JP2020033297A - 化粧料および洗浄料 - Google Patents
化粧料および洗浄料 Download PDFInfo
- Publication number
- JP2020033297A JP2020033297A JP2018160878A JP2018160878A JP2020033297A JP 2020033297 A JP2020033297 A JP 2020033297A JP 2018160878 A JP2018160878 A JP 2018160878A JP 2018160878 A JP2018160878 A JP 2018160878A JP 2020033297 A JP2020033297 A JP 2020033297A
- Authority
- JP
- Japan
- Prior art keywords
- cosmetic
- oil
- cosmetics
- component
- cleaning agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 57
- 239000003599 detergent Substances 0.000 title claims abstract description 9
- 125000000217 alkyl group Chemical group 0.000 claims abstract description 14
- 125000004432 carbon atom Chemical group C* 0.000 claims abstract description 14
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 11
- 125000002924 primary amino group Chemical class [H]N([H])* 0.000 claims abstract 3
- 125000000467 secondary amino group Chemical class [H]N([*:1])[*:2] 0.000 claims abstract 3
- 239000012459 cleaning agent Substances 0.000 claims description 44
- -1 cationic polysaccharide Chemical class 0.000 claims description 36
- 239000002826 coolant Substances 0.000 claims description 14
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical group CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 13
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 13
- 229940041616 menthol Drugs 0.000 claims description 13
- 239000003945 anionic surfactant Substances 0.000 claims description 8
- UJNOLBSYLSYIBM-WISYIIOYSA-N [(1r,2s,5r)-5-methyl-2-propan-2-ylcyclohexyl] (2r)-2-hydroxypropanoate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(=O)[C@@H](C)O UJNOLBSYLSYIBM-WISYIIOYSA-N 0.000 claims description 6
- GPLRAVKSCUXZTP-UHFFFAOYSA-N diglycerol Chemical compound OCC(O)COCC(O)CO GPLRAVKSCUXZTP-UHFFFAOYSA-N 0.000 claims description 6
- ZYTMANIQRDEHIO-KXUCPTDWSA-N isopulegol Chemical compound C[C@@H]1CC[C@@H](C(C)=C)[C@H](O)C1 ZYTMANIQRDEHIO-KXUCPTDWSA-N 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
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- 239000005017 polysaccharide Substances 0.000 claims description 6
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 claims description 5
- 241000723346 Cinnamomum camphora Species 0.000 claims description 5
- 229930008380 camphor Natural products 0.000 claims description 5
- 229960000846 camphor Drugs 0.000 claims description 5
- 239000001525 mentha piperita l. herb oil Substances 0.000 claims description 4
- 235000019477 peppermint oil Nutrition 0.000 claims description 4
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 claims description 3
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 claims description 3
