JP2020527563A - ５−フルオロ−４−イミノ−３−メチル−１−トシル−３，４−ジヒドロピリミジン−２−オンの多形体 - Google Patents

５−フルオロ−４−イミノ−３−メチル−１−トシル−３，４−ジヒドロピリミジン−２−オンの多形体 Download PDF

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JP2020527563A
JP2020527563A JP2020502159A JP2020502159A JP2020527563A JP 2020527563 A JP2020527563 A JP 2020527563A JP 2020502159 A JP2020502159 A JP 2020502159A JP 2020502159 A JP2020502159 A JP 2020502159A JP 2020527563 A JP2020527563 A JP 2020527563A
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solution
compound
mixture
crystalline
composition
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JP2020527563A5 (enExample
Inventor
グラバニク，ミカエル
スエズ，ガル
ネメット，ゾルターン
アラシビ，サマア
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アダマ・マクテシム・リミテッド
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Publication of JP2020527563A publication Critical patent/JP2020527563A/ja
Publication of JP2020527563A5 publication Critical patent/JP2020527563A5/ja
Priority to JP2023118871A priority Critical patent/JP2023145572A/ja
Priority to JP2025124685A priority patent/JP2025163080A/ja
Pending legal-status Critical Current

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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/54—1,3-Diazines; Hydrogenated 1,3-diazines
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01P—BIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
    • A01P3/00—Fungicides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
    • C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
    • C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
    • C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
    • C07D239/46—Two or more oxygen, sulphur or nitrogen atoms
    • C07D239/47—One nitrogen atom and one oxygen or sulfur atom, e.g. cytosine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Environmental Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Zoology (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • General Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • Health & Medical Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
JP2020502159A 2017-07-17 2018-07-16 ５−フルオロ−４−イミノ−３−メチル−１−トシル−３，４−ジヒドロピリミジン−２−オンの多形体 Pending JP2020527563A (ja)

Priority Applications (2)

Application Number Priority Date Filing Date Title
JP2023118871A JP2023145572A (ja) 2017-07-17 2023-07-21 ５－フルオロ－４－イミノ－３－メチル－１－トシル－３，４－ジヒドロピリミジン－２－オンの多形体
JP2025124685A JP2025163080A (ja) 2017-07-17 2025-07-25 ５－フルオロ－４－イミノ－３－メチル－１－トシル－３，４－ジヒドロピリミジン－２－オンの多形体

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201762533509P 2017-07-17 2017-07-17
US62/533,509 2017-07-17
PCT/IB2018/000875 WO2019038583A1 (en) 2017-07-17 2018-07-16 5-FLUORO-4-IMINO-3-METHYL-1-TOSYL-3,4-DIHYDROPYRIMIDIN-2-ONE POLYMORPHS

Related Child Applications (1)

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JP2023118871A Division JP2023145572A (ja) 2017-07-17 2023-07-21 ５－フルオロ－４－イミノ－３－メチル－１－トシル－３，４－ジヒドロピリミジン－２－オンの多形体

Publications (2)

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JP2020527563A true JP2020527563A (ja) 2020-09-10
JP2020527563A5 JP2020527563A5 (enExample) 2021-08-26

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JP2020502159A Pending JP2020527563A (ja) 2017-07-17 2018-07-16 ５−フルオロ−４−イミノ−３−メチル−１−トシル−３，４−ジヒドロピリミジン−２−オンの多形体
JP2023118871A Pending JP2023145572A (ja) 2017-07-17 2023-07-21 ５－フルオロ－４－イミノ－３－メチル－１－トシル－３，４－ジヒドロピリミジン－２－オンの多形体
JP2025124685A Pending JP2025163080A (ja) 2017-07-17 2025-07-25 ５－フルオロ－４－イミノ－３－メチル－１－トシル－３，４－ジヒドロピリミジン－２－オンの多形体

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JP2023118871A Pending JP2023145572A (ja) 2017-07-17 2023-07-21 ５－フルオロ－４－イミノ－３－メチル－１－トシル－３，４－ジヒドロピリミジン－２－オンの多形体
JP2025124685A Pending JP2025163080A (ja) 2017-07-17 2025-07-25 ５－フルオロ－４－イミノ－３－メチル－１－トシル－３，４－ジヒドロピリミジン－２－オンの多形体

