JP4212480B2 - 化粧料 - Google Patents
化粧料 Download PDFInfo
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- JP4212480B2 JP4212480B2 JP2004000172A JP2004000172A JP4212480B2 JP 4212480 B2 JP4212480 B2 JP 4212480B2 JP 2004000172 A JP2004000172 A JP 2004000172A JP 2004000172 A JP2004000172 A JP 2004000172A JP 4212480 B2 JP4212480 B2 JP 4212480B2
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- powder
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- 239000002537 cosmetic Substances 0.000 title claims description 40
- 239000000843 powder Substances 0.000 claims description 94
- 239000002131 composite material Substances 0.000 claims description 39
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 24
- 229920000620 organic polymer Polymers 0.000 claims description 14
- 229920003169 water-soluble polymer Polymers 0.000 claims description 13
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 12
- 239000000377 silicon dioxide Substances 0.000 claims description 12
- -1 sericite Chemical compound 0.000 claims description 11
- 229920001577 copolymer Polymers 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 6
- 229910052588 hydroxylapatite Inorganic materials 0.000 claims description 5
- XYJRXVWERLGGKC-UHFFFAOYSA-D pentacalcium;hydroxide;triphosphate Chemical compound [OH-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O XYJRXVWERLGGKC-UHFFFAOYSA-D 0.000 claims description 5
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 4
- 239000001856 Ethyl cellulose Substances 0.000 claims description 4
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 4
- 229920001249 ethyl cellulose Polymers 0.000 claims description 4
- 235000019325 ethyl cellulose Nutrition 0.000 claims description 4
- 229950004354 phosphorylcholine Drugs 0.000 claims description 4
- PYJNAPOPMIJKJZ-UHFFFAOYSA-N phosphorylcholine chloride Chemical compound [Cl-].C[N+](C)(C)CCOP(O)(O)=O PYJNAPOPMIJKJZ-UHFFFAOYSA-N 0.000 claims description 4
- 150000003839 salts Chemical class 0.000 claims description 4
- 229910052582 BN Inorganic materials 0.000 claims description 3
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 3
- 108010035532 Collagen Proteins 0.000 claims description 3
- 102000008186 Collagen Human genes 0.000 claims description 3
- 230000005540 biological transmission Effects 0.000 claims description 3
- 229920001436 collagen Polymers 0.000 claims description 3
- 229960004667 ethyl cellulose Drugs 0.000 claims description 3
- 229910000000 metal hydroxide Inorganic materials 0.000 claims description 3
- 150000004692 metal hydroxides Chemical class 0.000 claims description 3
- 229910044991 metal oxide Inorganic materials 0.000 claims description 3
- 150000004706 metal oxides Chemical group 0.000 claims description 3
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 claims description 2
- FHVDTGUDJYJELY-UHFFFAOYSA-N 6-{[2-carboxy-4,5-dihydroxy-6-(phosphanyloxy)oxan-3-yl]oxy}-4,5-dihydroxy-3-phosphanyloxane-2-carboxylic acid Chemical compound O1C(C(O)=O)C(P)C(O)C(O)C1OC1C(C(O)=O)OC(OP)C(O)C1O FHVDTGUDJYJELY-UHFFFAOYSA-N 0.000 claims description 2
