材)13に蒸着する。ここで、異種の蒸着材料、2種類のうち、主成分であるホスト材料を第1蒸着材料A、また微量添加成分であるドーピング材料を第2蒸着材料Bといい、第1,第2蒸着材料A,Bを加熱して気化させたものをそれぞれ第1蒸発材料、第2蒸発材料という。   As shown in FIGS. 1-3, this vacuum evaporation apparatus manufactures the display part of an organic electroluminescent display, for example, In the evaporation chamber 11a of the vacuum evaporation container 11, for example, two types of vapor deposition materials are made into a glass substrate ( Vapor deposition is performed on the vapor deposition member 13. Here, of the two types of vapor deposition materials, the host material which is the main component of the two types is referred to as the first vapor deposition material A, and the doping material which is the trace addition component is referred to as the second vapor deposition material B. The materials obtained by heating and evaporating A and B are referred to as a first evaporation material and a second evaporation material, respectively.

この真空蒸着装置は、真空ポンプ(図示せず)が接続されて蒸着室11aを形成する真空蒸着容器11と、第1,第2蒸着材料A,Bをそれぞれ加熱して気化させる蒸発装置12と、複数の保持ローラ14aを介してガラス基板13を一定高さに保持し水平な移動方向(以下、x方向という)に沿って所定速度で移動させる基板保持移動装置(移動装置)14とを具備している。   The vacuum deposition apparatus includes a vacuum deposition container 11 that is connected to a vacuum pump (not shown) to form a deposition chamber 11a, and an evaporation apparatus 12 that heats and vaporizes the first and second deposition materials A and B, respectively. And a substrate holding and moving device (moving device) 14 that holds the glass substrate 13 at a constant height via a plurality of holding rollers 14a and moves the glass substrate 13 at a predetermined speed along a horizontal moving direction (hereinafter referred to as the x direction). is doing.

前記蒸発装置12は、真空蒸着容器11の下部で外側に設けられて第1蒸着材料Aを加熱し気化する第1蒸発部(蒸発部)21Aおよび第2蒸着材料Bを加熱し気化する第2蒸発部(蒸発部)21Bと、第1,第2蒸発部21A,21Bから蒸発された第1,第2蒸発材料をそれぞれ蒸着室11a内に導入する第1,第2誘導管22A,22Bと、蒸着室11a内に設けられて第1,第2蒸発材料をそれぞれガラス基板13に向かって放出する放出部23とを具備し、前記第1,第2誘導管22A,22Bには、真空蒸着容器11の外側に、第1,第2蒸発材料の流量をそれぞれ調整する第1,第2流量制御弁24A,24Bが介在されている。   The evaporation device 12 is provided outside at a lower portion of the vacuum evaporation container 11 and heats and vaporizes the first evaporation part (evaporation part) 21A for heating and vaporizing the first evaporation material A and the second evaporation material B. An evaporating section (evaporating section) 21B, and first and second induction pipes 22A and 22B for introducing the first and second evaporating materials evaporated from the first and second evaporating sections 21A and 21B into the vapor deposition chamber 11a, respectively. And a discharge portion 23 provided in the vapor deposition chamber 11a for discharging the first and second evaporation materials toward the glass substrate 13, respectively. The first and second guide tubes 22A and 22B are provided with vacuum vapor deposition. First and second flow rate control valves 24A and 24B for adjusting the flow rates of the first and second evaporation materials are interposed outside the container 11, respectively.

前記第1蒸発部21Aおよび第2蒸発部21Bは、第1,第2蒸着材料A,Bをそれぞれ収容するセル(坩堝)21a,21aと、これらセル21a,21aに収容された第1,第2蒸着材料A,Bを加熱し気化する加熱装置21b,21bが設けられている。   The first evaporator 21A and the second evaporator 21B include cells (crucibles) 21a and 21a for storing the first and second vapor deposition materials A and B, respectively, and the first and first cells accommodated in the cells 21a and 21a. (2) Heating devices 21b and 21b for heating and vaporizing the vapor deposition materials A and B are provided.

前記放出部23には、上下2段に所定の隙間をあけて配設された第1拡散容器(拡散部)23Aおよび第2拡散容器(拡散部)23Bと、複数のノズル組25A,25Bを有するノズル群25とが具備されている。前記第1,第2拡散容器23A,23Bは横長の箱体状で、x方向に直交する横断方向(以下、y方向という)に沿って配置されている。第1拡散容器23A内には第1蒸発材料を均一に分散させる拡散空間(バッファ空間ともいう)が形成され、さらに第2拡散容器23Bを貫通した第1誘導管22Aが接続されている。また第2拡散容器23B内には第2蒸発材料を均一に分散させる拡散空間(バッファ空間ともいう)が形成され、さらに第2誘導管22Bが接続されている。   The discharge part 23 includes a first diffusion container (diffusion part) 23A and a second diffusion container (diffusion part) 23B arranged with a predetermined gap in two upper and lower stages, and a plurality of nozzle sets 25A and 25B. And a nozzle group 25 having the same. The first and second diffusion containers 23A and 23B have a horizontally long box shape, and are arranged along a transverse direction (hereinafter referred to as y direction) orthogonal to the x direction. A diffusion space (also referred to as a buffer space) for uniformly dispersing the first evaporation material is formed in the first diffusion container 23A, and a first guide pipe 22A penetrating the second diffusion container 23B is connected thereto. Further, a diffusion space (also referred to as a buffer space) for uniformly dispersing the second evaporation material is formed in the second diffusion container 23B, and a second guide tube 22B is further connected.

