JP2024035408A - 熱分析装置 - Google Patents

熱分析装置 Download PDF

Info

Publication number
JP2024035408A
JP2024035408A JP2022139845A JP2022139845A JP2024035408A JP 2024035408 A JP2024035408 A JP 2024035408A JP 2022139845 A JP2022139845 A JP 2022139845A JP 2022139845 A JP2022139845 A JP 2022139845A JP 2024035408 A JP2024035408 A JP 2024035408A
Authority
JP
Japan
Prior art keywords
gas
heating furnace
flow path
component
sample
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2022139845A
Other languages
English (en)
Japanese (ja)
Other versions
JP2024035408A5 (enExample
Inventor
弘一郎 則武
Koichiro Noritake
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rigaku Denki Co Ltd
Rigaku Corp
Original Assignee
Rigaku Denki Co Ltd
Rigaku Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rigaku Denki Co Ltd, Rigaku Corp filed Critical Rigaku Denki Co Ltd
Priority to JP2022139845A priority Critical patent/JP2024035408A/ja
Priority to EP23194215.2A priority patent/EP4332569A1/en
Priority to US18/241,342 priority patent/US20240077396A1/en
Priority to CN202311125206.2A priority patent/CN117647558A/zh
Publication of JP2024035408A publication Critical patent/JP2024035408A/ja
Publication of JP2024035408A5 publication Critical patent/JP2024035408A5/ja
Pending legal-status Critical Current

Links

Images

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N7/00Analysing materials by measuring the pressure or volume of a gas or vapour
    • G01N7/14Analysing materials by measuring the pressure or volume of a gas or vapour by allowing the material to emit a gas or vapour, e.g. water vapour, and measuring a pressure or volume difference
    • G01N7/16Analysing materials by measuring the pressure or volume of a gas or vapour by allowing the material to emit a gas or vapour, e.g. water vapour, and measuring a pressure or volume difference by heating the material
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/20Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/24Suction devices
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/40Concentrating samples
    • G01N1/405Concentrating samples by adsorption or absorption
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44Sample treatment involving radiation, e.g. heat
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/02Investigating or analyzing materials by the use of thermal means by investigating changes of state or changes of phase; by investigating sintering
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0006Calibrating gas analysers
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0009General constructional details of gas analysers, e.g. portable test equipment
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0009General constructional details of gas analysers, e.g. portable test equipment
    • G01N33/0011Sample conditioning
    • G01N33/0021Sample conditioning involving the use of a carrier gas for transport to the sensor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N2030/0075Separation due to differential desorption
    • G01N2030/008Thermal desorption
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/06Preparation
    • G01N30/08Preparation using an enricher
    • G01N2030/085Preparation using an enricher using absorbing precolumn
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/06Preparation
    • G01N30/12Preparation by evaporation
    • G01N2030/126Preparation by evaporation evaporating sample
    • G01N2030/128Thermal desorption analysis
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0009General constructional details of gas analysers, e.g. portable test equipment
    • G01N33/0027General constructional details of gas analysers, e.g. portable test equipment concerning the detector
    • G01N33/0036General constructional details of gas analysers, e.g. portable test equipment concerning the detector specially adapted to detect a particular component
    • G01N33/004CO or CO2

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Immunology (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)
JP2022139845A 2022-09-02 2022-09-02 熱分析装置 Pending JP2024035408A (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP2022139845A JP2024035408A (ja) 2022-09-02 2022-09-02 熱分析装置
EP23194215.2A EP4332569A1 (en) 2022-09-02 2023-08-30 Thermal analysis apparatus
US18/241,342 US20240077396A1 (en) 2022-09-02 2023-09-01 Thermal analysis apparatus
CN202311125206.2A CN117647558A (zh) 2022-09-02 2023-09-01 热分析装置

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2022139845A JP2024035408A (ja) 2022-09-02 2022-09-02 熱分析装置

Publications (2)

Publication Number Publication Date
JP2024035408A true JP2024035408A (ja) 2024-03-14
JP2024035408A5 JP2024035408A5 (enExample) 2024-10-28

Family

ID=87863485

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2022139845A Pending JP2024035408A (ja) 2022-09-02 2022-09-02 熱分析装置

Country Status (4)

Country Link
US (1) US20240077396A1 (enExample)
EP (1) EP4332569A1 (enExample)
JP (1) JP2024035408A (enExample)
CN (1) CN117647558A (enExample)