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 2
- 229920002101 Chitin Polymers 0.000 claims description 2
- 229920001661 Chitosan Polymers 0.000 claims description 2
- 235000017788 Cydonia oblonga Nutrition 0.000 claims description 2
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 claims description 2
- 229920001503 Glucan Polymers 0.000 claims description 2
- 229920002683 Glycosaminoglycan Polymers 0.000 claims description 2
- 229920002907 Guar gum Polymers 0.000 claims description 2
- 229920002472 Starch Polymers 0.000 claims description 2
- 230000002378 acidificating effect Effects 0.000 claims description 2
- 229940072056 alginate Drugs 0.000 claims description 2
- 235000010443 alginic acid Nutrition 0.000 claims description 2
- 229920000615 alginic acid Polymers 0.000 claims description 2
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 2
- 235000010418 carrageenan Nutrition 0.000 claims description 2
- 239000000679 carrageenan Substances 0.000 claims description 2
- 229920001525 carrageenan Polymers 0.000 claims description 2
- 229940113118 carrageenan Drugs 0.000 claims description 2
- 239000000665 guar gum Substances 0.000 claims description 2
- 235000010417 guar gum Nutrition 0.000 claims description 2
- 229960002154 guar gum Drugs 0.000 claims description 2
- 229920000591 gum Polymers 0.000 claims description 2
- 229920002674 hyaluronan Polymers 0.000 claims description 2
- 229960003160 hyaluronic acid Drugs 0.000 claims description 2
- ORUIBWPALBXDOA-UHFFFAOYSA-L magnesium fluoride Chemical compound [F-].[F-].[Mg+2] ORUIBWPALBXDOA-UHFFFAOYSA-L 0.000 claims description 2
- 229910001635 magnesium fluoride Inorganic materials 0.000 claims description 2
- 229920000609 methyl cellulose Polymers 0.000 claims description 2
- 239000001923 methylcellulose Substances 0.000 claims description 2
- 235000010981 methylcellulose Nutrition 0.000 claims description 2
- 239000010445 mica Substances 0.000 claims description 2
- 229910052618 mica group Inorganic materials 0.000 claims description 2
- 239000001814 pectin Substances 0.000 claims description 2
- 235000010987 pectin Nutrition 0.000 claims description 2
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- 235000019698 starch Nutrition 0.000 claims description 2
- 239000000454 talc Substances 0.000 claims description 2
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- 229940082509 xanthan gum Drugs 0.000 claims description 2
- 239000011787 zinc oxide Substances 0.000 claims description 2
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 2
- 229920003229 poly(methyl methacrylate) Polymers 0.000 claims 1
- 239000004926 polymethyl methacrylate Substances 0.000 claims 1
- 241000894007 species Species 0.000 claims 1
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- 239000000203 mixture Substances 0.000 description 6
- 239000002932 luster Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 4
- 239000011248 coating agent Substances 0.000 description 4