前記ノズル群25は、図4に示すように、y方向に沿って所定間隔tごとにライン状に配置された複数のノズル組25A,25Bからなり、各ノズル組25A,25Bは、第1拡散容器23Aの上面の所定位置に突設された第1ノズル筒(ノズル)25aと、第2拡散容器23Bの所定位置に突設された第2ノズル筒(ノズル)25bとがそれぞれx方向に近接配置されている。また第1ノズル組25Aと第2ノズル組25Bは、y方向に交互に配置されるとともに、第1ノズル筒25aと第2ノズル筒25bが逆位置に配置され、全体として第1ノズル筒25aと第2ノズル筒25bがいわゆる千鳥状に配置される。   As shown in FIG. 4, the nozzle group 25 includes a plurality of nozzle sets 25A and 25B arranged in a line at predetermined intervals t along the y direction, and each nozzle set 25A and 25B is a first diffusion. A first nozzle cylinder (nozzle) 25a protruding at a predetermined position on the upper surface of the container 23A and a second nozzle cylinder (nozzle) 25b protruding at a predetermined position of the second diffusion container 23B are close to each other in the x direction. Has been placed. The first nozzle set 25A and the second nozzle set 25B are alternately arranged in the y direction, and the first nozzle cylinder 25a and the second nozzle cylinder 25b are arranged in opposite positions, and the first nozzle cylinder 25a as a whole The second nozzle cylinders 25b are arranged in a so-called staggered pattern.

ここで「近接配置」とは、第1ノズル筒25aと第2ノズル筒25bとが互いに接している状態から、図4に示す所定の隙間δ(たとえば約15mm以下)をあけて配置された状態を含むものとする。   Here, “adjacent arrangement” means a state in which the first nozzle cylinder 25a and the second nozzle cylinder 25b are arranged with a predetermined gap δ (for example, about 15 mm or less) shown in FIG. Shall be included.

また第1ノズル筒25aは第1拡散容器23Aの上面に突設され、さらに第2ノズル筒25bは、基端部が第2拡散容器23Bの上面に接続開口され、先端部が第1拡散容器23Aの貫通穴に断熱部材を介して挿入されてその上面に突出されているが、図11(a)に示すように、上部に配置される第1拡散容器23Aの第1ノズル筒25aを筒状とせずに、第1拡散容器23Aの上面板に穿設開口されたノズル口(ノズル)25a’としてもよい。   The first nozzle cylinder 25a protrudes from the upper surface of the first diffusion container 23A, and the second nozzle cylinder 25b has a base end connected to the upper surface of the second diffusion container 23B and a distal end at the first diffusion container. As shown in FIG. 11 (a), the first nozzle cylinder 25a of the first diffusion container 23A disposed at the upper part is inserted into the through hole of 23A through the heat insulating member and protruded from the upper surface thereof. Instead of the shape, a nozzle port (nozzle) 25a ′ opened in the upper surface plate of the first diffusion container 23A may be used.

基板保持移動装置14は、たとえば図示するローラ駆動式の直線移動機構が採用され、ガラス基板13の両側辺部を、それぞれx方向に所定間隔ごとに配置された保持ローラ14aにより下方から保持させるとともに、保持ローラ14aを駆動装置(図示せず)により回転させることでガラス基板13を所定速度でx方向に移動させる。なお、ローラ駆動式以外に、ねじ軸式やラック・ピニオン式などの公知の他の直線移動機構を採用してもよい。   The substrate holding and moving device 14 employs, for example, a roller-driven linear moving mechanism shown in the figure, and holds both side portions of the glass substrate 13 from below by holding rollers 14a arranged at predetermined intervals in the x direction. The glass substrate 13 is moved in the x direction at a predetermined speed by rotating the holding roller 14a by a driving device (not shown). In addition to the roller drive type, other known linear movement mechanisms such as a screw shaft type and a rack and pinion type may be employed.

また第1,第2拡散容器23A,23Bには、第1,第2蒸発材料の冷却や付着を防止するために加熱ヒータ(図示せず)がそれぞれ設けられており、この輻射熱対策として、第1,第2拡散容器23A,23Bを覆い、かつ第1,第2ノズル筒25a,25bの対応位置に開口部が形成された防熱カバー(図示せず)が設けられる。さらにこの防熱カバー上に冷却板(図示せず)を設けて輻射熱を効果的に放散させることもできる。   Each of the first and second diffusion containers 23A and 23B is provided with a heater (not shown) for preventing cooling and adhesion of the first and second evaporation materials. A heat insulating cover (not shown) is provided which covers the first and second diffusion containers 23A and 23B and has openings formed at corresponding positions of the first and second nozzle cylinders 25a and 25b. Further, a cooling plate (not shown) can be provided on the heat insulating cover to effectively dissipate radiant heat.

そして、この真空蒸着装置には、図2に示すように、ガラス基板13に蒸着される膜厚を調整する膜厚制御装置26が設けられている。この膜厚制御装置26は、蒸着作業開始時などに、真空蒸着室11内のノズル群25の上方に配置された膜厚センサ27の検出信号と、第1,第2蒸発部21A,21Bのセル21a,21aに設置された温度センサ28A,28Bの検出信号とに基づいて、一定の蒸発量が検出されると、第1,第2蒸発部21A,21Bの加熱装置21b,21bを一定温度に保持しつつ、第1,第2流量制御弁24A,24Bを所定の開度で開放し、さらに基板保持移動装置駆動部14bによりガラス基板13を所定速度で移動してガラス基板13上に蒸着膜を形成する。また、膜厚の制御に際して、セル21a,21aの温度を一定に保持し、第1,第2流量制御弁24A,24Bにより蒸発流量を制御することにより、膜厚を均一に制御することができる。   The vacuum deposition apparatus is provided with a film thickness control device 26 that adjusts the film thickness deposited on the glass substrate 13 as shown in FIG. The film thickness control device 26 detects the detection signal of the film thickness sensor 27 disposed above the nozzle group 25 in the vacuum vapor deposition chamber 11 and the first and second evaporation units 21A and 21B at the start of the vapor deposition operation. When a certain amount of evaporation is detected based on the detection signals of the temperature sensors 28A and 28B installed in the cells 21a and 21a, the heating devices 21b and 21b of the first and second evaporators 21A and 21B are kept at a constant temperature. The first and second flow rate control valves 24A and 24B are opened at a predetermined opening degree while the glass substrate 13 is held at a predetermined speed, and the glass substrate 13 is moved at a predetermined speed by the substrate holding and moving device driving unit 14b to deposit on the glass substrate 13. A film is formed. Further, when controlling the film thickness, the temperature of the cells 21a, 21a is kept constant, and the film thickness can be controlled uniformly by controlling the evaporation flow rate by the first and second flow control valves 24A, 24B. .

また実施の形態1では、図4,図5に示すように、第1,第2ノズル筒25a,25bからガラス基板13までの蒸着距離Hが決定されると、x方向の上流側(下流側)の第1,第2ノズル筒25a,25bからガラス基板13の前辺部(後辺部)の移動始点(移動終点)までのノズル筒−始終点間距離:x0が決まる。またy方向で最も外側の第1,第2ノズル組25A,25Bの第1,第2ノズル筒25a,25bからガラス基板13の両側辺までのノズル筒−基板側辺間距離:y0も十分に長く決定される。ここでx0≧y0に設定されているが、ガラス基板13の中央部と、移動方向の前後辺部、左右側辺部も膜厚が均一となるように適宜設定されていればよい。なお、ノズル筒−基板側辺間距離:y0は、ライン状に配置されたy0におけるノズル組25A,25Bの間隔(ピッチ)を中央部より小さくしたり、y0における第1,第2ノズル筒25a,25bの口径を大きくすることにより、適宜短く変更することが可能となる。   In the first embodiment, as shown in FIGS. 4 and 5, when the deposition distance H from the first and second nozzle cylinders 25a, 25b to the glass substrate 13 is determined, the upstream side (downstream side) in the x direction. ) From the first and second nozzle cylinders 25a and 25b to the movement start point (movement end point) of the front side (rear side) of the glass substrate 13 is determined. Also, the distance between the nozzle cylinder and the substrate side from the first and second nozzle cylinders 25a and 25b of the outermost first and second nozzle sets 25A and 25B in the y direction to both sides of the glass substrate 13: y0 is also sufficient. Determined long. Here, x0 ≧ y0 is set, but the central portion of the glass substrate 13, the front and rear side portions, and the left and right side portions in the moving direction may be appropriately set so that the film thickness is uniform. The nozzle cylinder-substrate side distance: y0 is such that the interval (pitch) between the nozzle sets 25A and 25B in y0 arranged in a line is smaller than the central portion, or the first and second nozzle cylinders 25a in y0. , 25b can be shortened as appropriate by increasing the diameter.

またここで、各ノズル組25の第1,第2ノズル筒25a,25bの口径を同一に設定し、x0≧y0とした場合に、蒸発レート10Å/secで、膜厚の均一性を±5%以内とすることができた。   Here, when the diameters of the first and second nozzle cylinders 25a and 25b of each nozzle set 25 are set to be the same and x0 ≧ y0, the film thickness uniformity is ± 5 at an evaporation rate of 10 Å / sec. %.

上記構成において、第1蒸発部21Aで加熱装置21bによりセル21aが加熱されて第1蒸着材料Aが気化され、気化された第1蒸発材料が第1誘導管22Aから第1拡散容器23Aの拡散空間に導入されて均一に分散され、さらに第1蒸発材料が第1拡散容器23Aから第1ノズル筒25aを介して上方に向かって放出される。また第2蒸発部21Bで加熱装置21bによりセル21aが加熱されて第2蒸着材料Bが気化され、気化された第2蒸発材料Bが第2誘導管22Bから第2拡散容器23Bの拡散空間に導入されて均一に分散され、さらに第2蒸発材料が第2拡散容器23Bから第2ノズル筒25bを介して上方に向かって放出される。そして、第1ノズル筒25aから放出された第1蒸発材料と第2ノズル筒25bから放出された第2蒸発材料が共に、基板保持移動装置14により移動されるガラス基板13上にそれぞれ蒸着される。   In the above configuration, the cell 21a is heated by the heating device 21b in the first evaporation section 21A to vaporize the first vapor deposition material A, and the vaporized first evaporation material diffuses from the first induction tube 22A to the first diffusion container 23A. It is introduced into the space and uniformly dispersed, and the first evaporation material is further discharged upward from the first diffusion container 23A through the first nozzle cylinder 25a. In addition, the cell 21a is heated by the heating device 21b in the second evaporation section 21B to vaporize the second vapor deposition material B, and the vaporized second evaporation material B enters the diffusion space of the second diffusion container 23B from the second induction tube 22B. Introduced and uniformly dispersed, the second evaporation material is further discharged upward from the second diffusion container 23B through the second nozzle cylinder 25b. Then, both the first evaporation material released from the first nozzle cylinder 25a and the second evaporation material released from the second nozzle cylinder 25b are deposited on the glass substrate 13 moved by the substrate holding and moving device 14, respectively. .

上記実施の形態1によれば、蒸発装置12において第1,第2拡散容器23A,23Bでそれぞれ均一に分散された第1,第2蒸発材料が、近接配置された第1,第2ノズル筒25a,25bからそれぞれガラス基板13に向かって放出される。これにより各蒸発流がそれぞれコサイン則によりほぼ重なった状態で広がり、また第2ノズル筒25a,25bを有する第1,第2ノズル組25A,25Bがy方向にライン状に配置されることで、x方向に移動されるガラス基板13全体に成分量比が均一な蒸着膜を形成することができる。   According to the first embodiment, the first and second nozzle cylinders in which the first and second evaporation materials uniformly dispersed in the first and second diffusion containers 23A and 23B in the evaporator 12 are arranged in proximity to each other. 25a and 25b are emitted toward the glass substrate 13, respectively. As a result, the respective evaporative flows spread in a substantially overlapping state according to the cosine law, and the first and second nozzle sets 25A and 25B having the second nozzle cylinders 25a and 25b are arranged in a line in the y direction. A vapor deposition film having a uniform component amount ratio can be formed on the entire glass substrate 13 moved in the x direction.

またライン状に配置された第1,第2ノズル組25A,25Bの第1,第2ノズル筒25a,25bが千鳥状に配置されることから、膜厚方向における成分量比のむらをなくして均一な蒸着膜を形成することができる。   Further, since the first and second nozzle cylinders 25a and 25b of the first and second nozzle sets 25A and 25B arranged in a line are arranged in a staggered manner, the variation in the component amount ratio in the film thickness direction is eliminated and uniform. A vapor-deposited film can be formed.

なお、図6(a)に示すように、各ノズル組25Eの第1,第2ノズル筒25a,25bがy方向に位置ずれした千鳥状の配置であってもよい。
また図6(b)に示すように、第1,第2ノズル筒25a,25bを千鳥状に配置するのでなく、第1,第2ノズル組25C,25Dの第1,第2ノズル筒25a,25bをy方向に沿ってほぼ接した状態で配置し、第1,第2ノズル組25C,25Dをy方向に沿って所定の間隔t’をあけてライン状に配置してもよい。なお、ここでは第1ノズル組25Cと第2ノズル組25Dとは、第1,第2ノズル筒25a,25bの位置がy方向に逆に配置され、第1ノズル筒25aが内側となるように、y方向の中心線CLの一方側に第1ノズル組25Cが、他方側に第2ノズル組25Dが配置されている。
In addition, as shown to Fig.6 (a), the staggered arrangement | positioning which the 1st, 2nd nozzle cylinder 25a, 25b of each nozzle set 25E shifted in the y direction may be sufficient.
In addition, as shown in FIG. 6B, the first and second nozzle cylinders 25a and 25b are not arranged in a staggered manner, but the first and second nozzle cylinders 25a and 25D of the first and second nozzle groups 25C and 25D are arranged. 25b may be arranged in a state of being substantially in contact with the y direction, and the first and second nozzle sets 25C and 25D may be arranged in a line at a predetermined interval t ′ along the y direction. Here, the first nozzle set 25C and the second nozzle set 25D are arranged so that the positions of the first and second nozzle cylinders 25a and 25b are reversed in the y direction, and the first nozzle cylinder 25a is on the inner side. The first nozzle set 25C is arranged on one side of the center line CL in the y direction, and the second nozzle set 25D is arranged on the other side.

[実施の形態2]
この実施の形態2は、実施の形態1における第1,第2ノズル組25A,25Bの第1,第2ノズル筒25a,25bを、同心状に外嵌された二重管ノズルとしたもので、図7〜図9を参照して説明する。なお、実施の形態1と同一部材には同一符号を付して説明を省略する。
[Embodiment 2]
In the second embodiment, the first and second nozzle cylinders 25a and 25b of the first and second nozzle sets 25A and 25B in the first embodiment are formed as double tube nozzles fitted concentrically. This will be described with reference to FIGS. The same members as those in the first embodiment are denoted by the same reference numerals and description thereof is omitted.

