CA3207884A1 - Method of synthesizing a molecular sieve of mww framework type - Google Patents
Method of synthesizing a molecular sieve of mww framework type Download PDFInfo
- Publication number
- CA3207884A1 CA3207884A1 CA3207884A CA3207884A CA3207884A1 CA 3207884 A1 CA3207884 A1 CA 3207884A1 CA 3207884 A CA3207884 A CA 3207884A CA 3207884 A CA3207884 A CA 3207884A CA 3207884 A1 CA3207884 A1 CA 3207884A1
- Authority
- CA
- Canada
- Prior art keywords
- molecular sieve
- source
- synthesis mixture
- hydroxide
- pdda
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
- C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
- B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/61—Surface area
- B01J35/615—100-500 m2/g
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/61—Surface area
- B01J35/617—500-1000 m2/g
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/63—Pore volume
- B01J35/633—Pore volume less than 0.5 ml/g
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/70—Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
- C07C2/54—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition of unsaturated hydrocarbons to saturated hydrocarbons or to hydrocarbons containing a six-membered aromatic ring with no unsaturation outside the aromatic ring
- C07C2/64—Addition to a carbon atom of a six-membered aromatic ring
- C07C2/66—Catalytic processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
- B01J2235/05—Nuclear magnetic resonance [NMR]
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
- B01J2235/15—X-ray diffraction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
- B01J2235/30—Scanning electron microscopy; Transmission electron microscopy
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/86—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by NMR- or ESR-data
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/14—Pore volume
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Catalysts (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US202163155990P | 2021-03-03 | 2021-03-03 | |
| US63/155,990 | 2021-03-03 | ||
| EP21167971 | 2021-04-13 | ||
| EP21167971.7 | 2021-04-13 | ||
| PCT/EP2022/055235 WO2022184759A1 (en) | 2021-03-03 | 2022-03-02 | Method of synthesizing a molecular sieve of mww framework type |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA3207884A1 true CA3207884A1 (en) | 2022-09-09 |
Family
ID=80735780
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA3207884A Pending CA3207884A1 (en) | 2021-03-03 | 2022-03-02 | Method of synthesizing a molecular sieve of mww framework type |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US20240101435A1 (https=) |
| EP (1) | EP4301700A1 (https=) |
| JP (1) | JP2024509153A (https=) |
| CN (1) | CN117043108B (https=) |
| CA (1) | CA3207884A1 (https=) |
| WO (1) | WO2022184759A1 (https=) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN119143147B (zh) * | 2023-06-15 | 2026-04-21 | 中国石油化工股份有限公司 | P修饰的金属掺杂mww分子筛及其制备方法和应用 |
Family Cites Families (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3117135A1 (de) | 1981-04-30 | 1982-11-18 | Bayer Ag, 5090 Leverkusen | Kristallines alumosilicat, verfahren zu dessen herstellung sowie dessen verwendung zur katalytischen umwandlung von methanol und/oder dimethylether in kohlenwasserstoffe |
| US4826667A (en) | 1986-01-29 | 1989-05-02 | Chevron Research Company | Zeolite SSZ-25 |
| US4954325A (en) | 1986-07-29 | 1990-09-04 | Mobil Oil Corp. | Composition of synthetic porous crystalline material, its synthesis and use |
| IT1205681B (it) | 1987-05-26 | 1989-03-31 | Eniricerche Spa | Materiale sintetico cristallino poroso contenente ossidi di silicio e boro |
