GB1439469A - Process for the pyrolytic analysis of liquids - Google Patents
Process for the pyrolytic analysis of liquidsInfo
- Publication number
- GB1439469A GB1439469A GB5774473A GB5774473A GB1439469A GB 1439469 A GB1439469 A GB 1439469A GB 5774473 A GB5774473 A GB 5774473A GB 5774473 A GB5774473 A GB 5774473A GB 1439469 A GB1439469 A GB 1439469A
- Authority
- GB
- United Kingdom
- Prior art keywords
- carrier gas
- furnace
- combustion
- cell
- sample
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000007788 liquid Substances 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 239000012159 carrier gas Substances 0.000 abstract 5
- 239000000567 combustion gas Substances 0.000 abstract 3
- 238000002485 combustion reaction Methods 0.000 abstract 3
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 abstract 3
- 229910052753 mercury Inorganic materials 0.000 abstract 3
- 239000000428 dust Substances 0.000 abstract 2
- 239000010865 sewage Substances 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 abstract 1
- 229910021536 Zeolite Inorganic materials 0.000 abstract 1
- 238000010521 absorption reaction Methods 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 abstract 1
- 229910052709 silver Inorganic materials 0.000 abstract 1
- 239000004332 silver Substances 0.000 abstract 1
- 210000002268 wool Anatomy 0.000 abstract 1
- 239000010457 zeolite Substances 0.000 abstract 1
- 229910001928 zirconium oxide Inorganic materials 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/18—Water
- G01N33/1806—Biological oxygen demand [BOD] or chemical oxygen demand [COD]
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/12—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using combustion
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/18—Water
- G01N33/1826—Organic contamination in water
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Pathology (AREA)
- Immunology (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Medicinal Chemistry (AREA)
- Food Science & Technology (AREA)
- Molecular Biology (AREA)
- Biodiversity & Conservation Biology (AREA)
- Biomedical Technology (AREA)
- Emergency Medicine (AREA)
- Combustion & Propulsion (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Abstract
1439469 Pyrolytic analysis BAYER AG 13 Dec 1973 [15 Dec 1972] 57744/73 Heading G1B A process for the pyrolytic analysis of liquids, for example sewage, comprises injecting a sample of the liquid together with a carrier gas comprising air into a combustion furnace and passing it repeatedly through the hottest zone of the furnace where the sample is burnt in the absence of a catalyst at temperatures of from 1000‹ to 1200‹C, and delivering the combustion gases to an analyzer. In the furnace 3 of Fig. 2, the carrier gas is preheated by passing it through line 8, and the preheated carrier gas entering at 7 together with injected sample passes through concentric tubes 6, 5 in the hottest part of the furnace for the combustion step. The process may be carried out to determine organic carbon using the apparatus of Fig. 1 (not shown) in which air as carrier gas passes through zeolite adsorbers and through precombustion line 8, and the combustion gases pass through a CaCl 2 bottle and a dust filter to a CO 2 analyzer. In the apparatus of Fig. 3 (not shown), total oxygen demand may be determined using a high temperature zirconium oxide measuring cell. In the apparatus of Fig. 4, used for the determination of total mercury in sewage, the carrier gas passes through dust filter 20 and mercury filter 21 of silver wool to pump 22 and the combustion system. Combustion gases flow through shortest possible tube 24, which may be capillary tubing and is heated, to heated measuring cell 25 of a mercury absorption photometer. The windows 30 of the cell may be kept clear of deposit by streams of heated air injected through annular nozzles (31), Fig. 5 (not shown). In another embodiment a windowless cell may be used and tube 24 has i.d. 1 to 4 mm. and length 200 to 400mm.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19722261456 DE2261456B2 (en) | 1972-12-15 | 1972-12-15 | PYROLYTIC ANALYSIS OF LIQUIDS |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1439469A true GB1439469A (en) | 1976-06-16 |
Family
ID=5864534
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB5774473A Expired GB1439469A (en) | 1972-12-15 | 1973-12-13 | Process for the pyrolytic analysis of liquids |
Country Status (9)
| Country | Link |
|---|---|
| JP (1) | JPS4991298A (en) |
| BE (1) | BE808626A (en) |
