JP2022519269A - 有機化合物におけるまたは関連する改善 - Google Patents
有機化合物におけるまたは関連する改善 Download PDFInfo
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- JP2022519269A JP2022519269A JP2021545367A JP2021545367A JP2022519269A JP 2022519269 A JP2022519269 A JP 2022519269A JP 2021545367 A JP2021545367 A JP 2021545367A JP 2021545367 A JP2021545367 A JP 2021545367A JP 2022519269 A JP2022519269 A JP 2022519269A
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Abstract
Description
しかしながら、かかる組み合わせを含むデオドラントおよび制汗剤は、依然として欠点に悩まされている。主な不利な点は、2つの異なるカプセル化された香料組成物を提供する必要があることであり、これは、製剤の価格および複雑さを増大させる。さらにまた、あるタイプのコアシェルマイクロカプセルは、ホルムアルデヒド、イソシアネート、アクリラート、またはイミンの使用に起因して、消費者製品中のこれらの材料の量は、課せられたしきい値制限をはるかに下回ってはいるが、物議を醸している。
これらの問題は、請求項1に記載のカプセル化された組成物によって解決される。組成物は、マトリックスに封入された少なくとも1つの香料および/または化粧品成分を含む。マトリックスは、デンプンおよびヘミセルロースを含む。
デンプンマトリックスへのヘミセルロースの添加が、マトリックスの改変を引き起こし、水分および機械的(例として、摩擦)活性化の下で、その香料放出特性を改善することが見出された。その結果得られる香料カプセルは、製造において簡便であり、および費用効果が高い。さらにまた、それらは非毒性であり、および生分解性である天然ベースの多糖類から調製される。したがって、かかるカプセルは、増大した消費者アピールを有する。
水溶性加工デンプンは、乳化および乳化安定化能力を有する。それらは、デンプン加工剤の疎水性に起因して、水中油型エマルションの形態でフレグランスおよび/または化粧品の油滴を封入する能力を有する。本明細書において上述のとおりの加工デンプンは、高い乳化およびカプセル化性能、高固形分でも低粘度、および優れた耐酸化性を包含する多くの利点をもたらし、良好なフレグランスおよび/または化粧品の保存および敏感な成分の安定化を確実にする。
本発明の好ましい態様において、カプセル化された組成物は、さらに、マンニトールを含む。かかる組成物において、マンニトールの割合は、1~30重量%、好ましくは5~15重量%、さらにより好ましくは8~12重量%であり得る。
好ましくは、少なくとも50重量%、より具体的には少なくとも60重量%、さらにより具体的には少なくとも80重量%の香料成分は、2.0以上、より具体的には、2.5以上、さらにより具体的には3.0以上のcLog[P]を有する。フレグランス成分のcLog[P]の値は、Daylight Chemical Information Systems, Inc., Daylight CIS, Irvine, Californiaから入手できるPomona92データベースを包含する多くのデータベースで報告されている。
本発明によるカプセル化された組成物において、デンプンの割合は、30~90重量%、好ましくは35~80重量%、さらにより好ましくは40~70重量%であり得る。
本発明によるカプセル化された組成物において、ヘミセルロースの割合は、0.02~20重量%、好ましくは0.1~10重量%、さらにより好ましくは0.5~5重量%であり得る。本発明の特に好ましい態様において、ヘミセルロースの割合は0.75~2重量%である。
本文脈において、粒子のサイズは、Beckman Coulter LS13 320粒子サイズアナライザーを使用したレーザー散乱によって測定する。このデバイスは、光散乱の原理を使用することによって、乾燥粉末形態の粒子のサイズ分布を測定する。標準的な操作手順において、粒子径は体積および/または数で表される。