すなわち、図7〜図9に示すように、ノズル群35におけるすべてのノズル組35Aは、第1拡散容器23Aの上板に突設された第1ノズル筒(ノズル)35aと、第2拡散容器23Bから第1拡散容器23Aの上下方向の貫通穴23aに断熱部材(図示せず)を介して挿入され第1拡散容器23A上に突出された第2ノズル筒(ノズル)35bからなり、第2ノズル筒35bは第1ノズル筒35a内に同一軸心上に配置されて二重管ノズルに構成され、第1拡散容器23Aの上にy方向に沿ってライン状に所定のピッチで配置されている。   That is, as shown in FIGS. 7 to 9, all the nozzle sets 35 </ b> A in the nozzle group 35 include a first nozzle cylinder (nozzle) 35 a protruding from the upper plate of the first diffusion container 23 </ b> A and the second diffusion container. A second nozzle cylinder (nozzle) 35b which is inserted through a heat insulating member (not shown) into the vertical through hole 23a of the first diffusion container 23A from 23B and protrudes on the first diffusion container 23A, and the second The nozzle cylinder 35b is arranged on the same axis in the first nozzle cylinder 35a to form a double pipe nozzle, and is arranged on the first diffusion container 23A in a line shape along the y direction at a predetermined pitch. Yes.

もちろん、図11(b)に示すように、第1ノズル筒35aを筒状とせずに、第1拡散容器23Aの上板に穿設開口された第1ノズル口(ノズル)35a’としてもよい。
上記実施の形態2によれば、ガラス基板13の移動方向と直交する方向にライン状に配置された複数のノズル群35を、各ノズル組35Aを第2蒸発材料を放出する第2ノズル筒35bの外周部に、第1蒸発材料を放出する第1ノズル筒35aを同一軸心上に外嵌して配置した二重管ノズルに構成したので、第1,第2蒸発材料の蒸発流が互いに重なり合ってガラス基板13に蒸着されることにより、ガラス基板13に均一な膜厚で蒸着膜を形成することができ、第1蒸着材料Aおよび第2蒸着材料Bの成分量比もさらに均一にすることができる。
Of course, as shown in FIG. 11 (b), the first nozzle cylinder 35a may be a first nozzle opening (nozzle) 35a 'opened in the upper plate of the first diffusion container 23A without forming the first nozzle cylinder 35a. .
According to the second embodiment, the plurality of nozzle groups 35 arranged in a line in a direction orthogonal to the moving direction of the glass substrate 13 are used as the second nozzle cylinder 35b that discharges the second evaporation material from each nozzle set 35A. The first nozzle cylinder 35a that discharges the first evaporating material is formed on the outer periphery of the double tube nozzle so as to be fitted on the same axis, so that the evaporating flows of the first and second evaporating materials are mutually connected. By overlapping and vapor-depositing on the glass substrate 13, it is possible to form a vapor-deposited film with a uniform film thickness on the glass substrate 13, and to make the component amount ratio of the first vapor-deposited material A and the second vapor-deposited material B even more uniform. be able to.

なお、上記実施の形態1,2では、蒸発装置12の第1蒸発部21Aと第2蒸発部21Bとを、真空蒸着容器11の外側に配置したが、次の実施の形態3のように、真空蒸着容器11内に蒸発装置12の全体を配置することもできる。   In the first and second embodiments, the first evaporation unit 21A and the second evaporation unit 21B of the evaporation device 12 are arranged outside the vacuum evaporation container 11, but as in the following third embodiment, The entire evaporation apparatus 12 can also be disposed in the vacuum evaporation container 11.

[実施の形態3]
実施の形態1,2では、基板保持移動装置14を設けてガラス基板13をx方向に移動させたが、この実施の形態3では、蒸発源移動装置41により蒸発装置12をx方向に移動するように構成したもので、図10を参照して説明する。なお、先の実施の形態1,2と同一部材には同一符号を付して説明を省略する。
[Embodiment 3]
In the first and second embodiments, the substrate holding / moving device 14 is provided and the glass substrate 13 is moved in the x direction. In the third embodiment, the evaporation device 12 is moved in the x direction by the evaporation source moving device 41. This will be described with reference to FIG. Note that the same members as those in the first and second embodiments are denoted by the same reference numerals and description thereof is omitted.

蒸発源移動装置41は、蒸着室11aの底部に複数のリニアレール42が敷設され、このリニアレール42にリニアベアリングを介して移動台43が移動自在に設置されている。そしてこの移動台43に、第1,第2蒸発部21A,21B、第1,第2誘導管22A,22B、第1,第2拡散容器23A,23B、第1,第2流量制御弁24A,24B、ノズル群25(または35)を有する蒸発装置12が設置されている。真空蒸着容器11の外側には、駆動ロッド44を介して移動台43を押し引き駆動するねじ軸式の駆動部45が設けられている。   In the evaporation source moving device 41, a plurality of linear rails 42 are laid on the bottom of the vapor deposition chamber 11a, and a moving table 43 is movably installed on the linear rails 42 via linear bearings. The moving table 43 includes first and second evaporators 21A and 21B, first and second induction pipes 22A and 22B, first and second diffusion containers 23A and 23B, first and second flow control valves 24A, The evaporator 12 having 24B and the nozzle group 25 (or 35) is installed. A screw shaft type drive unit 45 that pushes and pulls the moving table 43 through a drive rod 44 is provided outside the vacuum deposition container 11.