| CH (1) | CH573598A5 (en) |
| DE (1) | DE2261456B2 (en) |
| FR (1) | FR2214380A5 (en) |
| GB (1) | GB1439469A (en) |
| IT (1) | IT1013563B (en) |
| NL (1) | NL7317039A (en) |
| SE (1) | SE400836B (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004025292A1 (en) * | 2002-09-02 | 2004-03-25 | Lar Analytik Und Umweltmesstechnik Gmbh | Method for determining the oxygen requirement of an aqueous solution for a purification process |
| ITMI20091439A1 (en) * | 2009-08-07 | 2011-02-08 | Eurovector S P A | IMPROVED PYROLYSIS REACTOR FOR HIGH-TEMPERATURE CONVERSION |
| CN107880970A (en) * | 2017-11-14 | 2018-04-06 | 华北电力大学（保定） | A kind of microwave radiation formula low-temperature pyrolysis of coal demercuration system and application method |
| CN111366678A (en) * | 2020-04-03 | 2020-07-03 | 河南华豫达消防安全检测有限公司 | Drying device for air pipeline of paving material combustion test device |
| EP4332569A1 (en) * | 2022-09-02 | 2024-03-06 | Rigaku Corporation | Thermal analysis apparatus |
| EP4141442A4 (en) * | 2021-03-12 | 2024-06-19 | HORIBA, Ltd. | Element analysis device, operation method for element analysis device, and work program for element analysis device |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2534259A1 (en) * | 1975-07-31 | 1977-02-17 | Bayer Ag | INCINERATOR FOR PYROLYTIC ANALYSIS |
| US4244917A (en) * | 1979-05-09 | 1981-01-13 | Conoco, Inc. | Sample pyrolysis oven |
| US5064617A (en) * | 1990-02-16 | 1991-11-12 | Leco Corporation | Combustion system |
| DE19923139A1 (en) * | 1999-05-03 | 2000-12-07 | Lar Analytik & Umweltmestechni | Method and device for the digestion of an aqueous solution for carbon content determination |
| DE102006049349B4 (en) * | 2006-10-19 | 2010-12-02 | Iav Gmbh Ingenieurgesellschaft Auto Und Verkehr | Method and device for monitoring the functional properties of a lubricant |
| DE102014118138A1 (en) * | 2014-12-08 | 2016-06-09 | Lar Process Analysers Ag | Analysis arrangement for water and wastewater analysis |
-
1972
- 1972-12-15 DE DE19722261456 patent/DE2261456B2/en not_active Ceased
-
1973
- 1973-12-10 IT IT296473A patent/IT1013563B/en active
- 1973-12-12 NL NL7317039A patent/NL7317039A/xx not_active Application Discontinuation
- 1973-12-13 JP JP13822173A patent/JPS4991298A/ja active Pending
- 1973-12-13 SE SE7316859A patent/SE400836B/en unknown
- 1973-12-13 GB GB5774473A patent/GB1439469A/en not_active Expired
- 1973-12-13 CH CH1749673A patent/CH573598A5/xx not_active IP Right Cessation
- 1973-12-14 FR FR7344828A patent/FR2214380A5/fr not_active Expired
- 1973-12-14 BE BE138854A patent/BE808626A/en unknown
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004025292A1 (en) * | 2002-09-02 | 2004-03-25 | Lar Analytik Und Umweltmesstechnik Gmbh | Method for determining the oxygen requirement of an aqueous solution for a purification process |
| CN100353165C (en) * | 2002-09-02 | 2007-12-05 | 拉尔分析和环境测试技术有限公司 | Method for determining the oxygen requirement of an aqueous solution for a purification process |
| ITMI20091439A1 (en) * | 2009-08-07 | 2011-02-08 | Eurovector S P A | IMPROVED PYROLYSIS REACTOR FOR HIGH-TEMPERATURE CONVERSION |
| EP2284530A1 (en) * | 2009-08-07 | 2011-02-16 | Eurovector S.p.A. | Improved pyrolysis reactor for high temperature conversion |
| CN107880970A (en) * | 2017-11-14 | 2018-04-06 | 华北电力大学（保定） | A kind of microwave radiation formula low-temperature pyrolysis of coal demercuration system and application method |
| CN107880970B (en) * | 2017-11-14 | 2023-10-31 | 华北电力大学（保定） | Microwave radiation type coal low-temperature pyrolysis mercury removal system and use method thereof |
| CN111366678A (en) * | 2020-04-03 | 2020-07-03 | 河南华豫达消防安全检测有限公司 | Drying device for air pipeline of paving material combustion test device |
| CN111366678B (en) * | 2020-04-03 | 2022-06-10 | 河南华豫达工程技术有限公司 | Drying device for air pipeline of paving material combustion test device |
| EP4141442A4 (en) * | 2021-03-12 | 2024-06-19 | HORIBA, Ltd. | Element analysis device, operation method for element analysis device, and work program for element analysis device |
| EP4332569A1 (en) * | 2022-09-02 | 2024-03-06 | Rigaku Corporation | Thermal analysis apparatus |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2261456A1 (en) | 1974-07-11 |
| SE400836B (en) | 1978-04-10 |
| CH573598A5 (en) | 1976-03-15 |
| JPS4991298A (en) | 1974-08-31 |
| DE2261456B2 (en) | 1976-10-21 |
| FR2214380A5 (en) | 1974-08-09 |
| NL7317039A (en) | 1974-06-18 |
| IT1013563B (en) | 1977-03-30 |
| BE808626A (en) | 1974-06-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |