JP2023027804A - 抗ウイルス性成形体およびその用途 - Google Patents
抗ウイルス性成形体およびその用途 Download PDFInfo
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- JP2023027804A JP2023027804A JP2021133078A JP2021133078A JP2023027804A JP 2023027804 A JP2023027804 A JP 2023027804A JP 2021133078 A JP2021133078 A JP 2021133078A JP 2021133078 A JP2021133078 A JP 2021133078A JP 2023027804 A JP2023027804 A JP 2023027804A
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- resin
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- JXKBGDWVKKEDGU-UHFFFAOYSA-M silver;perbromate Chemical compound [Ag+].[O-]Br(=O)(=O)=O JXKBGDWVKKEDGU-UHFFFAOYSA-M 0.000 description 1
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- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- QUTYHQJYVDNJJA-UHFFFAOYSA-K trisilver;2-hydroxypropane-1,2,3-tricarboxylate Chemical compound [Ag+].[Ag+].[Ag+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O QUTYHQJYVDNJJA-UHFFFAOYSA-K 0.000 description 1
- CMPGARWFYBADJI-UHFFFAOYSA-L tungstic acid Chemical compound O[W](O)(=O)=O CMPGARWFYBADJI-UHFFFAOYSA-L 0.000 description 1
- 241000701161 unidentified adenovirus Species 0.000 description 1
- 241001529453 unidentified herpesvirus Species 0.000 description 1
- 241000712461 unidentified influenza virus Species 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
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- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
- A61L2/23—Solid substances, e.g. granules, powders, blocks, tablets
- A61L2/238—Metals or alloys, e.g. oligodynamic metals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
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Abstract
Description
本開示の抗ウイルス性成形体は、銀系抗ウイルス剤を含み、表面特性として、濡れ特性および抽出銀イオン量(水を抽出液とした特定の抽出試験による銀イオン量)が特定の範囲に調整されている。
本開示の抗ウイルス性成形体における表面のぬれ張力(濡れ指数)は40~60mN/m(40mN/m以上60mN/m以下)であり、好ましくは40~55mN/m、さらに好ましくは40~50mN/mである。ぬれ張力が小さすぎると、抗ウイルス性が低下する。特に、本開示の抗ウイルス性成形体では、後述する銀イオン量が高くても、ぬれ張力が小さいと、抗ウイルス性が低下する。一方、ぬれ張力が大きすぎると、表面の滑り性が低下する傾向があり、耐擦傷性試験において傷が入り易くなる。
本開示の抗ウイルス性成形体は、銀系抗ウイルス剤を含む。本開示では、銀系抗ウイルス剤の種類は、抗ウイルス性成形体の表面に前記銀イオン量を付与できればよく、特に限定されるものではない。
本開示の抗ウイルス性成形体は、成形性および機械的特性のバランスに優れる点から、抗ウイルス剤に加えて、樹脂成分を含むのが好ましい。