| US5250277A (en) | 1991-01-11 | 1993-10-05 | Mobil Oil Corp. | Crystalline oxide material |
| US5236575A (en) | 1991-06-19 | 1993-08-17 | Mobil Oil Corp. | Synthetic porous crystalline mcm-49, its synthesis and use |
| US5827491A (en) | 1993-04-26 | 1998-10-27 | Mobil Oil Corporation | Process for preparing the synthetic porous crystalline material MCM-56 |
| US5362697A (en) | 1993-04-26 | 1994-11-08 | Mobil Oil Corp. | Synthetic layered MCM-56, its synthesis and use |
| ES2124154B1 (es) | 1995-11-08 | 1999-12-01 | Univ Politecnica De Valencia C | Metodo de preparaciion y propiedades cataliticas de un solido microporoso con alta superficie externa. |
| ES2105982B1 (es) | 1995-11-23 | 1998-07-01 | Consejo Superior Investigacion | Zeolita itq-1 |
| CN1311757A (zh) | 1998-07-29 | 2001-09-05 | 埃克森化学专利公司 | 制备分子筛的方法 |
| US6756030B1 (en) | 2003-03-21 | 2004-06-29 | Uop Llc | Crystalline aluminosilicate zeolitic composition: UZM-8 |
| US7713513B2 (en) | 2003-03-21 | 2010-05-11 | Uop Llc | High silica zeolites: UZM-8HS |
| ES2246704B1 (es) | 2004-05-28 | 2007-06-16 | Universidad Politecnica De Valencia | Zeolita itq-30. |
| CN101384367B (zh) | 2006-02-14 | 2012-05-30 | 埃克森美孚化学专利公司 | 一种制造mcm-22族分子筛的方法 |
| BRPI0713674A2 (pt) | 2006-07-28 | 2012-10-23 | Exxonmobil Chemical Patents Inc. | formulações farmarcêuticas e composições de um antagonista seletivo cxcr2 ou cxcr1 e métodos para o uso do mesmo visando o tratamento de distúrbios inflamatórios |
| EP2051805B1 (en) * | 2006-07-28 | 2019-10-02 | ExxonMobil Chemical Patents Inc. | A mcm-22 family molecular sieve composition, its method of making, and use for hydrocarbon conversions |
| KR101097536B1 (ko) | 2006-07-28 | 2011-12-22 | 엑손모빌 케미칼 패턴츠 인코포레이티드 | 신규 분자체 조성물, 이의 제조 방법 및 이의 사용 방법 |
| DE102008003103A1 (de) | 2008-01-01 | 2009-07-02 | Lts Lohmann Therapie-Systeme Ag | Einweginjektor mit zweikolbigem Zweikammersystem |
| RU2509055C2 (ru) | 2008-07-28 | 2014-03-10 | Эксонмобил Кемикэл Пейтентс Инк. | Новая молекулярно-ситовая композиция емм-12, способы ее получения и применения |
| WO2010021795A1 (en) | 2008-07-28 | 2010-02-25 | Exxonmobil Chemical Patents Inc. | A novel molecular sieve composition emm-12, a method of making and a process of using the same |
| CN103827033B (zh) | 2011-09-16 | 2016-05-11 | 埃克森美孚化学专利公司 | 改进的mcm-56制造方法 |
| WO2015112293A1 (en) | 2014-01-27 | 2015-07-30 | Exxonbobil Chemical Patents Inc. | Synthesis of molecular sieves having mww framework structure |
| US10173903B2 (en) * | 2014-06-16 | 2019-01-08 | University Of Houston System | Zeolite compositions and methods for tailoring zeolite crystal habits with growth modifiers |
| EP3718970A4 (en) * | 2017-11-28 | 2020-10-07 | Mitsui Mining & Smelting Co., Ltd. | MWW TYPE ZEOLITE, ITS PRODUCTION METHOD AND CRACKING CATALYST |
| KR102267465B1 (ko) * | 2019-08-14 | 2021-06-22 | 고려대학교 산학협력단 | 단순 소성을 통한 나노판형 제올라이트의 제조방법과 이로부터 제조된 나노판형 제올라이트 입자 |
| CN111977663A (zh) * | 2020-08-25 | 2020-11-24 | 西北大学 | 一种多级孔道结构沸石分子筛及其制备方法和应用 |
-
2022
- 2022-03-02 US US18/264,271 patent/US20240101435A1/en active Pending
- 2022-03-02 CN CN202280018224.8A patent/CN117043108B/zh active Active
- 2022-03-02 CA CA3207884A patent/CA3207884A1/en active Pending
- 2022-03-02 EP EP22710036.9A patent/EP4301700A1/en active Pending
- 2022-03-02 JP JP2023553242A patent/JP2024509153A/ja active Pending
- 2022-03-02 WO PCT/EP2022/055235 patent/WO2022184759A1/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| EP4301700A1 (en) | 2024-01-10 |
| WO2022184759A1 (en) | 2022-09-09 |
| JP2024509153A (ja) | 2024-02-29 |
| US20240101435A1 (en) | 2024-03-28 |
| CN117043108A (zh) | 2023-11-10 |
| CN117043108B (zh) | 2026-02-13 |
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