JP3611600B2 - 活性炭の製造方法 - Google Patents
活性炭の製造方法 Download PDFInfo
- Publication number
- JP3611600B2 JP3611600B2 JP20453694A JP20453694A JP3611600B2 JP 3611600 B2 JP3611600 B2 JP 3611600B2 JP 20453694 A JP20453694 A JP 20453694A JP 20453694 A JP20453694 A JP 20453694A JP 3611600 B2 JP3611600 B2 JP 3611600B2
- Authority
- JP
- Japan
- Prior art keywords
- activation
- carbonization
- temperature
- activated carbon
- ion exchanger
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims description 44
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 238000000034 method Methods 0.000 claims description 23
- 230000004913 activation Effects 0.000 claims description 19
- 150000002500 ions Chemical class 0.000 claims description 17
- 230000008569 process Effects 0.000 claims description 14
- 238000003763 carbonization Methods 0.000 claims description 13
- 229910052760 oxygen Inorganic materials 0.000 claims description 9
- 230000003647 oxidation Effects 0.000 claims description 8
- 238000007254 oxidation reaction Methods 0.000 claims description 8
- 239000012298 atmosphere Substances 0.000 claims description 7
- 239000011347 resin Substances 0.000 claims description 7
- 229920005989 resin Polymers 0.000 claims description 7
- 239000001301 oxygen Substances 0.000 claims description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 5
- 150000001768 cations Chemical class 0.000 claims description 5
- 230000001590 oxidative effect Effects 0.000 claims description 5
- 229920001577 copolymer Polymers 0.000 claims description 4
- 238000000197 pyrolysis Methods 0.000 claims description 4
- 238000010000 carbonizing Methods 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000001994 activation Methods 0.000 description 17
- 229910052799 carbon Inorganic materials 0.000 description 9
- 239000000463 material Substances 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 230000004580 weight loss Effects 0.000 description 5
- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 4
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 4
- 239000004005 microsphere Substances 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- 229910052717 sulfur Inorganic materials 0.000 description 4
- 239000011593 sulfur Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 238000005054 agglomeration Methods 0.000 description 3
- 230000002776 aggregation Effects 0.000 description 3
- 238000002485 combustion reaction Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000001179 sorption measurement Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 230000003213 activating effect Effects 0.000 description 2
- 239000003245 coal Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 238000009656 pre-carbonization Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000011282 treatment Methods 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 229920000049 Carbon (fiber) Polymers 0.000 description 1
- 235000013162 Cocos nucifera Nutrition 0.000 description 1
- 244000060011 Cocos nucifera Species 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000005539 carbonized material Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 235000019645 odor Nutrition 0.000 description 1
- 239000003415 peat Substances 0.000 description 1
- 238000005554 pickling Methods 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006277 sulfonation reaction Methods 0.000 description 1
- 125000000542 sulfonic acid group Chemical group 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/336—Preparation characterised by gaseous activating agents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10555693A | 1993-08-12 | 1993-08-12 | |
US105556 | 2002-03-25 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH07165407A JPH07165407A (ja) | 1995-06-27 |
JP3611600B2 true JP3611600B2 (ja) | 2005-01-19 |
Family
ID=22306493
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP20453694A Expired - Lifetime JP3611600B2 (ja) | 1993-08-12 | 1994-08-05 | 活性炭の製造方法 |
Country Status (6)
Country | Link |
---|---|
JP (1) | JP3611600B2 (it) |
KR (1) | KR950005742A (it) |
CA (1) | CA2128979A1 (it) |
FR (1) | FR2708922B1 (it) |
GB (1) | GB2280898B (it) |
IT (1) | IT1273678B (it) |
Families Citing this family (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19752593C5 (de) * | 1997-11-27 | 2005-02-17 | Helsa-Werke Helmut Sandler Gmbh & Co. Kg | Verfahren zur Herstellung von Aktivkohle aus Polymeren mit aromatischen Kernen |
US6143835A (en) * | 1998-04-03 | 2000-11-07 | Solutia Inc. | Polyacrylonitrile polymer treatment |