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Country Link
US (1) US11632954B2 (enExample)
EP (1) EP3655396A1 (enExample)
JP (3) JP2020527563A (enExample)
CN (2) CN118515619A (enExample)
AR (1) AR112276A1 (enExample)
AU (1) AU2018320492C1 (enExample)
CA (1) CA3069619A1 (enExample)
IL (5) IL309708B1 (enExample)
MA (1) MA49639A (enExample)
WO (1) WO2019038583A1 (enExample)
ZA (1) ZA202000411B (enExample)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EA202191250A1 (ru) 2018-11-05 2021-08-20 Адама Мактешим Лтд. Смеси и композиции, включающие 5-фтор-4-имино-3-метил-1-тозил-3,4-дигидропиримидин-2-он, и способы их применения
JP2022541318A (ja) * 2019-07-22 2022-09-22 アダマ・マクテシム・リミテッド 殺菌組合せ物、混合物および組成物、ならびにそれらの使用
US12466796B2 (en) * 2019-09-23 2025-11-11 Adama Makhteshim Ltd. Process for preparing 5-(fluoro-4-imino-3-methyl)-1-tosyl-3,4 dihydropyrimidine-(1H)-one and derivatives of the compound
AU2021267206A1 (en) * 2020-05-04 2022-12-08 Adama Makhteshim Ltd. Mixtures and compositions comprising 5-fluoro-4-imino-3- methyl-1-tosyl-3,4-dihydropyrimidin-2-one, and methods of use thereof
CA3206570A1 (en) 2021-01-27 2022-08-04 Alexandra ROSENMUND 5-fluoro-4-imino-3-methyl-1-tosyl-3,4-dihydropyrimidin-2(1 h)-one for controlling plant diseases
CA3216622A1 (en) 2021-05-04 2022-11-10 Stefano Luca Giaffreda Crystalline forms of 5-fluoro-4-imino-3-methyl-1-tosyl-3,4- dihydropyrimidin-2-one, and mixtures, compositions and methods of use thereof
AU2023227455A1 (en) 2022-03-03 2024-09-19 Adama Makhteshim Ltd. Fungicidal combinations, mixtures and compositions and uses thereof
CA3257550A1 (en) 2022-05-26 2023-11-30 Adama Makhteshim Ltd. FUNGICIDAL COMBINATIONS, MIXTURES AND COMPOSITIONS AND THEIR USES
EP4565066A1 (en) 2022-08-03 2025-06-11 Adama Makhteshim Ltd. 5-fluoro-4-imino-3-methyl-1-tosyl-3,4-dihydropyrimidin-2(1h)-one for fungicide-resistant fungus
AU2024233301A1 (en) 2023-03-09 2025-09-18 Adama Makhteshim Ltd. Fungicidal combinations, mixtures and compositions and uses thereof
WO2024189563A1 (en) 2023-03-14 2024-09-19 Adama Makhteshim Ltd. Liquid compositions containing 5-(fluoro-4-imino-3-methyl)-1-tosyl-3,4 dihydropyrimidine-(1h)-one and derivatives thereof and a uv absorber
AR132381A1 (es) 2023-04-11 2025-06-18 Adama Makhteshim Ltd Compuestos y procesos relativos a flumetilsulforim
WO2025046581A1 (en) 2023-08-31 2025-03-06 Adama Makhteshim Ltd. Fungicidal combinations, mixtures and compositions and uses thereo
WO2025114931A1 (en) 2023-11-28 2025-06-05 Adama Makhteshim Ltd. Fungicidal combinations, mixtures and compositions and uses thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010517995A (ja) * 2007-02-01 2010-05-27 マクテシム・ケミカル・ワークス・リミテツド ３−（ｅ）−２−｛２−［６−（２−シアノフェノキシ）ピリミジン−４−イルオキシ］フェニル｝−３−メトキシアクリレートの多形体
JP2016503816A (ja) * 2012-12-31 2016-02-08 ダウ アグロサイエンシィズ エルエルシー 殺真菌剤としての３−アルキル−５−フルオロ−４置換イミノ−３，４−ジヒドロピリミジン−２（１ｈ）−オン誘導体
WO2016106138A1 (en) * 2014-12-23 2016-06-30 Dow Agrosciences Llc 5-fluoro-4-imino-3-(alkyl/substituted alkyl)-1-(arylsulfonyl)-3,4-dihydropyrimidin-2(1h)-one as a seed treatment
JP2017501197A (ja) * 2013-12-31 2017-01-12 アダマ・マクテシム・リミテッド ５−フルオロ−４−イミノ−３−（アルキル／置換アルキル）−１−（アリールスルホニル）−３，４−ジヒドロピリミジン−２（１ｈ）−オンおよびそれらの調製方法

