JP4451499B2 - ピリチオン塩粒子の製造方法 - Google Patents
ピリチオン塩粒子の製造方法 Download PDFInfo
- Publication number
- JP4451499B2 JP4451499B2 JP54054998A JP54054998A JP4451499B2 JP 4451499 B2 JP4451499 B2 JP 4451499B2 JP 54054998 A JP54054998 A JP 54054998A JP 54054998 A JP54054998 A JP 54054998A JP 4451499 B2 JP4451499 B2 JP 4451499B2
- Authority
- JP
- Japan
- Prior art keywords
- pyrithione
- salt
- zinc
- water
- particles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/89—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members with hetero atoms directly attached to the ring nitrogen atom
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4933—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having sulfur as an exocyclic substituent, e.g. pyridinethione
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y5/00—Nanobiotechnology or nanomedicine, e.g. protein engineering or drug delivery
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Molecular Biology (AREA)
- Medicinal Chemistry (AREA)
- Medical Informatics (AREA)
- General Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Biophysics (AREA)
- Cosmetics (AREA)
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US4079397P | 1997-03-14 | 1997-03-14 | |
US60/040,793 | 1997-03-14 | ||
US09/032,959 US6017936A (en) | 1997-03-14 | 1998-03-02 | Method for producing particles of pyrithione salts and particles so produced |
US09/032,959 | 1998-03-02 | ||
PCT/US1998/004139 WO1998041505A1 (en) | 1997-03-14 | 1998-03-04 | Method for producing particles of pyrithione salts |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2001516359A JP2001516359A (ja) | 2001-09-25 |
JP4451499B2 true JP4451499B2 (ja) | 2010-04-14 |
Family
ID=26709102
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP54054998A Expired - Lifetime JP4451499B2 (ja) | 1997-03-14 | 1998-03-04 | ピリチオン塩粒子の製造方法 |
Country Status (10)
Country | Link |
---|---|
US (1) | US6017936A (ko) |
EP (1) | EP0983242A4 (ko) |
JP (1) | JP4451499B2 (ko) |
KR (1) | KR100580134B1 (ko) |
CN (1) | CN1136194C (ko) |
AU (1) | AU6680898A (ko) |
BR (1) | BR9808257A (ko) |
CA (1) | CA2283882A1 (ko) |
ID (1) | ID23513A (ko) |
WO (1) | WO1998041505A1 (ko) |
Families Citing this family (51)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6242007B1 (en) * | 1997-04-28 | 2001-06-05 | Arch Chemicals, Inc. | Non-spherical and non-platelet forms of pyrithione salts and methods of making same |
US6465015B1 (en) | 1998-02-24 | 2002-10-15 | Arch Chemicals, Inc. | Sonic method of enhancing chemical reactions to provide uniform, non-agglomerated particles |
GB9813640D0 (en) * | 1998-06-24 | 1998-08-26 | Unilever Plc | Antimicrobial hair treatment composition |
US7942958B1 (en) * | 1998-07-22 | 2011-05-17 | Arch Chemicals, Inc. | Composite biocidal particles |
US6682724B2 (en) * | 1999-02-23 | 2004-01-27 | Arch Chemcials, Inc. | Sonic method of enhancing chemical reactions to provide uniform, non-agglomerated particles |
US6432432B1 (en) * | 1999-03-05 | 2002-08-13 | Arch Chemicals, Inc. | Chemical method of making a suspension, emulsion or dispersion of pyrithione particles |
WO2000073272A1 (fr) * | 1999-05-31 | 2000-12-07 | Yoshitomi Fine Chemicals, Ltd. | Pyrithione de cuivre de grande purete, et procede de production correspondant |
JP3532500B2 (ja) * | 1999-05-31 | 2004-05-31 | キクチカラー株式会社 | 船底塗料用防汚剤およびそれに用いる高純度銅ピリチオンの製造方法 |
DE19961278A1 (de) * | 1999-12-18 | 2001-06-21 | Cognis Deutschland Gmbh | Verwendung von nanoskaligen Antischuppenwirkstoffen |
KR100634967B1 (ko) * | 2000-01-21 | 2006-10-16 | 주식회사 코오롱 | 무기염이 제거된 금속 피리치온 미세 분산액 및 그의제조방법 |
US6627665B2 (en) * | 2001-09-28 | 2003-09-30 | Arch Chemicals, Inc. | Non-dusting copper pyrithione dispersion |
US6821326B2 (en) * | 2002-12-20 | 2004-11-23 | Arch Chemicals, Inc. | Small particle copper pyrithione |
