JP2024160422A - １－ハロ－２，６，１４－トリメチルオクタデカン化合物、並びにそれを用いた５，１３，１７－トリメチルアルカン化合物の製造方法 - Google Patents

１－ハロ－２，６，１４－トリメチルオクタデカン化合物、並びにそれを用いた５，１３，１７－トリメチルアルカン化合物の製造方法 Download PDF

Info

Publication number
JP2024160422A
JP2024160422A JP2023075366A JP2023075366A JP2024160422A JP 2024160422 A JP2024160422 A JP 2024160422A JP 2023075366 A JP2023075366 A JP 2023075366A JP 2023075366 A JP2023075366 A JP 2023075366A JP 2024160422 A JP2024160422 A JP 2024160422A
Authority
JP
Japan
Prior art keywords
compound
formula
halo
reaction
halogen atom
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2023075366A
Other languages
English (en)
Japanese (ja)
Other versions
JP2024160422A5 (enExample
Inventor
裕樹 三宅
Hiroki Miyake
有真 菅原
Yuma SUGAWARA
武 渡辺
Takeshi Watanabe
剛 金生
Takeshi Kanao
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shin Etsu Chemical Co Ltd
Original Assignee
Shin Etsu Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shin Etsu Chemical Co Ltd filed Critical Shin Etsu Chemical Co Ltd
Priority to JP2023075366A priority Critical patent/JP2024160422A/ja
Priority to US18/648,639 priority patent/US20240368061A1/en
Priority to EP24173051.4A priority patent/EP4458792A1/en
Priority to CN202410539199.9A priority patent/CN118878395A/zh
Publication of JP2024160422A publication Critical patent/JP2024160422A/ja
Publication of JP2024160422A5 publication Critical patent/JP2024160422A5/ja
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/01—Acyclic saturated compounds containing halogen atoms containing chlorine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/075—Acyclic saturated compounds containing halogen atoms containing bromine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/32—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from compounds containing hetero-atoms other than or in addition to oxygen or halogen
    • C07C1/325—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from compounds containing hetero-atoms other than or in addition to oxygen or halogen the hetero-atom being a metal atom
    • C07C1/326—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from compounds containing hetero-atoms other than or in addition to oxygen or halogen the hetero-atom being a metal atom the hetero-atom being a magnesium atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/26—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only halogen atoms as hetero-atoms
    • C07C1/30—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only halogen atoms as hetero-atoms by splitting-off the elements of hydrogen halide from a single molecule
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/16—Preparation of halogenated hydrocarbons by replacement by halogens of hydroxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/263—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions
    • C07C17/2632—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions involving an organo-magnesium compound, e.g. Grignard synthesis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
    • C07C2/86—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon
    • C07C2/861—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon the non-hydrocarbon contains only halogen as hetero-atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/36—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/36—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal
    • C07C29/38—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones
    • C07C29/40—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones with compounds containing carbon-to-metal bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/02—Monohydroxylic acyclic alcohols
    • C07C31/125—Monohydroxylic acyclic alcohols containing five to twenty-two carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/48—Preparation of compounds having groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/30—Compounds having groups
    • C07C43/303—Compounds having groups having acetal carbon atoms bound to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/511—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition involving transformation of singly bound oxygen functional groups to >C = O groups
    • C07C45/513—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition involving transformation of singly bound oxygen functional groups to >C = O groups the singly bound functional group being an etherified hydroxyl group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00—Compounds having —CHO groups
    • C07C47/02—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C9/00—Aliphatic saturated hydrocarbons
    • C07C9/22—Aliphatic saturated hydrocarbons with more than fifteen carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
    • C07F3/02—Magnesium compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2023075366A 2023-05-01 2023-05-01 １－ハロ－２，６，１４－トリメチルオクタデカン化合物、並びにそれを用いた５，１３，１７－トリメチルアルカン化合物の製造方法 Pending JP2024160422A (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP2023075366A JP2024160422A (ja) 2023-05-01 2023-05-01 １－ハロ－２，６，１４－トリメチルオクタデカン化合物、並びにそれを用いた５，１３，１７－トリメチルアルカン化合物の製造方法
US18/648,639 US20240368061A1 (en) 2023-05-01 2024-04-29 1-halo-2,6,14-trimethyloctadecane compound and process for preparing 5,13,17-trimethylalkane compound therefrom
EP24173051.4A EP4458792A1 (en) 2023-05-01 2024-04-29 1-halo-2,6,14-trimethyloctadecane compound and process for preparing 5,13,17-trimethylalkane compound therefrom
CN202410539199.9A CN118878395A (zh) 2023-05-01 2024-04-30 1-卤代-2,6,14-三甲基十八烷化合物和从其制备5,13,17-三甲基烷烃化合物的方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2023075366A JP2024160422A (ja) 2023-05-01 2023-05-01 １－ハロ－２，６，１４－トリメチルオクタデカン化合物、並びにそれを用いた５，１３，１７－トリメチルアルカン化合物の製造方法