Family Cites Families (37)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3309359A (en) 1965-10-22 1967-03-14 Hoffmann La Roche N-mono-acyl-5-fluorocytosine derivatives and process
US3368938A (en) 1966-01-13 1968-02-13 Hoffmann La Roche Controlling fungi with 5-fluorocytosine
US3635977A (en) 1969-11-03 1972-01-18 American Cyanamid Co Certain 6-trifluoromethylcytosines and thiocytosines their synthesis and their use in the synthesis of uracisls and thiouracil
US3868373A (en) 1970-01-27 1975-02-25 Hoffmann La Roche 4-Amino-5-fluoro-2-tri(lower alkyl) silyloxypyrimidines
US4009272A (en) 1971-10-23 1977-02-22 Bayer Aktiengesellschaft Penicillins
US4845081A (en) 1984-10-18 1989-07-04 University Of Florida Aminomethyl derivatives of biologically active substances, and enhanced delivery thereof across topical membranes
DE3821711A1 (de) 1988-06-28 1990-02-08 Bayer Ag Thiazolopyrimidin-derivate, verfahren zu ihrer herstellung und ihre verwendung als schaedlingsbekaempfungsmittel
JP3217191B2 (ja) 1992-07-16 2001-10-09 ビーエーエスエフ アクチェンゲゼルシャフト ヘテロ芳香族化合物およびこれを含有する植物保護剤
PL324486A1 (en) 1995-07-05 1998-05-25 Du Pont Fungicidal pyrimidinones
GT199900185A (es) 1998-11-06 2001-04-18 Novedosa pirimidin-4-enamina como fungicida.
WO2003018051A1 (en) 2001-08-27 2003-03-06 Vic Jira Anti-fungal composition
US20080269238A1 (en) 2004-04-01 2008-10-30 Takeda Pharmaceutical Company Limited Thiazolopyrimidine Derivative
JP4887500B2 (ja) 2004-09-16 2012-02-29 国立大学法人岐阜大学 ヌクレオシド類似体またはその塩
US8679514B2 (en) 2005-07-27 2014-03-25 Basf Se Fungicidal mixtures based on azolopyrimidinylamines
TWI402034B (zh) 2005-07-28 2013-07-21 Dow Agrosciences Llc 具有被層狀液晶覆膜包覆之油球之水包油乳化劑之農用組成物
IL172137A0 (en) * 2005-11-23 2006-04-10 Maktheshim Chemical Works Ltd Process for prep aring pyridinamines
WO2008005303A2 (en) 2006-06-30 2008-01-10 Janssen Pharmaceutica N.V. Thiazolopyrimidine modulators of trpv1
US20100029483A1 (en) 2006-10-16 2010-02-04 Rhodia Inc. Agricultural adjuvant compositions, pesticide compositions, and methods for using such compositions
US8093245B2 (en) 2006-12-14 2012-01-10 Lexicon Pharmaceuticals, Inc. 4-amino-1H-pyrimidin-2-one based compounds, compositions comprising them and methods of their use
US8314087B2 (en) 2007-02-16 2012-11-20 Amgen Inc. Nitrogen-containing heterocyclyl ketones and methods of use
UA107445C2 (uk) 2008-01-22 2015-01-12 ДАУ АГРОСАЙЄНСІЗ ЕлЕлСі 5-фторпіримідинові похідні як фунгіциди
US20100284959A1 (en) 2008-01-23 2010-11-11 Gene Arrest Ltd. Sequence specific double-stranded dna/rna binding compounds and uses thereof
UA107651C2 (en) 2008-08-01 2015-02-10 Dow Agrosciences Llc Use of 5-fluorocytosine as a fungicide
BRPI1010111A2 (pt) 2009-06-18 2015-08-25 Basf Se Mistura fungicida, fungicida, composto de triazol, uso de uma mistura fungicida, composição agroquímica, semente e método para o controle de fungos patogênicos
PL2462134T3 (pl) 2009-08-07 2014-10-31 Adama Makhteshim Ltd Pochodne n1-sulfonylo-5-fluoropirymidynonu
UA112284C2 (uk) 2009-08-07 2016-08-25 ДАУ АГРОСАЙЄНСІЗ ЕлЕлСі Похідні 5-фторпіримідинону
US8318758B2 (en) 2009-08-07 2012-11-27 Dow Agrosciences, Llc 5-fluoro-2-oxopyrimidine-1(2H)-carboxylate derivatives
UA107671C2 (en) 2009-08-07 2015-02-10 Dow Agrosciences Llc N1-substityted-5-fluoro-2-oxopyrimidinone-1(2h)-carboxamide derivatives
UA106889C2 (uk) 2009-08-07 2014-10-27 ДАУ АГРОСАЙЄНСІЗ ЕлЕлСі Похідні n1-ацил-5-фторпіримідинону
UA106246C2 (ru) 2009-10-07 2014-08-11 ДАУ АГРОСАЙЄНСІЗ ЕлЕлСі Синергическая фунгицидная композиция, которая содержит 5-фторцитозин для борьбы с грибковыми болезнями зерновых культур
MX2012012530A (es) 2010-04-26 2012-12-17 Dow Agrosciences Llc Derivados de n1-sulfonil-5-fluorpirimidinona.
US20120208700A1 (en) 2011-02-11 2012-08-16 Dow Agrosciences Llc Stable agrochemical oil dispersions
JP6128658B2 (ja) 2011-08-17 2017-05-17 アダマ・マクテシム・リミテッド ５−フルオロ−４−イミノ−３−（置換）−３，４−ジヒドロピリミジン−２−（１ｈ）−オン誘導体
UA117123C2 (uk) 2012-12-28 2018-06-25 Адама Махтешім Лтд. Похідні 1-(заміщений бензоїл)-5-фтор-4-іміно-3-метил-3,4-дигідропіримідин-2(1h)-ону
UA117743C2 (uk) 2012-12-28 2018-09-25 Адама Махтешім Лтд. N-(заміщені)-5-фтор-4-іміно-3-метил-2-оксо-3,4-дигідропіримідин-1(2h)-карбоксамідні похідні
TWI652012B (zh) * 2013-05-20 2019-03-01 杜邦股份有限公司 殺真菌吡唑的固態形式
NZ722436A (en) 2013-12-31 2018-01-26 Adama Makhteshim Ltd Synergistic fungicidal mixtures and compositions for fungal control