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- ZSZRUEAFVQITHH-UHFFFAOYSA-N 2-(2-methylprop-2-enoyloxy)ethyl 2-(trimethylazaniumyl)ethyl phosphate Chemical compound CC(=C)C(=O)OCCOP([O-])(=O)OCC[N+](C)(C)C ZSZRUEAFVQITHH-UHFFFAOYSA-N 0.000 description 3
- SOGAXMICEFXMKE-UHFFFAOYSA-N alpha-Methyl-n-butyl acrylate Natural products CCCCOC(=O)C(C)=C SOGAXMICEFXMKE-UHFFFAOYSA-N 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
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- 239000000049 pigment Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 229920000178 Acrylic resin Polymers 0.000 description 2
- 239000004925 Acrylic resin Substances 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 239000004677 Nylon Substances 0.000 description 2
- 102000016611 Proteoglycans Human genes 0.000 description 2
- 108010067787 Proteoglycans Proteins 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 230000001771 impaired effect Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 229920001778 nylon Polymers 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- LNAZSHAWQACDHT-XIYTZBAFSA-N (2r,3r,4s,5r,6s)-4,5-dimethoxy-2-(methoxymethyl)-3-[(2s,3r,4s,5r,6r)-3,4,5-trimethoxy-6-(methoxymethyl)oxan-2-yl]oxy-6-[(2r,3r,4s,5r,6r)-4,5,6-trimethoxy-2-(methoxymethyl)oxan-3-yl]oxyoxane Chemical compound CO[C@@H]1[C@@H](OC)[C@H](OC)[C@@H](COC)O[C@H]1O[C@H]1[C@H](OC)[C@@H](OC)[C@H](O[C@H]2[C@@H]([C@@H](OC)[C@H](OC)O[C@@H]2COC)OC)O[C@@H]1COC LNAZSHAWQACDHT-XIYTZBAFSA-N 0.000 description 1
- 241001237961 Amanita rubescens Species 0.000 description 1
- 241000258957 Asteroidea Species 0.000 description 1
- 241000251730 Chondrichthyes Species 0.000 description 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 239000004909 Moisturizer Substances 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- 241000276425 Xiphophorus maculatus Species 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 238000000149 argon plasma sintering Methods 0.000 description 1
- 108010045569 atelocollagen Proteins 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- 210000000845 cartilage Anatomy 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
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Landscapes
- Cosmetics (AREA)
Description
凸レンズ型架橋メタクリル酸メチル末100g(積水化成品製、テクポリマーL−XC−F005M)を板状シリカ末(水澤化学製、シルリーフ)100gとヘンシェルミキサーで高速混合させた上に2−メタクリロイルオキシエチルホスホリルコリン・メタクリル酸ブチル共重合体5重量%水溶液を100g噴霧添加し、均一に分散させた後、減圧下で60℃加熱し揮発分を除去し、複合機能粉体1を得た。
球状12ナイロン粉末60g(atochem社製、オルガゾール2002)および窒化ホウ素30g(水島合金鉄製、セラムブランシュSHP−4)をらいかい機で混合し、鮫軟骨抽出のプロテオグリカン乾燥物10gと水500gを加え、ホモミキサーで分散させ、80℃で2時間撹拌した。その後、水をろ過し、固形分を乾燥、粉砕して複合機能粉体2を得た。
球状ポリアクリル酸エチル45g(松本油脂製、マイクロスフェアー)に硫酸バリウム(堺化学工業製、板状硫酸バリウム)65gを混合した粉体に水溶性コラーゲン液(アテロコラーゲン1重量%水溶液)100gを添加しながらスプレードライ方式で加えて、混合乾燥を行い複合機能粉体3を得た。
凸レンズ型架橋メタクリル酸メチル末100g(積水化成品製、テクポリマーL−XC−F005M)を板状シリカ末(水澤化学製、シルリーフ)100gとヘンシェルミキサーで高速混合し、比較複合粉体1を得た。
凸レンズ型架橋メタクリル酸メチル末100g(積水化成品製、テクポリマーL−XC−F005M)に2−メタクリロイルオキシエチルホスホリルコリン・メタクリル酸ブチル共重合体5重量%水溶液を100g噴霧添加し、均一に分散させた後、減圧下で60℃加熱し揮発分を除去し、比較複合粉体2を得た。
板状シリカ末(水澤化学製、シルリーフ)100gに2−メタクリロイルオキシエチルホスホリルコリン・メタクリル酸ブチル共重合体5重量%水溶液を100g噴霧添加し、均一に分散させた後、減圧下で60℃加熱し揮発分を除去し、比較複合粉体3を得た。