この駆動部45では、前記駆動ロッド44が、ガイドロッド45aに案内される駆動部材45bに連結され、さらに移動用回転駆動装置(電動モータ)45cにより回転駆動されるねじ軸45dがx方向に配設されている。そしてねじ軸45dに駆動部材45bに設けられた雌ねじ部材45eが螺合され、駆動ロッド44は真空シール用の蛇腹45fにより覆われている。したがって、移動用回転駆動装置45cによりねじ軸45dを回転駆動し雌ねじ部材45eを介して駆動部材45bを移動させ、さらに駆動ロッド44を介して移動台43をx方向に往復移動させることができる。   In the drive unit 45, the drive rod 44 is connected to a drive member 45b guided by a guide rod 45a, and a screw shaft 45d that is rotationally driven by a moving rotary drive device (electric motor) 45c is arranged in the x direction. It is installed. A female screw member 45e provided on the drive member 45b is screwed onto the screw shaft 45d, and the drive rod 44 is covered with a bellows 45f for vacuum sealing. Accordingly, the screw shaft 45d can be rotationally driven by the rotary drive device 45c for movement, the drive member 45b can be moved via the female screw member 45e, and the movable table 43 can be reciprocated in the x direction via the drive rod 44.

またガラス基板13は基板保持具46により保持されている。
さらに蒸着作業開始前には、真空蒸着室11内の一方の端部(図10左側)で防着板で区画されたレート調整部に蒸発装置12を移動させて膜厚センサ27により蒸発流密度を検出し調整する。
The glass substrate 13 is held by a substrate holder 46.
Further, before the vapor deposition operation is started, the evaporation apparatus 12 is moved to the rate adjusting section partitioned by the deposition preventing plate at one end (the left side in FIG. 10) in the vacuum vapor deposition chamber 11, and the evaporation flow density is measured by the film thickness sensor 27. Detect and adjust.

上記実施の形態3によれば、実施の形態1,2の基板保持移動装置14に替えて蒸発装置12を移動させる蒸発源移動装置41を設け、基板保持具46によりガラス基板13を固定状態で保持されることにより、実施の形態1,2と同様の作用効果を奏することができる。   According to the third embodiment, the evaporation source moving device 41 for moving the evaporation device 12 is provided in place of the substrate holding and moving device 14 of the first and second embodiments, and the glass substrate 13 is fixed by the substrate holder 46. By being held, the same effects as those of the first and second embodiments can be obtained.

なお、上記実施の形態1〜3では、第1,第2拡散容器23A,23Bを上下に配置したが、ガラス基板13の移動方向に並べて設置することもできる。
また異種の蒸着材料を2種類としたが、3種類以上とすることもできる。この場合、複数の拡散容器を、上下位置に3段以上に配置したり、またはx方向への並設と上下配置とを組み合わせて設置してもよく、またノズル筒を折り曲げてたり傾斜させることもできる。
In the first to third embodiments, the first and second diffusion containers 23A and 23B are arranged up and down. However, they can be arranged side by side in the moving direction of the glass substrate 13.
Further, although two kinds of different vapor deposition materials are used, three or more kinds can be used. In this case, a plurality of diffusion containers may be arranged in three or more stages in the vertical position, or may be installed in combination with the parallel arrangement in the x direction and the vertical arrangement, and the nozzle tube is bent or inclined. You can also.

さらに、蒸発源移動装置41と部材保持移動装置14とを並設し、蒸発装置12とガラス基板13とをそれぞれ相対方向に移動させて蒸着することもできる。   Further, the evaporation source moving device 41 and the member holding and moving device 14 can be arranged in parallel, and the evaporation device 12 and the glass substrate 13 can be moved in the relative directions to perform the deposition.

本発明に係る真空蒸着装置の実施の形態1を示す蒸発装置の斜視図である。It is a perspective view of the evaporation apparatus which shows Embodiment 1 of the vacuum evaporation system which concerns on this invention. 同真空蒸着装置を示す横断面図である。It is a cross-sectional view which shows the same vacuum evaporation system. 同真空蒸着装置を示す概略縦断面図である。It is a schematic longitudinal cross-sectional view which shows the same vacuum evaporation system. 同蒸発装置のノズル組の配置とガラス基板の関係を示す平面図である。It is a top view which shows the arrangement | positioning of the nozzle group of the same evaporation apparatus, and the relationship of a glass substrate. 同蒸発装置のノズル組の配置とガラス基板の関係を示す正面図である。It is a front view which shows the arrangement | positioning of the nozzle group of the same evaporation apparatus, and the relationship of a glass substrate. 蒸発装置の第1,第2ノズル筒の配置の変形例をそれぞれ示す平面図で、(a)は千鳥配置の変形例、(b)はy方向の配置例を示すものである。It is a top view which shows the modification of arrangement | positioning of the 1st, 2nd nozzle cylinder of an evaporator, respectively, (a) shows the modification of zigzag arrangement, (b) shows the example of arrangement | positioning of ay direction. 本発明に係る真空蒸着装置の実施の形態2を示す蒸発装置の斜視図である。It is a perspective view of the evaporation apparatus which shows Embodiment 2 of the vacuum evaporation system which concerns on this invention. 同真空蒸着装置を示す横断面図である。It is a cross-sectional view which shows the same vacuum evaporation system. 同蒸発装置の拡散容器を示す横断面図である。It is a cross-sectional view which shows the diffusion container of the evaporation apparatus. 本発明に係る真空蒸着装置の実施の形態3を示し、蒸発装置の縦断面図である。It is Embodiment 3 of the vacuum evaporation system which concerns on this invention, and is a longitudinal cross-sectional view of an evaporation apparatus. ノズル組の変形例を示す縦断面図で、(a)は実施の形態1のノズル組の変形例を示し、(b)は実施の形態2のノズル組の変形例を示す。FIG. 6 is a longitudinal sectional view showing a modified example of the nozzle set, where (a) shows a modified example of the nozzle set of the first embodiment, and (b) shows a modified example of the nozzle set of the second embodiment. 移動する基板に2つの材料を蒸着する場合の従来の蒸着装置の構成図である。It is a block diagram of the conventional vapor deposition apparatus in the case of vapor-depositing two materials on the moving board | substrate. 同従来の蒸着装置に防着板を付加した時の構成図である。It is a block diagram when an adhesion prevention board is added to the conventional vapor deposition apparatus.