a)水中で少なくとも1つの香料および/または化粧品成分、デンプンおよびヘミセルロースを含むエマルションを調製すること;
b)エマルションを乾燥、とりわけ噴霧乾燥または二酸化ケイ素へ吸着させて、カプセル化された組成物を得ること、
を含む。
本明細書において上述のとおりのプロセスにおいて、ステップa)において調製されたエマルションは、2~60重量%、好ましくは5~40重量%、さらにより好ましくは10~30重量%のデンプンの割合を有し得る。
本明細書において上述のとおりのプロセスにおいて、ステップa)において調製されたエマルションは、0.001~10重量%、好ましくは0.01~5重量%、さらにより好ましくは0.1~1.0重量%のヘミセルロースの割合を有し得る。
本明細書において上述のとおりのプロセスにおいて、ステップa)において調製されたエマルションは、10~90重量%、好ましくは30~80重量%、さらにより好ましくは50~60重量%の水の割合を有し得る。
本発明はまた、本明細書において上述のとおりの方法によって得ることができるカプセル化された組成物に関する。
本発明のさらなる特徴および特定の利点は、いくつかの例の以下の記載から明らかになる。
添加剤スクリーニングのために、1重量%の添加剤(キトサン、アルギナート、ポリビニルアルコールまたはタマリンドカーネルパウダー)と共にデンプンマトリックスを含むいくつかのカプセル化された香料組成物を、例2に従う方法によって調製した。
嗅覚評価のために、0.4重量%のカプセル化された香料組成物を、それぞれの場合において、標準的な制汗剤ベースに添加した。0.2gの生成物を布パッチの中央に置き、スパチュラによって生成物を布の上に広げた。生成物を布の上に残して4時間乾燥した。次いで、20人のパネリストのパネルが、各段階に対し0~5のスケールに従ってスコアを付けることによって、以下の評価を実施した:
- 活性化前:適用の4時間後の乾式評価;
- 摩擦-活性化:布を折り、それを2回こする;活性化直後のブーストを評価する;
- 水分-活性化:布に水を直接2回スプレーする;活性化直後のブーストを評価する。
摩擦活性化の値は、活性化前に加えて得られたスコアを表し、水分活性化の値は、摩擦活性化に加えて得られたスコアを表す。
水道水(55.0g)をステンレス鋼ビーカーに量り入れた。続いて、デンプンナトリウムオクテニルスクシナートE1450(18.7g)、デンプン加工Hi-Cap 100(2.2g)、マルトデキストリンGlucidex IT-19(5.3g)、および例1で述べた添加剤(0.5g)を同じビーカーに量り入れた。得られた混合物を最初にステンレス鋼棒で手動で撹拌し、次いでIKAT25 Ultra-Turrax Homogenizerで13,500rpmで均質化して均一な溶液を得た。この得られた混合物に、香油(17.8g)を添加した。次いで、同じホモジナイザーを使用して、22,000~24,000rpmで20~30分間高剪断混合を行い、エマルションを生成した。液滴サイズは、動的光散乱によって0.5~2μmの間に制御された。
- 入口温度:190℃
- 出口温度:90℃
- ペリスタルティックポンプ速度:485mL/h
- 空気流量:3.7m/s
得られた噴霧乾燥粉末を、密閉された混合容器内で二酸化ケイ素Aerosil 200(0.5g)と混合した。
水道水(45.0g)をステンレス鋼ビーカーに量り入れた。続いて、デンプンナトリウムオクテニルスクシナートE1450(21.9g)、マンニトール60(5.5g)、およびタマリンドカーネルパウダー(0.5g)を同じビーカーに量り入れた。得られた混合物を最初にステンレス鋼棒で手動で撹拌し、次いでIKAT25 Ultra-Turrax Homogenizerで13,500rpmで均質化して均一な溶液を得た。この得られた混合物に、香油(27.3g)を添加した。次いで、同じホモジナイザーを使用して、22,000~24,000rpmで20~30分間高剪断混合を行い、エマルションを生成した。液滴サイズは、動的光散乱によって0.5~2μmの間に制御された。
- 入口温度:190℃
- 出口温度:90℃
- ペリスタルティックポンプ速度:485mL/h
