JP2024509153A - Ｍｗｗ骨格型の分子ふるいを合成する方法 - Google Patents

Ｍｗｗ骨格型の分子ふるいを合成する方法 Download PDF

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JP2024509153A
JP2024509153A JP2023553242A JP2023553242A JP2024509153A JP 2024509153 A JP2024509153 A JP 2024509153A JP 2023553242 A JP2023553242 A JP 2023553242A JP 2023553242 A JP2023553242 A JP 2023553242A JP 2024509153 A JP2024509153 A JP 2024509153A
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hydroxide
molecular sieve
pdda
synthesis mixture
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JPWO2022184759A5 (https=
JP2024509153A5 (https=
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シーナー サルティピ
マーク エイチ アントニス
アーロン ダブリュー ピーターズ
スコット ジェイ ウェイゲル
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エクソンモービル ケミカル パテンツ インコーポレイテッド
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/615—100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/617—500-1000 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/633—Pore volume less than 0.5 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/70—Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
    • C07C2/54—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition of unsaturated hydrocarbons to saturated hydrocarbons or to hydrocarbons containing a six-membered aromatic ring with no unsaturation outside the aromatic ring
    • C07C2/64—Addition to a carbon atom of a six-membered aromatic ring
    • C07C2/66—Catalytic processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/05—Nuclear magnetic resonance [NMR]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/30—Scanning electron microscopy; Transmission electron microscopy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/86—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by NMR- or ESR-data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/14—Pore volume

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
JP2023553242A 2021-03-03 2022-03-02 Ｍｗｗ骨格型の分子ふるいを合成する方法 Pending JP2024509153A (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US202163155990P 2021-03-03 2021-03-03
US63/155,990 2021-03-03
EP21167971 2021-04-13
EP21167971.7 2021-04-13
PCT/EP2022/055235 WO2022184759A1 (en) 2021-03-03 2022-03-02 Method of synthesizing a molecular sieve of mww framework type

Publications (3)

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JP2024509153A true JP2024509153A (ja) 2024-02-29
JPWO2022184759A5 JPWO2022184759A5 (https=) 2025-03-07
JP2024509153A5 JP2024509153A5 (https=) 2025-03-07

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US (1) US20240101435A1 (https=)
EP (1) EP4301700A1 (https=)
JP (1) JP2024509153A (https=)
CN (1) CN117043108B (https=)
CA (1) CA3207884A1 (https=)
WO (1) WO2022184759A1 (https=)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN119143147B (zh) * 2023-06-15 2026-04-21 中国石油化工股份有限公司 P修饰的金属掺杂mww分子筛及其制备方法和应用

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009544567A (ja) * 2006-07-28 2009-12-17 エクソンモービル・ケミカル・パテンツ・インク Ｍｃｍ−２２族モレキュラーシーブ組成物、その合成法及び炭化水素変換におけるその使用法
JP2019099458A (ja) * 2017-11-28 2019-06-24 国立研究開発法人産業技術総合研究所 Ｍｗｗ型ゼオライト及びその製造方法、並びにクラッキング触媒
CN111977663A (zh) * 2020-08-25 2020-11-24 西北大学 一种多级孔道结构沸石分子筛及其制备方法和应用
JP2021031383A (ja) * 2019-08-14 2021-03-01 コリア ユニバーシティ リサーチ アンド ビジネス ファウンデーションＫｏｒｅａ Ｕｎｉｖｅｒｓｉｔｙ Ｒｅｓｅａｒｃｈ Ａｎｄ Ｂｕｓｉｎｅｓｓ Ｆｏｕｎｄａｔｉｏｎ 単純焼成を用いたナノ板状ゼオライトの製造方法及びこれによって製造されたナノ板状ゼオライト粒子

