JP4680462B2 - アルカリ金属メトキサイドの製造方法 - Google Patents

アルカリ金属メトキサイドの製造方法 Download PDF

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Publication number
JP4680462B2
JP4680462B2 JP2001543481A JP2001543481A JP4680462B2 JP 4680462 B2 JP4680462 B2 JP 4680462B2 JP 2001543481 A JP2001543481 A JP 2001543481A JP 2001543481 A JP2001543481 A JP 2001543481A JP 4680462 B2 JP4680462 B2 JP 4680462B2
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Prior art keywords
tower
methanol
column
alkali metal
reaction
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Expired - Fee Related
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JP2001543481A
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Japanese (ja)
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JP2003516373A (ja
JP2003516373A5 (enExample
Inventor
グート，ヨーゼフ
フリードリヒ，ホルガー
シュテルツェル，ハンス−ヨーゼフ
カイベル，ゲルト
ブルカルト，キルステン
ホフマン，エルケ
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BASF SE
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BASF SE
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Publication of JP2003516373A5 publication Critical patent/JP2003516373A5/ja
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Publication of JP4680462B2 publication Critical patent/JP4680462B2/ja
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/28—Evaporating with vapour compression
    • B01D1/284—Special features relating to the compressed vapour
    • B01D1/2856—The compressed vapour is used for heating a reboiler or a heat exchanger outside an evaporator
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/68—Preparation of metal alcoholates
    • C07C29/70—Preparation of metal alcoholates by converting hydroxy groups to O-metal groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2001543481A 1999-12-08 2000-12-08 アルカリ金属メトキサイドの製造方法 Expired - Fee Related JP4680462B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19959153A DE19959153A1 (de) 1999-12-08 1999-12-08 Verfahren zur Herstellung von Alkalimethylaten
DE19959153.9 1999-12-08
PCT/EP2000/012440 WO2001042178A1 (de) 1999-12-08 2000-12-08 Verfahren zur herstellung von alkalimethylaten

Publications (3)

Publication Number Publication Date
JP2003516373A JP2003516373A (ja) 2003-05-13
JP2003516373A5 JP2003516373A5 (enExample) 2008-01-31
JP4680462B2 true JP4680462B2 (ja) 2011-05-11

Family

ID=7931845

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2001543481A Expired - Fee Related JP4680462B2 (ja) 1999-12-08 2000-12-08 アルカリ金属メトキサイドの製造方法

Country Status (11)

Country Link
US (1) US6759560B2 (enExample)
EP (1) EP1242345B1 (enExample)
JP (1) JP4680462B2 (enExample)
KR (1) KR100686683B1 (enExample)
CN (1) CN1167658C (enExample)
AT (1) ATE276222T1 (enExample)
AU (1) AU3008501A (enExample)
DE (2) DE19959153A1 (enExample)
HU (1) HU229495B1 (enExample)
MY (1) MY126773A (enExample)
WO (1) WO2001042178A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI828051B (zh) * 2021-02-05 2024-01-01 德商贏創運營有限公司 鹼金屬烷氧化物之高能效製備方法

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DE10008634A1 (de) * 2000-02-24 2001-08-30 Basf Ag Trennwandkolonne zur Auftrennung eines Vielstoffgemisches
JP4484572B2 (ja) * 2003-08-21 2010-06-16 昭和電工株式会社 ヘキサフルオロエタンの製造方法およびその用途
CN1298689C (zh) * 2004-08-13 2007-02-07 于志波 碱法生产甲/乙醇钠工艺
JP4229395B2 (ja) * 2004-09-27 2009-02-25 旭化成ケミカルズ株式会社 芳香族カーボネートの工業的製造方法
DE102005062654A1 (de) * 2005-12-23 2007-06-28 Basf Ag Verfahren zur Gewinnung von Alkoholaten
DE102007025904A1 (de) * 2007-06-01 2008-12-04 Evonik Degussa Gmbh Verfahren zur Herstellung von Alkalimetallalkoholaten
RU2358963C2 (ru) * 2007-08-10 2009-06-20 Закрытое акционерное общество "Химтэк Инжиниринг" Способ получения метилата калия
US20090134369A1 (en) * 2007-11-26 2009-05-28 Applied Nanoworks, Inc. Metal alkoxides, apparatus for manufacturing metal alkoxides, related methods and uses thereof
JP2012518667A (ja) * 2009-02-26 2012-08-16 ビーエーエスエフ ソシエタス・ヨーロピア メタノール／水−混合物の蒸留による後処理法並びにアルカリ金属メチラートの製造法
JP4803470B2 (ja) * 2009-10-05 2011-10-26 独立行政法人産業技術総合研究所 熱交換型蒸留装置
AR093211A1 (es) 2012-05-10 2015-05-27 Ypf Soc Anonima Metodo para preparar alcoxidos de metales alcalinos
WO2014165100A1 (en) * 2013-03-13 2014-10-09 Bp Corporation North America Inc. Method of recycling centrate to generate steam in a stripper
CN103288593B (zh) * 2013-06-04 2015-06-03 江苏乐科热力科技有限公司 机械蒸气再压缩甲醇钠生产装置及方法
CN103387483B (zh) * 2013-08-14 2015-06-17 重庆紫光化工股份有限公司 甲醇碱金属盐的生产装置和工艺
WO2016083175A1 (de) * 2014-11-24 2016-06-02 Basf Se Herstellung eines metallalkoxids mittels reaktivdestillation
CN108299159B (zh) * 2018-03-01 2020-06-12 浙江大学 一种连续制备2-甲基烯丙醇盐醇溶液的方法
CN109199298B (zh) * 2018-10-22 2024-01-23 东莞理工学院 一种除湿干燥装置及洗碗机
CN110204423A (zh) * 2019-07-12 2019-09-06 浙江圣安化工股份有限公司 一种碱金属醇盐的制备方法
EP4077253B1 (de) 2019-12-18 2024-06-12 Basf Se Verfahren zur herstellung von metallalkoholaten
EP4093724B1 (de) 2020-01-23 2024-01-31 Evonik Operations GmbH Verfahren zur gleichzeitigen herstellung von natrium- und kaliumalkoholaten
ES2978670T3 (es) 2020-01-23 2024-09-17 Evonik Operations Gmbh Procedimiento para la preparación energéticamente eficiente de alcoholatos de sodio y potasio
US20240025829A1 (en) * 2020-12-04 2024-01-25 Basf Se Integrated process for the parallel production of alkali metal methoxides
EP4074684B1 (de) 2021-04-16 2025-09-03 Evonik Operations GmbH Verfahren zur energieeffizienten herstellung von alkalimetallalkoholaten
EP4074685B1 (de) 2021-04-16 2025-09-03 Evonik Operations GmbH Verfahren zur energieeffizienten herstellung von alkalimetallalkoholaten
BR112023026333A2 (pt) 2021-06-16 2024-03-05 Evonik Operations Gmbh Processo para processamento de mistura metanol/água na produção de metóxidos de metais alcalinos em coluna de reação
JP2025511294A (ja) 2022-04-04 2025-04-15 エボニック オペレーションズ ゲーエムベーハー ポリエチレンテレフタレートの改良された解重合法
JP2025512918A (ja) 2022-04-04 2025-04-22 エボニック オペレーションズ ゲーエムベーハー ポリエチレンテレフタレートの改良された解重合法
KR20250092186A (ko) 2022-10-19 2025-06-23 에보닉 오퍼레이션스 게엠베하 폴리에틸렌 테레프탈레이트의 개선된 탈중합 방법
KR20250092187A (ko) 2022-10-19 2025-06-23 에보닉 오퍼레이션스 게엠베하 폴리에틸렌 테레프탈레이트의 개선된 탈중합 방법
JP2025536143A (ja) 2022-10-20 2025-10-31 エボニック オペレーションズ ゲーエムベーハー アルカリ金属メトキシドを製造するための改善された方法
EP4626569A1 (de) 2022-11-30 2025-10-08 Evonik Operations GmbH Verbessertes verfahren zur herstellung von alkalimetallmethanolaten
AR131179A1 (es) 2022-12-07 2025-02-26 Evonik Operations Gmbh Procedimiento mejorado para producir compuestos de alcóxidos metálicos
WO2024125775A1 (de) 2022-12-14 2024-06-20 Evonik Operations Gmbh Verbessertes verfahren zur herstellung von metallalkoholatverbindungen
CN120584149A (zh) 2023-01-23 2025-09-02 赢创运营有限公司 用于在挤出机中解聚聚对苯二甲酸亚烷基酯的方法
KR20250140524A (ko) 2023-01-23 2025-09-25 에보닉 오퍼레이션스 게엠베하 압출기에서 폴리알킬렌 테레프탈레이트의 해중합을 위한 공정
CN120584151A (zh) 2023-01-23 2025-09-02 赢创运营有限公司 用于在具有低熔点聚烯烃的混合物中解聚聚对苯二甲酸亚烷基酯的方法
WO2025125586A1 (en) 2023-12-14 2025-06-19 Basf Se Integrated process for simultaneously preparing alkali metal methoxides
WO2025125546A1 (en) 2023-12-14 2025-06-19 Basf Se Integrated process for simultaneously preparing alkali metal methoxides
WO2025125585A1 (en) 2023-12-14 2025-06-19 Basf Se Integrated process for simultaneous preparation of alkali metal methoxides
WO2025233486A1 (en) 2024-05-10 2025-11-13 Basf Se Integrated process for simultaneously preparing n mixtures comprising alkali metal methoxide and methanol and for preparing solid alkali metal methoxide

Family Cites Families (10)

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DE968903C (de) * 1952-05-13 1958-04-10 Huels Chemische Werke Ag Verfahren zur kontinuierlichen Herstellung von Alkalialkoholaten
US2877274A (en) * 1958-01-21 1959-03-10 Du Pont Production of sodium methoxide
DE3413212C1 (de) 1984-04-07 1985-09-12 Dynamit Nobel Ag, 5210 Troisdorf Verfahren zur Herstellung von wasserfreiem Kalium-tert.-butoxid
EP0192608B1 (de) * 1985-02-20 1991-07-24 Ciba-Geigy Ag Verfahren zur Herstellung von Alkalialkoholaten
DE3701268C1 (de) 1987-01-17 1988-04-14 Dynamit Nobel Ag Verfahren zur kontinuierlichen Herstellung von Kalium-tert.-butoxid
DE3702052C1 (de) * 1987-01-24 1988-07-14 Degussa Verfahren zur Herstellung von Natriumalkoholat hoher Reinheit aus dem Filtrationsrueckstand von schmelzelektrolytisch gewonnenem Rohnatrium
DE3723193A1 (de) * 1987-07-14 1989-01-26 Metallgesellschaft Ag Verfahren zur herstellung von alkoholaten
ATE81495T1 (de) * 1988-03-29 1992-10-15 Atochem Elf Sa Verfahren zur herstellung von natriumfluoralkoholaten.
FI94063C (fi) * 1993-08-17 1995-07-10 Kemira Oy Menetelmä alkalimetalli- tai ammoniumperoksodisulfaattisuolojen ja alkalimetallihydroksidin samanaikaiseksi valmistamiseksi
DE4418488A1 (de) * 1994-05-27 1995-11-30 Basf Ag Verfahren und Vorrichtung zur destillativen Trennung von Stoffgemischen

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI828051B (zh) * 2021-02-05 2024-01-01 德商贏創運營有限公司 鹼金屬烷氧化物之高能效製備方法

Also Published As

Publication number Publication date
AU3008501A (en) 2001-06-18
DE50007815D1 (de) 2004-10-21
KR20020060253A (ko) 2002-07-16
HU229495B1 (en) 2014-01-28
EP1242345A1 (de) 2002-09-25
CN1167658C (zh) 2004-09-22
HUP0301074A2 (hu) 2003-08-28
KR100686683B1 (ko) 2007-02-27
EP1242345B1 (de) 2004-09-15
CN1409696A (zh) 2003-04-09
HUP0301074A3 (en) 2005-11-28
DE19959153A1 (de) 2001-06-21
ATE276222T1 (de) 2004-10-15
US20020183566A1 (en) 2002-12-05
JP2003516373A (ja) 2003-05-13
WO2001042178A1 (de) 2001-06-14
US6759560B2 (en) 2004-07-06
MY126773A (en) 2006-10-31

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