- 空気流量:3.7m/s
得られた噴霧乾燥粉末を、密閉された混合容器内で二酸化ケイ素Aerosil 200(0.5g)と混合した。
添加剤としてタマリンドカーネルパウダーを用いた例2に従って調製された、本発明によるカプセル化された組成物の安定性を評価し、同じフレグランスを含有する従来のデンプンカプセル化と比較した。例1と同じ嗅覚評価プロトコルを使用した。表2は、サンプルを37℃、相対湿度70%で1か月間エージングした後の結果をまとめたものである。従来のデンプンカプセル化(エントリー3および4)と比較して、本発明によるカプセル化された組成物(エントリー1および2)の優れた嗅覚性能が、すべての段階(活性化前、摩擦-活性化および水分-活性化)で保持されていることが分かる。
Claims (15)
- マトリックスに封入された少なくとも1つの香料および/または化粧品成分を含むカプセル化された組成物であって、マトリックスがデンプンおよびヘミセルロースを含む、前記組成物。
- デンプンが水溶性加工デンプンである、請求項1に記載のカプセル化された組成物。
- 水溶性加工デンプンが、漂白デンプン、ヒドロキシプロピルデンプン、ヒドロキシプロピル化リン酸架橋デンプン、ヒドロキシプロピル化グリセロール架橋デンプン、アセチル化リン酸架橋デンプン、無水酢酸でエステル化されたデンプンアセタート、酢酸ビニルでエステル化されたデンプンアセタート、アセチル化アジピン酸架橋デンプン、アセチル化グリセロール架橋デンプン、オクテニルコハク酸デンプンナトリウムおよびそれらの混合物からなる群から選択される、請求項2に記載のカプセル化された組成物。
- ヘミセルロースがキシログルカン、とりわけタマリンド種子から得ることができるキシログルカンである、請求項1~3のいずれか一項に記載のカプセル化された組成物。
- さらに、マルトデキストリン、マンニトールおよびそれらの混合物からなる群から選択される化合物を含む、請求項1~4のいずれか一項に記載のカプセル化された組成物。
- さらに、二酸化ケイ素、ナトリウム塩、カルシウム塩およびゼオライトからなる群から選択される流動剤を含む、請求項1~5のいずれか一項に記載のカプセル化された組成物。
- 少なくとも1つの香料および/または化粧品成分の割合が、10~50重量%、好ましくは20~47.5重量%、さらにより好ましくは30~45重量%である、請求項1~6のいずれか一項に記載のカプセル化された組成物。
- デンプンの割合が、30~90重量%、好ましくは35~80重量%、さらにより好ましくは40~70重量%である、請求項1~7のいずれか一項に記載のカプセル化された組成物。
- ヘミセルロースの割合が、0.02~20重量%、好ましくは0.1~10重量%、さらにより好ましくは0.5~5重量%である、請求項1~8のいずれか一項に記載のカプセル化された組成物。
- 組成物が、粒子形態である、請求項1~9のいずれか一項に記載のカプセル化された組成物。
- カプセル化された組成物、とりわけ請求項1~10のいずれか一項に記載の組成物を調製するプロセスであって、該プロセスが、以下のステップ:
a)水中で少なくとも1つの香料および/または化粧品成分、デンプンおよびヘミセルロースを含むエマルションを調製すること;
b)エマルションを乾燥、とりわけ噴霧乾燥させてまたは二酸化ケイ素へ吸着させて、カプセル化された組成物を得ること、
を含む、前記プロセス。 - 請求項11に記載のプロセスによって得ることができるカプセル化された組成物。
- デンプンマトリックスの特性、とりわけデンプンマトリックスに封入された少なくとも1つの香料および/または化粧品成分を含むカプセル化された組成物の特性、より具体的には、請求項1~10のいずれか一項に記載の組成物の特性を改変するためのヘミセルロースの使用。
- 請求項1~10のいずれか一項に記載のカプセル化された組成物を含む、消費者製品、好ましくはパーソナルケア製品、さらにより好ましくはデオドラントまたは制汗剤。
- パーソナルケア製品、とりわけデオドラントまたは制汗剤中の少なくとも1つの香料および/または化粧品成分の量を低減するための、請求項1~10のいずれか一項に記載のカプセル化された組成物の使用。
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