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- MDVYIGJINBYKOM-UHFFFAOYSA-N 3-[[5-Methyl-2-(1-methylethyl)cyclohexyl]oxy]-1,2-propanediol Chemical compound CC(C)C1CCC(C)CC1OCC(O)CO MDVYIGJINBYKOM-UHFFFAOYSA-N 0.000 claims description 3
- OFOBLEOULBTSOW-UHFFFAOYSA-L Malonate Chemical compound [O-]C(=O)CC([O-])=O OFOBLEOULBTSOW-UHFFFAOYSA-L 0.000 claims description 3
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- 239000012190 activator Substances 0.000 claims description 3
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 claims description 3
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- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 claims description 3
- 125000000524 functional group Chemical group 0.000 claims description 3
- 235000001050 hortel pimenta Nutrition 0.000 claims description 3
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 3
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- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 3
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- 235000014113 dietary fatty acids Nutrition 0.000 description 16
- 239000000194 fatty acid Substances 0.000 description 16
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- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 description 15
- 239000000203 mixture Substances 0.000 description 13
- 239000000843 powder Substances 0.000 description 13
- 150000003335 secondary amines Chemical class 0.000 description 13
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 12
- 150000004665 fatty acids Chemical class 0.000 description 11
- 239000004166 Lanolin Substances 0.000 description 10
- 238000009472 formulation Methods 0.000 description 10
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- 229940039717 lanolin Drugs 0.000 description 10
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 10
- 239000011734 sodium Substances 0.000 description 10
- 229910052708 sodium Inorganic materials 0.000 description 10
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 9
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- 239000003240 coconut oil Substances 0.000 description 9
- 229920001577 copolymer Polymers 0.000 description 9
- 238000011156 evaluation Methods 0.000 description 9
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- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 8
- 235000019864 coconut oil Nutrition 0.000 description 8
- NOPFSRXAKWQILS-UHFFFAOYSA-N docosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCO NOPFSRXAKWQILS-UHFFFAOYSA-N 0.000 description 8
- 239000000049 pigment Substances 0.000 description 8
- 150000003141 primary amines Chemical class 0.000 description 8
- SUZRRICLUFMAQD-UHFFFAOYSA-N N-Methyltaurine Chemical compound CNCCS(O)(=O)=O SUZRRICLUFMAQD-UHFFFAOYSA-N 0.000 description 7