符号の説明Explanation of symbols

A 第1蒸着材料
B 第2蒸着材料
11 真空蒸着容器
11a 蒸着室
12 蒸発装置
13 ガラス基板
14 基板保持移動装置
21A 第1蒸発部
21B 第2蒸発部
22A 第1誘導管
22B 第2誘導管
23 放出部
23A 第1拡散容器
23B 第2拡散容器
24A 第1流量調整弁
24B 第2流量調整弁
25 ノズル群
25A,25B ノズル組
25a 第1ノズル筒
25a’ 第1ノズル口
25b 第2ノズル筒
35 ノズル群
35A ノズル組
35a 第1ノズル筒
35b 第2ノズル筒
41 蒸発源移動装置
46 基板保持具
A 1st vapor deposition material B 2nd vapor deposition material 11 Vacuum vapor deposition container 11a Vapor deposition chamber 12 Evaporating device 13 Glass substrate 14 Substrate holding and moving device 21A First evaporating unit 21B Second evaporating unit 22A First induction tube 22B Second induction tube 23 Release Part 23A First diffusion container 23B Second diffusion container 24A First flow rate adjustment valve 24B Second flow rate adjustment valve 25 Nozzle group 25A, 25B Nozzle group 25a First nozzle cylinder 25a 'First nozzle port 25b Second nozzle cylinder 35 Nozzle group 35A Nozzle set 35a First nozzle cylinder 35b Second nozzle cylinder 41 Evaporation source moving device 46 Substrate holder

Claims (3)