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1439469A (en) * 1972-12-15 1976-06-16 Bayer Ag Process for the pyrolytic analysis of liquids
JPS5954944A (ja) * 1982-09-21 1984-03-29 Kazuo Makino 熱重量分析装置
JPS6153655B2 (enExample) * 1979-09-21 1986-11-19 Nippon Kokan Kk
JPH03272443A (ja) * 1990-03-22 1991-12-04 Rigaku Corp 熱分析方法及び熱分析装置
JPH05281171A (ja) * 1992-04-02 1993-10-29 Kyoto Electron Mfg Co Ltd 水分測定用試料加熱気化装置
JP2004132879A (ja) * 2002-10-11 2004-04-30 National Cardiovascular Center 高感度ガス分析システムおよびそれを用いたガス分析方法
JP2013160594A (ja) * 2012-02-03 2013-08-19 Horiba Ltd 元素分析装置
JP2017102102A (ja) * 2015-11-20 2017-06-08 株式会社日立ハイテクサイエンス 発生ガス分析装置及び発生ガス分析方法
JP2018533028A (ja) * 2015-11-09 2018-11-08 ブラベンダー メステクニク ゲゼルシャフト ミット ベシュレンクテル ハフツング ウント コンパニー コマンデイトゲゼルシャフト サンプルの水分を測定する装置及び方法
JP2019020375A (ja) * 2017-07-12 2019-02-07 株式会社堀場製作所 分析装置

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4162138B2 (ja) * 2003-10-27 2008-10-08 株式会社リガク 昇温脱離ガス分析装置
JP5363408B2 (ja) 2010-04-26 2013-12-11 日本碍子株式会社 発生気体分析装置
CN107655637B (zh) * 2016-07-26 2021-06-18 中国辐射防护研究院 一种碘吸附器泄漏检测的脉冲式卤素气体检测方法及设备
CN109254108B (zh) * 2017-07-12 2023-02-17 株式会社堀场制作所 分析装置和分析方法

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1439469A (en) * 1972-12-15 1976-06-16 Bayer Ag Process for the pyrolytic analysis of liquids
JPS6153655B2 (enExample) * 1979-09-21 1986-11-19 Nippon Kokan Kk
JPS5954944A (ja) * 1982-09-21 1984-03-29 Kazuo Makino 熱重量分析装置
JPH03272443A (ja) * 1990-03-22 1991-12-04 Rigaku Corp 熱分析方法及び熱分析装置
JPH05281171A (ja) * 1992-04-02 1993-10-29 Kyoto Electron Mfg Co Ltd 水分測定用試料加熱気化装置
JP2004132879A (ja) * 2002-10-11 2004-04-30 National Cardiovascular Center 高感度ガス分析システムおよびそれを用いたガス分析方法
JP2013160594A (ja) * 2012-02-03 2013-08-19 Horiba Ltd 元素分析装置
JP2018533028A (ja) * 2015-11-09 2018-11-08 ブラベンダー メステクニク ゲゼルシャフト ミット ベシュレンクテル ハフツング ウント コンパニー コマンデイトゲゼルシャフト サンプルの水分を測定する装置及び方法
JP2017102102A (ja) * 2015-11-20 2017-06-08 株式会社日立ハイテクサイエンス 発生ガス分析装置及び発生ガス分析方法
JP2019020375A (ja) * 2017-07-12 2019-02-07 株式会社堀場製作所 分析装置

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
本橋輝樹: ""TG-GC" による熱重量・反応ガス定量分析", リガクジャーナル, vol. 51(2), JPN6025031240, 2020, pages 1 - 5, ISSN: 0005656337 *

Also Published As

Publication number Publication date
CN117647558A (zh) 2024-03-05
EP4332569A1 (en) 2024-03-06
US20240077396A1 (en) 2024-03-07

Similar Documents

Publication Publication Date Title
US7851712B2 (en) Gravimetric moisture measurement instrument
US7104680B2 (en) Thermal analyzer with gas mixing chamber
KR101220668B1 (ko) 광범위 연속 희석기
US7141090B2 (en) Active filter temperature control
US11215554B2 (en) Gas detecting apparatus and method based on terahertz spectroscopy
JP2024035408A (ja) 熱分析装置
JP2024035409A (ja) 熱分析装置
US20180128798A1 (en) Methods and systems for analysing a fluid mixture
US11692914B2 (en) Diluting device for aerosol measurements
US5996397A (en) Reactive gas sampling/analyzing hygrometry system
JP6002404B2 (ja) 質量分析装置及びその使用方法、並びにガス透過特性測定方法
WO2002070116A1 (en) Assembly and method for mixing gases
JP5055504B2 (ja) オイルミスト濃度測定装置
CN112557240A (zh) 一种烟气湿度测试仪校准装置和方法
JP7183261B2 (ja) 複数の成分を含む流体サンプルの部分変換のための装置および方法、並びにこれらの成分のオンライン決定および分析のための方法
WO2019163059A1 (ja) 連続生産システム及び方法
JP7293248B2 (ja) ガス分析装置及びガス分析装置の校正方法
US6543932B1 (en) Enthalpy tunnel
US20230094819A1 (en) Method for Measuring Humidity
KR102418632B1 (ko) 오염물질센서용 전처리장치 및 오염물질센서용 전처리방법
Guan et al. The Effects of the Structural Tuning on the Sensing Performance of Extinguishant Detector Based on the Differential Pressure Principle
TWI854719B (zh) 氫氣消除器的測試裝置
EP3374759B1 (en) Gaz analyzer with protection for optical components
CN223065161U (zh) 反应釜
JP2000074798A (ja) ガス分析装置

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20240930

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20241018

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20241018

RD01 Notification of change of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7421

Effective date: 20250218

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20250725

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20250805

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20251003

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20251028

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20251111