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 7
- 239000002280 amphoteric surfactant Substances 0.000 description 7
- 238000013329 compounding Methods 0.000 description 7
- 239000002453 shampoo Substances 0.000 description 7
- 229960003080 taurine Drugs 0.000 description 7
- ZDSCFBCGDDCJFZ-UHFFFAOYSA-N 2-(methylamino)ethanesulfonic acid;sodium Chemical compound [Na].CNCCS(O)(=O)=O ZDSCFBCGDDCJFZ-UHFFFAOYSA-N 0.000 description 6
- 239000002253 acid Substances 0.000 description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 239000004205 dimethyl polysiloxane Substances 0.000 description 6
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 6
- 239000003205 fragrance Substances 0.000 description 6
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- 239000007787 solid Substances 0.000 description 6
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 6
- ALYNCZNDIQEVRV-UHFFFAOYSA-N 4-aminobenzoic acid Chemical compound NC1=CC=C(C(O)=O)C=C1 ALYNCZNDIQEVRV-UHFFFAOYSA-N 0.000 description 5
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 5
- 239000006096 absorbing agent Substances 0.000 description 5
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 5
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- 239000011591 potassium Substances 0.000 description 5
- 229910052700 potassium Inorganic materials 0.000 description 5
- 239000003755 preservative agent Substances 0.000 description 5
- 239000001993 wax Substances 0.000 description 5
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 4
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 description 4
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- 229940005581 sodium lactate Drugs 0.000 description 1
- 235000011088 sodium lactate Nutrition 0.000 description 1
- 229940082004 sodium laurate Drugs 0.000 description 1
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 description 1
- 235000019333 sodium laurylsulphate Nutrition 0.000 description 1
- 229940045845 sodium myristate Drugs 0.000 description 1
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 1
- 229940045870 sodium palmitate Drugs 0.000 description 1
- 229940045920 sodium pyrrolidone carboxylate Drugs 0.000 description 1
- IWIUXJGIDSGWDN-UQKRIMTDSA-M sodium;(2s)-2-(dodecanoylamino)pentanedioate;hydron Chemical compound [Na+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CCC(O)=O IWIUXJGIDSGWDN-UQKRIMTDSA-M 0.000 description 1
- KKDONKAYVYTWGY-UHFFFAOYSA-M sodium;2-(methylamino)ethanesulfonate Chemical compound [Na+].CNCCS([O-])(=O)=O KKDONKAYVYTWGY-UHFFFAOYSA-M 0.000 description 1
- HYRLWUFWDYFEES-UHFFFAOYSA-M sodium;2-oxopyrrolidine-1-carboxylate Chemical compound [Na+].[O-]C(=O)N1CCCC1=O HYRLWUFWDYFEES-UHFFFAOYSA-M 0.000 description 1