樹脂成分が親水性硬化性樹脂を含む場合、抗ウイルス性成形体は、親水性硬化性樹脂および銀系抗ウイルス剤を含む硬化性組成物の硬化物で形成されており、前記硬化性組成物は、親水性硬化性樹脂に加えて、親水性硬化性樹脂の種類に応じて、さらに硬化剤を含んでいてもよい。前記硬化性組成物は、例えば、熱硬化性樹脂では、アミン類、多価カルボン酸類などの硬化剤を含んでいてもよく、光硬化性樹脂では光重合開始剤を含んでいてもよい。光重合開始剤としては、慣用の成分、例えば、アセトフェノン類またはプロピオフェノン類、ベンジル類、ベンゾイン類、ベンゾフェノン類、チオキサントン類、アシルホスフィンオキシド類などが例示できる。
前記硬化性組成物は、さらに他の成分を含んでいてもよい。他の成分としては、慣用の添加剤、例えば、抗菌剤、抗カビ剤、防腐剤、レベリング剤、安定剤(酸化防止剤、紫外線吸収剤など)、界面活性剤、水溶性高分子、カップリング剤(チタンカップリング剤、シランカップリング剤)、充填剤、架橋剤、着色剤、難燃剤、滑剤、ワックス、防曇剤、粘度調整剤、増粘剤、消泡剤などが挙げられる。他の成分の合計割合は、硬化性樹脂100質量部に対して、例えば0.01~100質量部、好ましくは0.1~10質量部、さらに好ましくは0.5~5質量部である。
本開示の抗ウイルス性成形体は抗ウイルス性に優れている。本開示の抗ウイルス性成形体は、ヒトまたは非ヒト動物に対して感染力を有するウイルスに有効であるが、対象となるウイルスは、エンベロープを有するウイルス(エンベロープウイルス)、エンベロープを有さないウイルス(非エンベロープウイルス)のいずれのウイルスであってもよい。また、対象となるウイルスは、DNAウイルス、RNAウイルスのいずれのウイルスであってもよい。
本開示の抗ウイルス性成形体の形状は、特に限定されず、用途に応じて適宜選択できる。具体的な形状としては、例えば、線状、繊維状、糸状などの一次元形状;フィルム状、シート状、板状などの二次元形状;柱状、ブロック状、錐状、球状、凹または凸状、棒状、中空状(管状)、リング状などの三次元形状などが挙げられる。
本開示の抗ウイルス性成形体は、形状および構造に応じて慣用の成形方法によって製造できる。本開示の抗ウイルス性成形体が硬化性樹脂および抗ウイルス剤を含む硬化性組成物の硬化物で形成された抗ウイルス層である場合、本開示の抗ウイルス性成形体は、基材の上に、硬化性樹脂および抗ウイルス剤を含む硬化性組成物を塗布して乾燥し、抗ウイルス層前駆体を得る乾燥工程、前記抗ウイルス層前駆体を硬化させる硬化工程を経て製造してもよい。
親水性基を含有するアクリレートA:アイカ工業(株)製「アイカアイトロンZ-942-5」、固形分40質量%、開始剤含有
親水性基を含有するアクリレートB:東亜合成(株)製「アロニックスMT-3567」、固形分100質量%
UV硬化性ウレタンアクリレート:共栄社化学(株)製「HX-RSC-NA」、固形分50質量%、開始剤含有
UV硬化性シリコーン系アクリレートA:(株)トクシキ製「AU-230」、固形分54質量%、フィラー粒子(平均粒径0.6μm)および開始剤含有
UV硬化性シリコーン系アクリレートB:(株)トクシキ製「AS-201S」、固形分59質量%、開始剤含有
光開始剤:IGMジャパン(同)製「Omnirad184」
架橋ポリメタクリル酸メチルの真球状粒子:積水化成品工業(株)製「テクポリマーSSX-115HXE」、平均粒径15μm
ポリエチレンテレフタレート(PET)フィルム:三菱ケミカル(株)製「ダイアホイル」
抗ウイルス剤:住化エンバイロメンタルサイエンス(株)製「ネオシントールAV-18F」。
富士フイルム和光純薬(株)製の濡れ試薬(ぬれ張力試験用混合液)を使用し、実施例および比較例で得られた積層フィルムの抗ウイルス層に対して、JIS K 6768:1999に準拠して室温(23℃)および湿度50%RHにおいて測定した。
自動・動的接触角計(協和界面科学(株)製「型式DCA-UZ」)を使用し、実施例および比較例で得られた積層フィルムの抗ウイルス層に対し、室温(23℃)および湿度50%RHにおいて、約2μLの純水の液滴を滴下し、滴下後2秒時点での接触角を3点測定して平均した。
実施例および比較例で得られた積層フィルム(5cm角)の表面を80体積%エタノールで清拭して消毒、乾燥した後、100μLのウイルス液(SARS-CoV-2/JP/Hiroshima-46059T/2020株)を抗ウイルス層の上に滴下し、上から無菌パラフィルム(4cm角)をかぶせて液体を広げた。湿箱に入れて24時間室温(23℃)で保存した後に、パラフィルムを取り去り、900μLの細胞培養液DMEMを加えて液体を回収した。さらに同試薬(細胞培養液DMEM)で10倍段階希釈してTCID50法によってウイルス感染価の対数減少値を測定した。詳しくは、抗ウイルス性能は、未処理の対照フィルム(ポリエチレンフィルム)を用いて得られたウイルス感染価の対数減少値をブランクとし、ブランクに対する増加分を抗ウイルス活性値として示した。
抽出試験では、純水を抽出液として用い、実施例および比較例で得られた積層フィルムの抗ウイルス層(抗ウイルス層の面積:49cm2(7cm×7cm))と抽出液(液量:100mL)とを室温(23℃)および大気圧下で24時間接触させた。なお、抗ウイルス層と抽出液とを接触させる方法としては、抽出液中に前記積層フィルムを浸漬する方法で実施した。
親水性基を含有するアクリレートA100質量部に、抗ウイルス剤0.3質量部を添加した。この溶液を、ワイヤーバーを用いて、PETフィルム上に流延した後、80℃のオーブン内に1分間放置し、溶液中の溶媒を蒸発させることで、厚みが約5μmのコート層を形成した。その後、高圧水銀ランプにより紫外線をコート層に約5秒間照射(積算光量約300mJ/cm2照射)することにより、実施例1の積層フィルムを得た。
親水性基を含有するアクリレートB5質量部、光開始剤0.2質量部、UV硬化性ウレタンアクリレート90質量部、メチルエチルケトン5質量部を混合した。また、この混合物に、抗ウイルス剤0.5質量部を添加した。この溶液を、ワイヤーバーを用いて、PETフィルム上に流延した後、80℃のオーブン内に1分間放置し、溶液中の溶媒を蒸発させることで、厚みが約5μmのコート層を形成した。その後、高圧水銀ランプにより紫外線をコート層に約5秒間照射(積算光量約300mJ/cm2照射)することにより、比較例1の積層フィルムを得た。
UV硬化性シリコーン系アクリレートA50質量部、UV硬化性シリコーン系アクリレートB8質量部、架橋ポリメタクリル酸メチルの真球状粒子0.4質量部、メチルエチルケトン42質量部を混合した。また、この混合物に、抗ウイルス剤0.35質量部を添加した。この溶液を、ワイヤーバーを用いて、PETフィルム上に流延した後、80℃のオーブン内に1分間放置し、溶液中の溶媒を蒸発させることで、厚みが約10μmのコート層を形成した。その後、高圧水銀ランプにより紫外線をコート層に約5秒間照射(積算光量約300mJ/cm2照射)することにより、比較例2の積層フィルムを得た。
Claims (11)
- 銀系抗ウイルス剤を含み、表面のぬれ張力が40~60mN/mであり、かつ水で抽出した単位面積当たりの銀イオン量が200ng/cm2以上である抗ウイルス性成形体。
- 親水性基を有する樹脂をさらに含む請求項1記載の抗ウイルス性成形体。
- 前記樹脂が硬化性樹脂であり、前記硬化性樹脂および前記銀系抗ウイルス剤を含む硬化性組成物の硬化物である請求項2記載の抗ウイルス性成形体。
- 表面の水接触角が40°以下である請求項1~3のいずれか一項に記載の抗ウイルス性成形体。
- コロナウイルス(SARS-CoV-2)を温度25℃で24時間作用させたとき、感染価の対数減少値が2以上である請求項1~4のいずれか一項に記載の抗ウイルス性成形体。
- 基材表面の少なくとも一部の領域に積層された抗ウイルス層である請求項1~5のいずれか一項に記載の抗ウイルス性成形体。
- 基材と、この基材表面の少なくとも一部の領域に積層された抗ウイルス層とを含む複合成形体であって、前記抗ウイルス層が、請求項1~6のいずれか一項に記載の抗ウイルス性成形体である複合成形体。
- 前記基材が透明材料である請求項7記載の複合成形体。
- 前記透明材料が、ガラス、セルロースエステル、(メタ)アクリル系重合体、ポリエステルまたはポリカーボネートである請求項8記載の複合成形体。
- 請求項7~9のいずれか一項に記載の複合成形体を含むタッチパネルセンサー。
- 銀系抗ウイルス剤を含む抗ウイルス性成形体において、表面のぬれ張力を40~60mN/mに調整し、かつ水で抽出した単位面積当たりの銀イオン量を200ng/cm2以上に調整することにより、コロナウイルス(SARS-CoV-2)の感染価を低減する方法。
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WO2005037296A1 (ja) * | 2003-10-16 | 2005-04-28 | Toagosei Co., Ltd. | 抗コロナウイルス剤 |
JP2006247402A (ja) * | 2006-03-23 | 2006-09-21 | Kenji Nakamura | 衛生マスク |
JP2015189152A (ja) * | 2014-03-28 | 2015-11-02 | 富士フイルム株式会社 | 抗菌層付き基材、抗菌シート、放射線撮影装置、タッチパネル |
JP2015189196A (ja) * | 2014-03-28 | 2015-11-02 | 富士フイルム株式会社 | 抗菌層付き基材、抗菌シート、放射線撮影装置、タッチパネル |
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WO2005037296A1 (ja) * | 2003-10-16 | 2005-04-28 | Toagosei Co., Ltd. | 抗コロナウイルス剤 |
JP2006247402A (ja) * | 2006-03-23 | 2006-09-21 | Kenji Nakamura | 衛生マスク |
JP2015189152A (ja) * | 2014-03-28 | 2015-11-02 | 富士フイルム株式会社 | 抗菌層付き基材、抗菌シート、放射線撮影装置、タッチパネル |
JP2015189196A (ja) * | 2014-03-28 | 2015-11-02 | 富士フイルム株式会社 | 抗菌層付き基材、抗菌シート、放射線撮影装置、タッチパネル |
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