US7481873B2 (en) * | 2002-12-20 | 2009-01-27 | Arch Chemicals, Inc. | Small particle copper pyrithione |
US20070053950A1 (en) * | 2005-02-28 | 2007-03-08 | Gajanan Shukla P | Composition of polymer microcapsules of biocide for coating material |
US7772421B2 (en) | 2005-05-31 | 2010-08-10 | Rhodia Inc. | Compositions having HASE rheology modifiers |
US8993506B2 (en) * | 2006-06-12 | 2015-03-31 | Rhodia Operations | Hydrophilized substrate and method for hydrophilizing a hydrophobic surface of a substrate |
US7524800B2 (en) | 2007-06-12 | 2009-04-28 | Rhodia Inc. | Mono-, di- and polyol phosphate esters in personal care formulations |
CA2690602C (en) * | 2007-06-12 | 2017-02-28 | Rhodia Inc. | Hard surface cleaning composition with hydrophilizing agent and method for cleaning hard surfaces |
WO2008157197A1 (en) * | 2007-06-12 | 2008-12-24 | Rhodia Inc. | Mono-, di- and polyol alkoxylate phosphate esters in oral care formulations and methods for using same |
US7557072B2 (en) * | 2007-06-12 | 2009-07-07 | Rhodia Inc. | Detergent composition with hydrophilizing soil-release agent and methods for using same |
US7608571B2 (en) * | 2007-07-20 | 2009-10-27 | Rhodia Inc. | Method for recovering crude oil from a subterranean formation utilizing a polyphosphate ester |
US9028878B2 (en) | 2009-02-03 | 2015-05-12 | Microbion Corporation | Bismuth-thiols as antiseptics for biomedical uses, including treatment of bacterial biofilms and other uses |
JP5674684B2 (ja) | 2009-02-03 | 2015-02-25 | マイクロビオン コーポレーション | 上皮組織、急性および慢性創傷、細菌性バイオフィルムならびに他の適応症のための消毒剤としてのビスマス−チオール |
US9408393B2 (en) | 2010-02-03 | 2016-08-09 | Microbion Corporation | Bismuth-thiols as antiseptics for agricultural, industrial and other uses |
DE102009031724A1 (de) * | 2009-07-01 | 2011-01-20 | E.T.I. Gmbh | Zusammensetzung zur Verhinderung / Verringerung der Mikroben-induzierten Biokorrosion durch Sulfatreduzierende Bakterien (SRB) und andere Mikroorganismen |
CN101862273B (zh) * | 2010-05-25 | 2012-07-04 | 张颖 | 改性微化2-巯基吡啶氧化物锌盐的制备方法 |
KR101821833B1 (ko) * | 2010-02-03 | 2018-01-25 | 마이크로비온 코포레이션 | 세균 균막의 치료 및 다른 용도를 포함하는, 생의학적 용도를 위한 방부제로서 비스무트-티올 |
US8969261B2 (en) | 2010-02-12 | 2015-03-03 | Rhodia Operations | Rheology modifier compositions and methods of use |
US9080135B2 (en) | 2010-02-12 | 2015-07-14 | Rhodia Operations | Compositions with freeze thaw stability |
KR101864671B1 (ko) | 2010-02-12 | 2018-06-05 | 로디아 오퍼레이션스 | 유동성 개질제 폴리머 |
MX2012009491A (es) * | 2010-02-16 | 2012-08-31 | Procter & Gamble | Metodo para proporcionar un maximo control contra el mal olor y la irritacion. |
BR112013010241B1 (pt) * | 2010-10-28 | 2018-03-20 | The Procter & Gamble Company | Composições para cuidados pessoais que compreendem uma piritiona e um quelador de ferro |
CN103167894A (zh) * | 2010-10-28 | 2013-06-19 | 宝洁公司 | 通过乌头酸酶抑制来抑制微生物生长 |
US8980876B2 (en) | 2010-10-28 | 2015-03-17 | The Procter & Gamble Company | Inhibition of microbial growth by aconitase inhibition |
US9119796B2 (en) | 2011-02-28 | 2015-09-01 | The Gillette Company | Razor comprising a molded shaving aid composition comprising a pyrithione source |
CN104202987B (zh) | 2011-08-15 | 2017-09-01 | 宝洁公司 | 个人护理方法 |
MX2014013686A (es) | 2012-05-11 | 2015-07-06 | Procter & Gamble | Composiciones para la limpieza personal que comprenden piritiona de zinc. |
BR112015022842A2 (pt) | 2013-03-14 | 2017-07-18 | Procter & Gamble | composições de sabonete em barra contendo zinco piritiona e um complexo metal-óxido de piridina |
WO2014169464A1 (en) | 2013-04-18 | 2014-10-23 | The Procter & Gamble Company | Personal care compositions containing zinc pyrithione and zinc-phosphonate complex |
CN103242228A (zh) * | 2013-04-27 | 2013-08-14 | 南京工业大学 | 一种连续可控制备小粒径吡啶硫酮盐颗粒的方法 |
US20150250697A1 (en) | 2014-03-07 | 2015-09-10 | The Procter & Gamble Company | Personal Care Compositions and Methods of Making Same |