Family Cites Families (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3117135A1 (de) 1981-04-30 1982-11-18 Bayer Ag, 5090 Leverkusen Kristallines alumosilicat, verfahren zu dessen herstellung sowie dessen verwendung zur katalytischen umwandlung von methanol und/oder dimethylether in kohlenwasserstoffe
US4826667A (en) 1986-01-29 1989-05-02 Chevron Research Company Zeolite SSZ-25
US4954325A (en) 1986-07-29 1990-09-04 Mobil Oil Corp. Composition of synthetic porous crystalline material, its synthesis and use
IT1205681B (it) 1987-05-26 1989-03-31 Eniricerche Spa Materiale sintetico cristallino poroso contenente ossidi di silicio e boro
US5250277A (en) 1991-01-11 1993-10-05 Mobil Oil Corp. Crystalline oxide material
US5236575A (en) 1991-06-19 1993-08-17 Mobil Oil Corp. Synthetic porous crystalline mcm-49, its synthesis and use
US5827491A (en) 1993-04-26 1998-10-27 Mobil Oil Corporation Process for preparing the synthetic porous crystalline material MCM-56
US5362697A (en) 1993-04-26 1994-11-08 Mobil Oil Corp. Synthetic layered MCM-56, its synthesis and use
ES2124154B1 (es) 1995-11-08 1999-12-01 Univ Politecnica De Valencia C Metodo de preparaciion y propiedades cataliticas de un solido microporoso con alta superficie externa.
ES2105982B1 (es) 1995-11-23 1998-07-01 Consejo Superior Investigacion Zeolita itq-1
CN1311757A (zh) 1998-07-29 2001-09-05 埃克森化学专利公司 制备分子筛的方法
US6756030B1 (en) 2003-03-21 2004-06-29 Uop Llc Crystalline aluminosilicate zeolitic composition: UZM-8
US7713513B2 (en) 2003-03-21 2010-05-11 Uop Llc High silica zeolites: UZM-8HS
ES2246704B1 (es) 2004-05-28 2007-06-16 Universidad Politecnica De Valencia Zeolita itq-30.
CN101384367B (zh) 2006-02-14 2012-05-30 埃克森美孚化学专利公司 一种制造mcm-22族分子筛的方法
BRPI0713674A2 (pt) 2006-07-28 2012-10-23 Exxonmobil Chemical Patents Inc. formulações farmarcêuticas e composições de um antagonista seletivo cxcr2 ou cxcr1 e métodos para o uso do mesmo visando o tratamento de distúrbios inflamatórios
KR101097536B1 (ko) 2006-07-28 2011-12-22 엑손모빌 케미칼 패턴츠 인코포레이티드 신규 분자체 조성물, 이의 제조 방법 및 이의 사용 방법
DE102008003103A1 (de) 2008-01-01 2009-07-02 Lts Lohmann Therapie-Systeme Ag Einweginjektor mit zweikolbigem Zweikammersystem
RU2509055C2 (ru) 2008-07-28 2014-03-10 Эксонмобил Кемикэл Пейтентс Инк. Новая молекулярно-ситовая композиция емм-12, способы ее получения и применения
WO2010021795A1 (en) 2008-07-28 2010-02-25 Exxonmobil Chemical Patents Inc. A novel molecular sieve composition emm-12, a method of making and a process of using the same
CN103827033B (zh) 2011-09-16 2016-05-11 埃克森美孚化学专利公司 改进的mcm-56制造方法
WO2015112293A1 (en) 2014-01-27 2015-07-30 Exxonbobil Chemical Patents Inc. Synthesis of molecular sieves having mww framework structure
US10173903B2 (en) * 2014-06-16 2019-01-08 University Of Houston System Zeolite compositions and methods for tailoring zeolite crystal habits with growth modifiers

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009544567A (ja) * 2006-07-28 2009-12-17 エクソンモービル・ケミカル・パテンツ・インク Ｍｃｍ−２２族モレキュラーシーブ組成物、その合成法及び炭化水素変換におけるその使用法
JP2019099458A (ja) * 2017-11-28 2019-06-24 国立研究開発法人産業技術総合研究所 Ｍｗｗ型ゼオライト及びその製造方法、並びにクラッキング触媒
JP2021031383A (ja) * 2019-08-14 2021-03-01 コリア ユニバーシティ リサーチ アンド ビジネス ファウンデーションＫｏｒｅａ Ｕｎｉｖｅｒｓｉｔｙ Ｒｅｓｅａｒｃｈ Ａｎｄ Ｂｕｓｉｎｅｓｓ Ｆｏｕｎｄａｔｉｏｎ 単純焼成を用いたナノ板状ゼオライトの製造方法及びこれによって製造されたナノ板状ゼオライト粒子
CN111977663A (zh) * 2020-08-25 2020-11-24 西北大学 一种多级孔道结构沸石分子筛及其制备方法和应用

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
YIN XIAOYAN ET AL., CATALYSIS COMMUNICATIONS, vol. 43, JPN6026008414, 2014, pages 218 - 222, ISSN: 0005807908 *

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EP4301700A1 (en) 2024-01-10
WO2022184759A1 (en) 2022-09-09
US20240101435A1 (en) 2024-03-28
CN117043108A (zh) 2023-11-10
CA3207884A1 (en) 2022-09-09
CN117043108B (zh) 2026-02-13

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