異種の蒸着材料をそれぞれ加熱して気化させる複数の蒸発装置と、真空蒸着容器内で前記蒸発装置から気化された複数の蒸発材料を蒸着させる被蒸着部材と、前記蒸発装置と被蒸着部材の少なくとも一方を直線方向に移動させる移動装置とを具備し、
前記蒸発装置に、異種の蒸着材料をそれぞれ加熱して気化する複数の蒸発部と、前記移動装置による移動方向を横断する方向で、かつ上下段に配置されて前記各蒸発部から導入された蒸発材料をそれぞれ拡散する複数の拡散容器と、上段の前記拡散容器の上面に開口されたノズル口、および下段側の前記拡散容器から上方に突設されたノズル筒が上段側の前記拡散容器を貫通して上段の前記拡散容器の上面に開口されたノズル口からそれぞれ被蒸着部材に向かって蒸発材料を放出するノズル群とを設け、
前記ノズル群は、異種の蒸着材料をそれぞれ放出するノズル口が移動装置による移動方向の前後位置に近接配置されたノズル組を有し、当該ノズル組は、移動装置による移動方向を横断する方向に所定間隔でライン状に配置され、さらに隣接するノズル組で同種の蒸着材料を放出するノズル口が移動装置による移動方向の前後位置に配置された
真空蒸着装置。
A plurality of evaporation devices that heat and vaporize different types of vapor deposition materials, a vapor deposition member that vapor deposits a plurality of vaporization materials vaporized from the vaporization device in a vacuum vapor deposition container, and at least one of the evaporation device and the vapor deposition member A moving device for moving one side in a linear direction,
A plurality of evaporation units that heat and vaporize different kinds of vapor deposition materials in the evaporation device, and evaporation introduced from the evaporation units arranged in the upper and lower stages in a direction crossing the moving direction by the moving device. A plurality of diffusion containers for diffusing the material, a nozzle opening opened on the upper surface of the upper diffusion container, and a nozzle cylinder protruding upward from the lower diffusion container penetrate the upper diffusion container And a nozzle group that discharges the evaporation material from the nozzle opening opened on the upper surface of the upper diffusion container toward the deposition target member,
The nozzle group has a nozzle set in which nozzle ports for discharging different kinds of vapor deposition materials are arranged close to front and rear positions in the moving direction by the moving device , and the nozzle set is in a direction crossing the moving direction by the moving device. A vacuum vapor deposition apparatus in which nozzle ports that are arranged in a line at predetermined intervals and that discharge nozzles of the same kind from adjacent nozzle groups are arranged in front and rear positions in the movement direction of the movement apparatus.
異種の蒸着材料をそれぞれ加熱して気化させる複数の蒸発装置と、真空蒸着容器内で前記蒸発装置から気化された複数の蒸発材料を蒸着させる被蒸着部材と、前記蒸発装置と被蒸着部材の少なくとも一方を直線方向に移動させる移動装置とを具備し、
前記蒸発装置に、異種の蒸着材料をそれぞれ加熱して気化する複数の蒸発部と、前記移動装置による移動方向を横断する方向で、かつ上下段に配置されて前記各蒸発部から導入された蒸発材料をそれぞれ拡散する複数の拡散容器と、上段の前記拡散容器の上面に開口されたノズル口、および下段側の前記拡散容器から上方に突設されたノズル筒が上段側の前記拡散容器を貫通して上段の前記拡散容器の上面に開口されたノズル口からそれぞれ被蒸着部材に向かって蒸発材料を放出するノズル群とを設け、
前記ノズル群は、異種の蒸着材料をそれぞれ放出するノズル口が、移動装置による移動方向でかつ移動方向を横断する方向に近接配置された複数のノズル組を有し、当該ノズル組が移動装置による移動方向を横断する方向に所定間隔でライン状に配置され、さらに隣接するノズル組で同種の蒸着材料を放出するノズル口が移動装置による移動方向の前後位置に配置された
真空蒸着装置。
A plurality of evaporation devices that heat and vaporize different types of vapor deposition materials, a vapor deposition member that vapor deposits a plurality of vaporization materials vaporized from the vaporization device in a vacuum vapor deposition container, and at least one of the evaporation device and the vapor deposition member A moving device for moving one side in a linear direction,
A plurality of evaporation units that heat and vaporize different kinds of vapor deposition materials in the evaporation device, and evaporation introduced from the evaporation units arranged in the upper and lower stages in a direction crossing the moving direction by the moving device. A plurality of diffusion containers for diffusing the material, a nozzle opening opened on the upper surface of the upper diffusion container, and a nozzle cylinder protruding upward from the lower diffusion container penetrate the upper diffusion container And a nozzle group that discharges the evaporation material from the nozzle opening opened on the upper surface of the upper diffusion container toward the deposition target member,
The nozzle group has a plurality of nozzle sets in which nozzle openings for discharging different kinds of vapor deposition materials are arranged close to each other in the direction of movement by the moving device and in the direction crossing the moving direction. A vacuum vapor deposition apparatus in which nozzle ports for discharging the same kind of vapor deposition material from adjacent nozzle groups are arranged in front and rear positions in the movement direction by a moving apparatus, arranged in a line at predetermined intervals in a direction crossing the movement direction .
異種の蒸着材料をそれぞれ加熱して気化させる複数の蒸発装置と、真空蒸着容器内で前記蒸発装置から気化された複数の蒸発材料を蒸着させる被蒸着部材と、前記蒸発装置と被蒸着部材の少なくとも一方を直線方向に移動させる移動装置とを具備し、
前記蒸発装置に、異種の蒸着材料をそれぞれ加熱して気化する複数の蒸発部と、前記移動装置による移動方向を横断する方向で、かつ上下段に配置されて前記各蒸発部から導入された蒸発材料をそれぞれ拡散する複数の拡散容器と、上段の前記拡散容器の上面に開口されたノズル口、および下段側の前記拡散容器から上方に突設されたノズル筒が上段側の前記拡散容器を貫通して上段の前記拡散容器の上面に開口されたノズル口からそれぞれ被蒸着部材に向かって蒸発材料を放出するノズル群とを設け、
前記ノズル群は、異種の蒸着材料をそれぞれ放出する複数のノズル口が、移動装置による移動方向を横断する方向に近接配置されたノズル組を有し、当該ノズル組は、移動装置による移動方向を横断する方向に所定間隔でライン状に配置され、異種の蒸着材料を放出するノズル口が移動装置による移動方向を横断する方向に沿って交互に配置された
真空蒸着装置。
A plurality of evaporation devices that heat and vaporize different types of vapor deposition materials, a vapor deposition member that vapor deposits a plurality of vaporization materials vaporized from the vaporization device in a vacuum vapor deposition container, and at least one of the evaporation device and the vapor deposition member A moving device for moving one side in a linear direction,
A plurality of evaporation units that heat and vaporize different kinds of vapor deposition materials in the evaporation device, and evaporation introduced from the evaporation units arranged in the upper and lower stages in a direction crossing the moving direction by the moving device. A plurality of diffusion containers for diffusing the material, a nozzle opening opened on the upper surface of the upper diffusion container, and a nozzle cylinder protruding upward from the lower diffusion container penetrate the upper diffusion container And a nozzle group that discharges the evaporation material from the nozzle opening opened on the upper surface of the upper diffusion container toward the deposition target member,
The nozzle group has a nozzle set in which a plurality of nozzle openings for discharging different kinds of vapor deposition materials are arranged close to each other in a direction crossing the moving direction by the moving device, and the nozzle set has a moving direction by the moving device. A vacuum vapor deposition apparatus in which nozzle ports that are arranged in a line at predetermined intervals in a transverse direction and that discharge nozzles of different types of vapor deposition materials are alternately arranged along a direction that traverses the movement direction of the movement apparatus.
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