CN104212216B (zh) * | 2014-08-14 | 2018-05-01 | 河北科技大学 | 用于水性涂料杀菌防霉的吡啶硫酮锌超细颗粒及其制备方法 |
CA2970714C (en) | 2014-12-11 | 2023-10-17 | University Of Houston System | Adsorption of fluorinated anesthetics within the pores of molecular crystals |
WO2016179446A1 (en) | 2015-05-06 | 2016-11-10 | The Procter & Gamble Company | Methods of cosmetically treating skin conditions with a cosmetic personal cleansing composition |
WO2018017557A1 (en) | 2016-07-19 | 2018-01-25 | Behr Process Corporation | Antimicrobial paint composition and related methods |
KR102405516B1 (ko) * | 2017-06-20 | 2022-06-03 | 코오롱생명과학 주식회사 | 피리치온 염의 제조 방법 및 이를 이용하여 제조된 피리치온 염 |
CN107628993A (zh) * | 2017-08-30 | 2018-01-26 | 重庆中邦科技有限公司 | 一种均匀片晶吡啶硫酸酮锌的生产方法 |
EP3829307A4 (en) | 2018-07-31 | 2022-08-03 | Microbion Corporation | BISMUTH-THIOL COMPOSITIONS AND METHODS OF USE |
JP2021533194A (ja) | 2018-07-31 | 2021-12-02 | マイクロビオン コーポレーション | ビスマス・チオール組成物及び創傷を治療する方法 |
KR20210090640A (ko) * | 2018-11-12 | 2021-07-20 | 가부시키가이샤 시세이도 | 화장료 |
CN113905715A (zh) | 2019-06-28 | 2022-01-07 | 宝洁公司 | 光增强处理方法 |
Family Cites Families (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2809971A (en) * | 1955-11-22 | 1957-10-15 | Olin Mathieson | Heavy-metal derivatives of 1-hydroxy-2-pyridinethiones and method of preparing same |
US2786847A (en) * | 1956-07-23 | 1957-03-26 | Reilly Tar & Chem Corp | 2-mercapto, alkanol pyridine-nu-oxides |
US3590035A (en) * | 1967-12-21 | 1971-06-29 | Procter & Gamble | Process for preparing pyridine n-oxide carbanion salts |
US3773770A (en) * | 1968-09-30 | 1973-11-20 | Procter & Gamble | Process for preparing pyridine n-oxide carbanion salts and derivatives thereof |
US3589999A (en) * | 1968-10-25 | 1971-06-29 | Ionics | Deionization process |
US4345080A (en) * | 1980-02-07 | 1982-08-17 | The Procter & Gamble Company | Pyridinethione salts and hair care compositions |
US4323683A (en) * | 1980-02-07 | 1982-04-06 | The Procter & Gamble Company | Process for making pyridinethione salts |
DE3127863A1 (de) * | 1981-07-15 | 1983-02-03 | Rütgerswerke AG, 6000 Frankfurt | Verfahren zur herstellung des zinksalzes von 2-merkaptopyridin-n-oxid in einer leicht filtrierbaren aber gut suspendierbaren form |
EP0133914B1 (en) * | 1983-07-06 | 1988-06-15 | Kao Corporation | Finely powdered polyvalent metal salts of 2-mercaptopyridine-n-oxide, method for producing the same, and antibacterial compositions comprising the same |
DE3584595D1 (de) * | 1984-08-29 | 1991-12-12 | Kao Corp | Antimikrobische suspensionen und antimikrobische haarbehandlungsmittel. |
US4940578A (en) * | 1987-06-18 | 1990-07-10 | Kao Corporation | Hair preparation |
US5230833A (en) * | 1989-06-09 | 1993-07-27 | Nalco Chemical Company | Low sodium, low metals silica polishing slurries |
US5104645A (en) * | 1990-02-02 | 1992-04-14 | The Proctor & Gamble Company | Antidandruff shampoo compositions |
US5246489A (en) * | 1992-09-04 | 1993-09-21 | Olin Corporation | Process for generating copper pyrithione in-situ in a paint formulation |
US5696083A (en) * | 1992-11-10 | 1997-12-09 | Olin Corporation | Personal care composition containing pyrithione and polymyxin |
US5424435A (en) * | 1993-10-18 | 1995-06-13 | Olin Corporation | 1-hydroxy-6-substituted-2-pyridones |
US5540860A (en) * | 1994-02-28 | 1996-07-30 | Olin Corporation | Process for preparing copper pyrithione |
JP4235849B2 (ja) * | 1994-07-19 | 2009-03-11 | シナネン株式会社 | 耐変色性及び分散性に優れた防臭化粧料 |
US5614538A (en) * | 1994-12-05 | 1997-03-25 | Olin Corporation | Synergistic antimicrobial composition containing pyrithione and alcohol |
US6465015B1 (en) * | 1998-02-24 | 2002-10-15 | Arch Chemicals, Inc. | Sonic method of enhancing chemical reactions to provide uniform, non-agglomerated particles |
-
1998