- CVYDEWKUJFCYJO-UHFFFAOYSA-M sodium;docosanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCCCCCC([O-])=O CVYDEWKUJFCYJO-UHFFFAOYSA-M 0.000 description 1
- GGXKEBACDBNFAF-UHFFFAOYSA-M sodium;hexadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCC([O-])=O GGXKEBACDBNFAF-UHFFFAOYSA-M 0.000 description 1
- RUTSRVMUIGMTHJ-UHFFFAOYSA-M sodium;tetradec-1-ene-1-sulfonate Chemical compound [Na+].CCCCCCCCCCCCC=CS([O-])(=O)=O RUTSRVMUIGMTHJ-UHFFFAOYSA-M 0.000 description 1
- JUQGWKYSEXPRGL-UHFFFAOYSA-M sodium;tetradecanoate Chemical compound [Na+].CCCCCCCCCCCCCC([O-])=O JUQGWKYSEXPRGL-UHFFFAOYSA-M 0.000 description 1
- 235000002316 solid fats Nutrition 0.000 description 1
- 229950003429 sorbitan palmitate Drugs 0.000 description 1
- 229960002920 sorbitol Drugs 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 229940032094 squalane Drugs 0.000 description 1
- 229940031439 squalene Drugs 0.000 description 1
- TUHBEKDERLKLEC-UHFFFAOYSA-N squalene Natural products CC(=CCCC(=CCCC(=CCCC=C(/C)CCC=C(/C)CC=C(C)C)C)C)C TUHBEKDERLKLEC-UHFFFAOYSA-N 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003871 sulfonates Chemical class 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 230000000475 sunscreen effect Effects 0.000 description 1
- 239000000516 sunscreening agent Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- SHWIJIJNPFXOFS-UHFFFAOYSA-N thiotaurine Chemical compound NCCS(O)(=O)=S SHWIJIJNPFXOFS-UHFFFAOYSA-N 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 229960001295 tocopherol Drugs 0.000 description 1
- 235000010384 tocopherol Nutrition 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 235000015961 tonic Nutrition 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
- 229960000716 tonics Drugs 0.000 description 1
- DQFBYFPFKXHELB-VAWYXSNFSA-N trans-chalcone Chemical compound C=1C=CC=CC=1C(=O)\C=C\C1=CC=CC=C1 DQFBYFPFKXHELB-VAWYXSNFSA-N 0.000 description 1
- 235000001019 trigonella foenum-graecum Nutrition 0.000 description 1
- QPQANCNBWQXGTQ-UHFFFAOYSA-N trihydroxy(trimethylsilylperoxy)silane Chemical compound C[Si](C)(C)OO[Si](O)(O)O QPQANCNBWQXGTQ-UHFFFAOYSA-N 0.000 description 1
- 229940117985 trimethyl pentaphenyl trisiloxane Drugs 0.000 description 1
- UUJLHYCIMQOUKC-UHFFFAOYSA-N trimethyl-[oxo(trimethylsilylperoxy)silyl]peroxysilane Chemical compound C[Si](C)(C)OO[Si](=O)OO[Si](C)(C)C UUJLHYCIMQOUKC-UHFFFAOYSA-N 0.000 description 1
- VLPFTAMPNXLGLX-UHFFFAOYSA-N trioctanoin Chemical compound CCCCCCCC(=O)OCC(OC(=O)CCCCCCC)COC(=O)CCCCCCC VLPFTAMPNXLGLX-UHFFFAOYSA-N 0.000 description 1
- 229960005066 trisodium edetate Drugs 0.000 description 1
- 229940045136 urea Drugs 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- 239000010497 wheat germ oil Substances 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 239000001052 yellow pigment Substances 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