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010517995A (ja) * 2007-02-01 2010-05-27 マクテシム・ケミカル・ワークス・リミテツド ３−（ｅ）−２−｛２−［６−（２−シアノフェノキシ）ピリミジン−４−イルオキシ］フェニル｝−３−メトキシアクリレートの多形体
JP2016503816A (ja) * 2012-12-31 2016-02-08 ダウ アグロサイエンシィズ エルエルシー 殺真菌剤としての３−アルキル−５−フルオロ−４置換イミノ−３，４−ジヒドロピリミジン−２（１ｈ）−オン誘導体
JP2017501197A (ja) * 2013-12-31 2017-01-12 アダマ・マクテシム・リミテッド ５−フルオロ−４−イミノ−３−（アルキル／置換アルキル）−１−（アリールスルホニル）−３，４−ジヒドロピリミジン−２（１ｈ）−オンおよびそれらの調製方法
JP2017502963A (ja) * 2013-12-31 2017-01-26 アダマ・マクテシム・リミテッド ５−フルオロ−４−イミノ−３−（アルキル／置換アルキル）−１−（アリールスルホニル）−３，４−ジヒドロピリミジン−２（１ｈ）−オンおよびそれらの調製方法
WO2016106138A1 (en) * 2014-12-23 2016-06-30 Dow Agrosciences Llc 5-fluoro-4-imino-3-(alkyl/substituted alkyl)-1-(arylsulfonyl)-3,4-dihydropyrimidin-2(1h)-one as a seed treatment

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
平山令明, 有機化合物結晶作製ハンドブック, JPN6014035600, 2008, pages 17 - 23, ISSN: 0005016703 *

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CN111094252A (zh) 2020-05-01
AR112276A1 (es) 2019-10-09
AU2018320492A1 (en) 2020-02-13
IL323266A (en) 2025-11-01
AU2018320492C1 (en) 2023-07-13
JP2023145572A (ja) 2023-10-11
IL271950B2 (en) 2024-06-01
BR112020000953A2 (pt) 2020-07-14
IL309708A (en) 2024-02-01
EP3655396A1 (en) 2020-05-27
CN111094252B (zh) 2024-05-24
JP2025163080A (ja) 2025-10-28
US20200229437A1 (en) 2020-07-23
AU2018320492B2 (en) 2022-12-01
CA3069619A1 (en) 2019-02-28
CN118515619A (zh) 2024-08-20
WO2019038583A1 (en) 2019-02-28
IL271950B1 (en) 2024-02-01
IL271950A (en) 2020-02-27
NZ761039A (en) 2023-09-29
US11632954B2 (en) 2023-04-25
ZA202000411B (en) 2023-10-25
MA49639A (fr) 2020-05-27
IL323267A (en) 2025-11-01
IL309708B1 (en) 2025-10-01
IL323268A (en) 2025-11-01

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