<肌のはり感>
10人の専門パネラーにより官能評価を行い、(1)の評価基準を用いて7段階に評価し、その平均値を(2)に示す基準で評価した。
(1)
7点:非常に良い
6点:良い
5点:やや良い
4点:普通
3点:やや悪い
2点:悪い
1点:非常に悪い
(2)
◎:6点以上
○:4点以上6点未満
△:3点以上4点未満
×:3点未満
<しわ隠し効果>
10人の専門パネラーにより官能評価を行い、次の基準で示した。
〇:8人以上が良いと感じた
△:4〜7人が良いと感じた
×:4人未満が良いと感じた
<肌のはり感>
10人の専門パネラーにより塗布から4時間後の官能評価を行い、(1)の評価基準を用いて7段階に評価し、その平均値を(2)に示す基準で評価した。
(1)
7点:非常に良い
6点:良い
5点:やや良い
4点:普通
3点:やや悪い
2点:悪い
1点:非常に悪い
(2)
◎:6点以上
○:4点以上6点未満
△:3点以上4点未満
×:3点未満
<しわ隠し効果>
肌のはり感の評価と同様に10人の専門パネラーにより塗布から4時間後の官能評価を行い、次の基準で示した。
〇:8人以上が良いと感じた
△:4〜7人が良いと感じた
×:4人未満が良いと感じた
Claims (10)
- 形状が、球状、紡錘状、半球状、凸レンズ状、ラグビーボール状の何れかである光透過性有機高分子粉体を、形状が板状の無機粉体から選ばれる1種又は2種以上の粉体及び水溶性高分子で被覆することにより、光の透過性と拡散反射性を高めた複合機能粉体を0.01〜25重量%含有する化粧料。
- 光透過性有機高分子粉体の形状が凸レンズ状であることを特徴とする請求項1記載の化粧料。
- 光透過性有機高分子粉体の平均粒子径が1〜50μmであることを特徴とする請求項1〜2のいずれかに記載の化粧料。
- 光透過性有機高分子粉体が架橋ポリメタクリル酸メチルであることを特徴とする請求項1〜3のいずれかに記載の化粧料。
- 板状の無機粉体が金属酸化物、金属水酸化物、金属酸化物又は金属水酸化物の水和物、無機塩、及び、これらの複合体から選ばれる1種又は2種以上のものであることを特徴とする請求項1〜4のいずれかに記載の化粧料。
- 板状の無機粉体の屈折率が2.3以下であることを特徴とする請求項1〜5のいずれかに記載の化粧料。
- 板状の無機粉体が、シリカ、アルミナ、ジルコニア、セリサイト、酸化亜鉛、タルク、マイカ、水酸化アルミニウム、ハイドロキシアパタイト、窒化ホウ素、炭酸カルシウム、フツ化マグネシウム、硫酸バリウムから選ばれる1種又は2種以上のものであることを特徴とする請求項1〜6のいずれかに記載の化粧料。
- 板状の無機粉体がシリカであることを特徴とする請求項1〜7のいずれかに記載の化粧料。
- 水溶性高分子の成分が、ヒアルロン酸およびその塩または誘導体、酸性ムコ多糖類、コラーゲンおよびその誘導体、プロテオグリカンおよびその誘導体、ホスホリルコリン/アクリル誘導体共重合体、カルボキシルビニルポリマー、カルボキシルメチルセルロース、カルボキシルエチルセルロース、メチルセルロース、エチルセルロース、キサンタンガム、アルギン酸塩、グルカン、カラギーナン、クインスシードガム、ペクチン、グアガム、デンプン、キチン、キトサンから選ばれる1
種又は2 種以上であることを特徴とする請求項1〜8のいずれかに記載の化粧料。 - 水溶性高分子の成分が、2−メタクリロイルオキシエチルホスホリルコリン・メタクリルブチル共重合体であることを特徴とする請求項1〜9のいずれかに記載の化粧料。
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JP4212480B2 true JP4212480B2 (ja) | 2009-01-21 |
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Cited By (1)
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---|---|---|---|---|
US7939841B2 (en) | 2004-12-31 | 2011-05-10 | Lg Electronics Inc. | High output light emitting diode and method for fabricating the same |
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JP4920962B2 (ja) * | 2005-05-20 | 2012-04-18 | 大東化成工業株式会社 | 複合有機粉末とそれを用いた製品 |
WO2007010623A1 (ja) * | 2005-07-22 | 2007-01-25 | Phg Corporation | 新規なポリペプチド及びその製造方法 |
JP2007284483A (ja) * | 2006-04-13 | 2007-11-01 | Daito Kasei Kogyo Kk | 吸湿性顔料およびそれを含有する化粧料 |
US8529923B2 (en) | 2009-08-04 | 2013-09-10 | Chanel Parfums Beaute | Cosmetic composition based on substantially hemispherical particles |
EP2643397B1 (en) | 2010-11-23 | 2014-09-10 | Unilever N.V. | Composite particles and compositions with composite particles |
CN103505376B (zh) * | 2012-06-20 | 2019-04-30 | 株式会社爱茉莉太平洋 | 用于阻断紫外线的有机、无机复合粉体及含有该复合粉体的化妆品组合物 |
KR101767207B1 (ko) | 2012-11-30 | 2017-08-11 | (주)아모레퍼시픽 | 생체친화성 고분자로 코팅된 무기분체 및 이를 함유하는 화장료 조성물 |
JP6219606B2 (ja) * | 2013-06-06 | 2017-10-25 | ポーラ化成工業株式会社 | 口唇化粧料 |
JP7236349B2 (ja) * | 2019-08-16 | 2023-03-09 | 信越化学工業株式会社 | 分散性粉体及び化粧料 |
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US7939841B2 (en) | 2004-12-31 | 2011-05-10 | Lg Electronics Inc. | High output light emitting diode and method for fabricating the same |
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