- 229910001928 zirconium oxide Inorganic materials 0.000 description 1
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
- OENHQHLEOONYIE-JLTXGRSLSA-N β-Carotene Chemical compound CC=1CCCC(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C OENHQHLEOONYIE-JLTXGRSLSA-N 0.000 description 1
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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Abstract
Description
例えば、清涼化剤とカチオン型界面活性剤を併用することにより、清涼感が向上することが知られている(特許文献1参照)。しかし、洗浄剤に配合しようとすると、含まれるアニオン性界面活性剤と複合体を形成してしまい、安定に配合して効果を発揮することができなかった。
また、メントールやカンファーといった清涼化剤と脂肪酸イソプロピルを併用することにより、清涼感が向上することが知られている(特許文献2参照)。しかし、しっとりさや泡立ちに満足できなかった。
また、清涼化剤と、トウガラシチンキ、ショウキョウチンキなど(特許文献3参照)やバニリルブチルエーテル(特許文献4参照)等の温感剤と、を併用することにより、清涼感が向上することが知られている。しかし、清涼化剤または温感剤の量を増やすと皮膚や眼への刺激を強めてしまい、清涼感に改善の余地があるものであった。
(a)清涼化剤
(b)分子内にアミド結合および炭素数10以上のアルキル鎖を有さない1級アミンおよび/または2級アミン 0.1〜1.2質量%
前記化粧料および洗浄料において、(b)1級アミンが下記式(I)で示されることが好適である。
(化1)
NH2−C(R1)2−CH2−R2 (I)
式(I)中、R1は水素原子またはメチル基、R2はOH、SO2H、SO2SH、SO3Hから選択される官能基である。
前記化粧料および洗浄料において、(b)2級アミンが下記式(II)で示されることが好適である。
(化2)
NHR3−CH2−CH2−R4 (II)
式(II)中、R3は炭素数1〜9のアルキル基、R2はOH、SO2H、SO2SH、SO3Hから選択されるいずれかである。
前記化粧料および洗浄料において、(a)成分の配合量が0.2〜1.2質量%であることが好適である。
前記化粧料および洗浄料において、pHが6.5以下であることが好適である。
前記化粧料および洗浄料において、(b)成分と(a)成分の配合比である(b)/(a)=0.01〜20であることが好適である。
前記化粧料および洗浄料において、(a)清涼化剤が、メントール、ハッカ油、l−メンチルグリセリルエーテル、乳酸メンチル、カンファー、イソプレゴール、ボルネオロール、シネオールメントン、スペアミント、ペパーミント、マロン酸メンチル、グリコシル−モノ−メンチル−O−アセテート、3−L−メントキシプロパン−1,2−ジオール、1−メンチル−3−ヒドロキシブチレートからなる群から選択される1種または2種以上のTRP M8活性化物質であることが好適である。
前記化粧料および洗浄料において、カチオン性多糖類 0.1〜1.0質量%を含むことが好適である。
前記化粧料および洗浄料において、アニオン性界面活性剤を含むことが好適である。
本発明にかかる化粧料および洗浄料は、(a)成分および(b)成分を含むことを特徴とする。
(a)清涼化剤
(b)分子内にアミド結合および炭素数10以上のアルキル鎖を有さない1級アミンおよび/または2級アミン 0.1〜1.2質量%
清涼化剤は、化粧料および洗浄料に通常使用されるものを用いることができる。
また、メントール、ハッカ油、l−メンチルグリセリルエーテル、乳酸メンチルであることがより好ましい。
配合量が1.2質量%を超えると、皮膚や眼に対して痛く感じる刺激が強くなり過ぎるため、好ましくない。
分子内にアミド結合および炭素数10以上のアルキル鎖を有さない1級アミンまたは2級アミンおよび/または2級アミンとしては、化粧料および洗浄料に通常使用されるものを用いることができる。
(化3)
NH2−C(R1)2−CH2−R2 (I)
式(I)中、R1は水素原子またはメチル基、R2はOH、SO2H、SO2SH、SO3Hから選択される官能基である。
(化4)
NHR3−CH2−CH2−R4 (II)
式(II)中、R3は炭素数1〜9のアルキル基、R2はOH、SO2H、SO2SH、SO3Hから選択されるいずれかである。
タウリンの市販品としては、例えば、アミノエチルスルホン酸(相互薬工株式会社製)等が挙げられる。また、N−メチルタウリンを含む市販品としては、MTS−50(クラリアント株式会社製)等が挙げられる。
配合量が1.2質量%を超えると、清涼感に劣る場合や組成物の粘性を高められない場合、使用後のベタツキを著しく高めてしまう場合がある。
カチオン性多糖類としては、例えば、カチオン化グアガム、カチオン化セルロース、カチオン化ローカストビーンガム、カチオン化タラガム、カチオン化フェヌクリークガム、カチオン化デンプン等が挙げられる。