US6277933B1 (en) | 1998-04-03 | 2001-08-21 | Solutia Inc. | Polyacrylonitrile particles by surfmer polymerization and sodium removal by chemical exchange |
DE19912154C5 (de) * | 1999-03-17 | 2007-02-01 | Carbotex Produktions-Und Veredelungsbetriebe Gmbh | Verfahren zur Herstellung von geformter Aktivkohle |
DE19912153B4 (de) | 1999-03-18 | 2004-08-19 | Carbotex Produktions-Und Veredelungsbetriebe Gmbh | Verfahren zur Herstellung von geformten Hochleistungsadsorbenzien |
DE19930732A1 (de) * | 1999-07-05 | 2001-01-18 | Sandler Helmut Helsa Werke | Verfahren zur gesteuerten Herstellung von Kugelaktivkohle |
JP3777123B2 (ja) | 2000-04-28 | 2006-05-24 | ブリュッヒャー ゲゼルシャフト ミット ベシュレンクテル ハフツング | 球状活性炭を製造する方法 |
DE50012022D1 (de) * | 2000-05-24 | 2006-03-30 | Carbotex Produktions Und Vered | Verfahren zur herstellung von geformter aktivkohle |
GB0019417D0 (en) | 2000-08-09 | 2000-09-27 | Mat & Separations Tech Int Ltd | Mesoporous carbons |
US8591855B2 (en) | 2000-08-09 | 2013-11-26 | British American Tobacco (Investments) Limited | Porous carbons |
CN1280189C (zh) * | 2001-04-17 | 2006-10-18 | Lg化学株式会社 | 球形碳及其制备方法 |
DE10148286A1 (de) * | 2001-09-29 | 2003-04-17 | Sandler Helmut Helsa Werke | Verfahren zur Herstellung von Aktivkohle mit einer definierten Porenstruktur |
US7651974B2 (en) | 2002-11-01 | 2010-01-26 | Kureha Chemical Industry Co., Ltd. | Adsorbent for oral administration |
CN1615908B (zh) | 2003-10-22 | 2011-09-28 | 株式会社吴羽 | 口服给药用吸附剂、以及肾病治疗或预防剂、和肝病治疗或预防剂 |
TWI370012B (en) | 2004-04-02 | 2012-08-11 | Kureha Corp | Adsorbent for oral administration, and agent for treating or preventing renal or liver disease |
TWI370013B (en) | 2004-04-02 | 2012-08-11 | Kureha Corp | Adsorbent for oral administration, and agent for treating or preventing renal or liver disease |
CN1304285C (zh) * | 2004-05-26 | 2007-03-14 | 王浦林 | 多微孔炭的制备方法及该方法所用的设备 |
GB0506278D0 (en) | 2005-03-29 | 2005-05-04 | British American Tobacco Co | Porous carbon materials and smoking articles and smoke filters therefor incorporating such materials |
DE102005062160A1 (de) * | 2005-12-19 | 2007-06-21 | BLüCHER GMBH | Aktivkohle für die medizinische Verwendung |
CA2665052C (en) * | 2006-10-09 | 2014-12-09 | British American Tobacco (Investments) Limited | Making discrete solid particles of polymeric material |
JP5312357B2 (ja) * | 2010-01-22 | 2013-10-09 | 東北電力株式会社 | 一酸化窒素用吸着材の製造方法 |
CN109896512A (zh) * | 2017-12-08 | 2019-06-18 | 中国科学院大连化学物理研究所 | 一种低成本制备离子交换树脂基多孔炭材料的方法 |
KR102370959B1 (ko) * | 2019-01-24 | 2022-03-07 | 한국화학연구원 | 수지 기반 활성탄의 제조방법 및 이에 따라 제조된 활성탄 |
KR102595632B1 (ko) * | 2021-11-12 | 2023-10-27 | 한국화학연구원 | 초고비표면적 구형 활성탄의 제조방법 및 이에 따라 제조된 활성탄 |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DD63768A (it) * | ||||
JPS5350088A (en) * | 1976-10-19 | 1978-05-08 | Sumitomo Chem Co Ltd | Production of spherical activated carbon |
JPS565313A (en) * | 1979-06-26 | 1981-01-20 | Kureha Chem Ind Co Ltd | Detoxificating spherical active carbon and preparing the same |
JPS5489010A (en) * | 1977-12-27 | 1979-07-14 | Kureha Chem Ind Co Ltd | Spherical activated charcoal antidote |
JPS5510971A (en) * | 1978-07-12 | 1980-01-25 | Sumitomo Chemical Co | Blood purifying device |
JPS61187698A (ja) * | 1985-02-15 | 1986-08-21 | 株式会社日立製作所 | 放射性イオン交換樹脂の処理方法及び装置 |
US4839331A (en) * | 1988-01-29 | 1989-06-13 | Rohm And Haas Company | Carbonaceous adsorbents from pyrolyzed polysulfonated polymers |
DE4304026B4 (de) * | 1992-02-28 | 2005-02-17 | Mhb Filtration Gmbh & Co. Kg | Verfahren zur Entsorgung von verbrauchten Ionenaustauschern |
DE4328219A1 (de) * | 1993-08-21 | 1995-02-23 | Hasso Von Bluecher | Aktivkohlekügelchen aus Ionenaustauschern |
-
1994
- 1994-07-25 IT ITMI941575A patent/IT1273678B/it active IP Right Grant
- 1994-07-27 CA CA002128979A patent/CA2128979A1/en not_active Abandoned
- 1994-08-01 KR KR1019940019011A patent/KR950005742A/ko not_active Application Discontinuation
- 1994-08-05 JP JP20453694A patent/JP3611600B2/ja not_active Expired - Lifetime
- 1994-08-09 GB GB9416022A patent/GB2280898B/en not_active Expired - Fee Related
- 1994-08-10 FR FR9409914A patent/FR2708922B1/fr not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
GB9416022D0 (en) | 1994-09-28 |
GB2280898B (en) | 1997-07-16 |
CA2128979A1 (en) | 1995-02-13 |
FR2708922B1 (fr) | 1996-09-06 |
GB2280898A (en) | 1995-02-15 |
KR950005742A (ko) | 1995-03-20 |
ITMI941575A1 (it) | 1996-01-25 |
FR2708922A1 (fr) | 1995-02-17 |
JPH07165407A (ja) | 1995-06-27 |
ITMI941575A0 (it) | 1994-07-25 |
IT1273678B (it) | 1997-07-09 |
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