Publications (2)

Publication Number Publication Date
JP2024160422A true JP2024160422A (ja) 2024-11-14
JP2024160422A5 JP2024160422A5 (enExample) 2025-11-20

Family

ID=90924511

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2023075366A Pending JP2024160422A (ja) 2023-05-01 2023-05-01 １－ハロ－２，６，１４－トリメチルオクタデカン化合物、並びにそれを用いた５，１３，１７－トリメチルアルカン化合物の製造方法

Country Status (4)

Country Link
US (1) US20240368061A1 (enExample)
EP (1) EP4458792A1 (enExample)
JP (1) JP2024160422A (enExample)
CN (1) CN118878395A (enExample)

Also Published As

Publication number Publication date
US20240368061A1 (en) 2024-11-07
EP4458792A1 (en) 2024-11-06
CN118878395A (zh) 2024-11-01

Similar Documents

Publication Publication Date Title
CN108727170B (zh) 1-卤代-6,9-十五碳二烯和制备(7z,10z)-7,10-十六碳二烯醛的方法
JP7019500B2 (ja) （９ｅ，１１ｚ）－９，１１－ヘキサデカジエニル＝アセテートの製造方法
JP6947690B2 (ja) （２Ｅ，６Ｚ）−２，６−ノナジエナールの製造方法及び（２Ｅ）−ｃｉｓ−６，７−エポキシ−２−ノネナールの製造方法
JP2693615B2 (ja) １‐ハロ‐４，６，１０‐ヘキサデカトリエン化合物およびその製造方法
CN109956850B (zh) 3,7-二甲基-7-辛烯醇和3,7-二甲基-7-辛烯基羧酸酯化合物的生产方法
JP2024160422A (ja) １－ハロ－２，６，１４－トリメチルオクタデカン化合物、並びにそれを用いた５，１３，１７－トリメチルアルカン化合物の製造方法
JP7255010B2 (ja) ８－ウンデセニル求核試薬及びその製造方法、並びに９－ドデセナール化合物の製造方法
JP7543242B2 (ja) ３，７－ジメチルアルカン化合物の製造方法
JP7291105B2 (ja) （９ｚ，１１ｅ）－９，１１－ヘキサデカジエナールの製造方法
JPS6212770B2 (enExample)
JP2024160423A (ja) １７－メチルアルカン化合物の製造方法
JP7678859B2 (ja) ホルミルアルケニル＝アルコキシメチル＝エーテル化合物の製造方法及びこれを用いた共役ジエン化合物の製造方法
JP7227864B2 (ja) １１－ハロ－３－ウンデセン化合物及びその製造方法、並びに９－ドデセナール化合物の製造方法
JP7216043B2 (ja) ６－イソプロペニル－３－メチル－９－デセニル＝アセテートの製造方法及びその中間体
JP7254665B2 (ja) ４－ペンテン－２－イナールの製造方法
JP7197446B2 (ja) ジアルコキシアルカジエンイン化合物及びその製造方法並びにジエンイナール化合物の製造方法
JPH0244459B2 (enExample)
JP2024173745A (ja) ハロアルキル＝アルコキシメチル＝エーテル化合物、並びにそれを用いた４，６，８，１０，１６－ペンタメチルドコサン及びその合成中間体の製造方法
JP2025038885A (ja) ８－（アシルオキシ）アルカナール化合物及びその製造方法、並びに該８－（アシルオキシ）アルカナール化合物を用いた２，９－ジアセトキシウンデカンの製造方法
JPS6313409B2 (enExample)
JP2024173744A (ja) ハロアルキル＝アルコキシメチル＝エーテル化合物、並びにそれを用いた１３，１５－ジメチルヘプタコサン及びその合成中間体の製造方法
JPH0546345B2 (enExample)
CN117164461A (zh) (4z,6e)-4,6-十一碳二烯基三甲基乙酸酯及由其制备(5z,7e)-5,7-十二碳二烯化合物的方法
JPS6254288B2 (enExample)
JPH0465065B2 (enExample)

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20240508

RD04 Notification of resignation of power of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7424

Effective date: 20250314

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20250522

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20251112