- 1998-03-02 US US09/032,959 patent/US6017936A/en not_active Expired - Lifetime
- 1998-03-04 CN CNB988033496A patent/CN1136194C/zh not_active Expired - Lifetime
- 1998-03-04 WO PCT/US1998/004139 patent/WO1998041505A1/en active IP Right Grant
- 1998-03-04 EP EP98908886A patent/EP0983242A4/en not_active Ceased
- 1998-03-04 AU AU66808/98A patent/AU6680898A/en not_active Abandoned
- 1998-03-04 BR BR9808257-4A patent/BR9808257A/pt not_active Application Discontinuation
- 1998-03-04 ID IDW991006A patent/ID23513A/id unknown
- 1998-03-04 KR KR1019997008312A patent/KR100580134B1/ko not_active IP Right Cessation
- 1998-03-04 CA CA002283882A patent/CA2283882A1/en not_active Abandoned
- 1998-03-04 JP JP54054998A patent/JP4451499B2/ja not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
EP0983242A1 (en) | 2000-03-08 |
JP2001516359A (ja) | 2001-09-25 |
KR100580134B1 (ko) | 2006-05-16 |
CA2283882A1 (en) | 1998-09-24 |
CN1136194C (zh) | 2004-01-28 |
ID23513A (id) | 2000-04-27 |
US6017936A (en) | 2000-01-25 |
EP0983242A4 (en) | 2001-02-21 |
WO1998041505A1 (en) | 1998-09-24 |
CN1268941A (zh) | 2000-10-04 |
BR9808257A (pt) | 2000-05-16 |
AU6680898A (en) | 1998-10-12 |
KR20000076218A (ko) | 2000-12-26 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JP4451499B2 (ja) | ピリチオン塩粒子の製造方法 | |
JP4263249B2 (ja) | 非球状及び非板状のピリチオン塩 | |
US8709460B2 (en) | Chemical method of making a suspension, emulsion or dispersion of pyrithione particles | |
US6682724B2 (en) | Sonic method of enhancing chemical reactions to provide uniform, non-agglomerated particles | |
US6242007B1 (en) | Non-spherical and non-platelet forms of pyrithione salts and methods of making same | |
US6465015B1 (en) | Sonic method of enhancing chemical reactions to provide uniform, non-agglomerated particles | |
KR102405516B1 (ko) | 피리치온 염의 제조 방법 및 이를 이용하여 제조된 피리치온 염 | |
TW448157B (en) | Method for producing particles of pyrithione salts | |
MXPA00008233A (en) | Sonic method of enhancing chemical reactions | |
MXPA99009491A (en) | In-situ generation of zinc pyrithione |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20041209 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20080812 |
|
A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20081112 |
|
A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20081222 |
|
A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20081211 |
|
A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20090126 |
|
A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20090109 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20090123 |
|
A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20090223 |
|
A02 | Decision of refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A02 Effective date: 20090310 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A821 Effective date: 20090609 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20090701 |
|
A911 | Transfer to examiner for re-examination before appeal (zenchi) |
Free format text: JAPANESE INTERMEDIATE CODE: A911 Effective date: 20090917 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20091009 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20091113 |
|
TRDD | Decision of grant or rejection written | ||
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20100108 |
|
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 |
|
A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20100128 |
|
R150 | Certificate of patent or registration of utility model |
Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20130205 Year of fee payment: 3 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20130205 Year of fee payment: 3 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20140205 Year of fee payment: 4 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
EXPY | Cancellation because of completion of term |