アニオン性界面活性剤としては、例えば、ラウリン酸ナトリウム、ラウリン酸カリウム、ヤシ油脂肪酸ナトリウム、ヤシ油脂肪酸カリウム、ミリスチン酸ナトリウム、ミリスチン酸カリウム、パルミチン酸ナトリウム、パルミチン酸カリウム、パルミチン酸トリエタノールアミン、ステアリン酸ナトリウム、ステアリン酸カリウム、ベヘン酸ナトリウム、ベヘン酸カリウム等の高級脂肪酸塩;ポリオキシエチレンラウリルエーテル硫酸ナトリウム、ポリオキシエチレンラウリルエーテル硫酸アンモニウム、ポリオキシエチレンラウリルエーテル硫酸トリエタノールアミン等のアルキルエーテル硫酸塩;ラウリル硫酸ナトリウム、ラウリル硫酸トリエタノールアミン等のアルキル硫酸塩;テトラデセンスルホン酸ナトリウム、テトラデセンスルホン酸カリウム等のα−オレフィンスルホン酸塩;N−ラウロイル−L−グルタミン酸ナトリウム、N−ラウロイル−L−グルタミン酸アンモニウム、N−ヤシ油脂肪酸アシル−L−グルタミン酸ナトリウム、N−ヤシ油脂肪酸アシル−L−グルタミン酸トリエタノールアミン、N−ラウロイルサルコシンナトリウム、N−ヤシ油脂肪酸アシルサルコシンナトリウム、N−ラウロイル−N−メチルβ−アラニンカリウム等のN−アシルアミノ酸塩;N−ラウロイルイセチオン酸ナトリウム、N−ラウロイルイセチオン酸カリウム等のアシルイセチオン酸塩;N−ヤシ油脂肪酸メチルタウリンナトリウム、N−ラウロイルメチルタウリンナトリウム、N−ヤシ油脂肪酸メチルタウリンカリウム等のN−アシルアルキルタウリン塩;ポリオキシエチレンスルホコハク酸ラウリル二ナトリウム等のスルホコハク酸エステル塩;ヤシ油脂肪酸加水分解コラーゲンカリウム等のN−アシルポリペプチド塩;ポリオキシエチレンラウリルエーテルリン酸ナトリウム等のアルキルエーテルリン酸塩;ドデカン−1,2−ジオール酢酸エーテルナトリウム等のヒドロキシエーテルカルボン酸塩;ポリオキシエチレンラウリルエーテル酢酸塩等のアルキルエーテルカルボン酸塩等が挙げられる。
天然動植物油及び半合成油としては、アボガド油、アマニ油、アーモンド油、オリーブ油、カヤ油、肝油、キョウニン油、小麦胚芽油、ゴマ油、コメ胚芽油、コメヌカ油、サザンカ油、サフラワー油、シナギリ油、シナモン油、タートル油、大豆油、茶実油、ツバキ油、月見草油、トウモロコシ油、ナタネ油、日本キリ油、胚芽油、パーシック油、パーム油、レッドパーム油、パーム核油、ヒマシ油、ヒマワリ油、ブドウ油、ホホバ油、マカデミアナッツ油、綿実油、ヤシ油、トリヤシ油脂肪酸グリセライド、落花生油、液状ラノリン、還元ラノリン、ラノリンアルコール、酢酸ラノリン、ラノリン脂肪酸イソプロピル、POEラノリンアルコールエーテル、POEラノリンアルコールアセテート、ラノリン脂肪酸ポリエチレングリコール、POE水素添加ラノリンアルコールエーテル、卵黄油等が挙げられる。
実施例の説明に先立ち本発明で用いた評価試験方法について説明する。
各サンプルを調製後、透明のガラス容器にて15℃にて2週間静置保管した後、外観を判定した。
○:透明であり、異物が浮遊・沈降していない。
×:透明でない、又は、異物が浮遊・沈降している。
専門パネル5名が、半頭比較の実使用評価試験にて、試験例1−1(基準品のシャンプー)に対するシャンプー泡立て中の清涼感の強弱を次の通り、評価した。
◎:専門パネル5名中、4名以上が「清涼感が強まった」と評価した。
○:専門パネル5名中、2名または3名が「清涼感が強まった」と評価した。
×:専門パネル5名中、「清涼感が強まった」と評価した人は1名以下であった。
専門パネル5名が、半頭比較の実使用評価試験にて、シャンプー使用時の泡のクリーミーさについて、次の通り、評価した。
◎:専門パネル5名中、4名以上が「とてもクリーミー」と評価した。
○:専門パネル5名中、2名または3名が「とてもクリーミー」と評価した。
△:専門パネル5名中、1名が「とてもクリーミー」と評価した。
×:専門パネル5名中、「とてもクリーミー」と評価した人はいなかった。
分子内にアミド結合を有する尿素、ヒドロキシエチル尿素、ピロリドンカルボン酸ナトリウムは、清涼感を向上させる効果がなかった。
また、3級アミンであるEDTA 2Na・2H2Oとトリエタノールアミンも、清涼感を向上させる効果がなかった。
また、4級アミンであるトリメチルグリシンも、清涼感を向上させる効果がなかった。
これに対して、タウリン、2−アミノ−2−メチル−1−プロパノール、N−メチルタウリンナトリウムを配合した頭髪洗浄料は、メントールが有する清涼感より優れた清涼感を有していた。
また、pHが6.5以下であることが好ましい。
これに対して、カチオン性ポリマーであるポリクオタニウム−7(試験例3−2)や(プロピルトリモニウムクロリドアクリルアミド/ジメチルアクリルアミド)コポリマー(試験例3−3)を配合した頭髪化粧料は、清涼感および泡のクリーミーさに改善の余地があるものであった。
メントール 0.6 質量%
N−メチルタウリンナトリウム 0.1
エタノール 45
PPG−20デシルテトラデセス−10 0.05
香料 0.1
水 残余
ココイルグルタミン酸カリウム 0.1 質量%
ラウリルベタイン 0.07
PEG−60水添ヒマシ油 1.0
グリセリン 10.0
ジプロピレングリコール 8.0
1,3−ブチレングリコール 4.0
ソルビトール 2.0
PEG400 2.0
メントール 0.2
フェノキシエタノール 0.5
タウリン 0.2
香料 0.1
水 残余
POE(20)ステアリン酸ソルビタン 2.0 質量%
ステアロイルメチルタウリンナトリウム 0.5
POE(5)ステアリン酸グリセリル 0.2
ベヘニルアルコール 1.8
ステアリルアルコール 1.8
ステアリン酸グリセリル 1.0
ミネラルオイル 12.0
エチルヘキサン酸セチル 5.0
N−ラウロイルグルタミン酸ジ(フィトステリル/オクチルドデシル)
2.0
ジプロピレングリコール 5.0
トレハロース 1.0
グリチルリチン酸ジカリウム 0.1
乳酸メンチル 0.2
アクリル酸/アクリル酸アルキル(C10−30)コポリマーカリウム
0.03
タウリン 0.1
キレート剤 適量
防腐剤 適量
香料 0.1
水 残余
POE(20)ステアリン酸ソルビタン 0.5 質量%
ステアロイルメチルタウリンナトリウム 0.05
ステアリルアルコール 0.5
セトステアリルアルコール 0.6
ジメチコン 5.0
ジイソステアリン酸グリセリル 1.0
エタノール 5.0
ブチレングリコール 10.0
グリセリン 1.0
トラネキサム酸 1.0
N−メチルタウリンナトリウム 0.3
キサンタンガム 0.05
ハッカ油 0.1
l−メンチルグリセリルエーテル 0.2
キレート剤 適量
防腐剤 適量
香料 0.15
水 残余
POE(20)パルミチン酸ソルビタン 0.8 質量%
ステアロイルメチルタウリンナトリウム 0.1
ベヘニルアルコール 0.4
バチルアルコール 0.2
シクロメチコン 9.0
フェニルトリメチコン 5.0
エタノール 2.0
ブチレングリコール 5.0
メントール 0.1
乳酸メンチル 0.1
タルク 2.0
二酸化チタン 1.0
クエン酸 0.05
N−メチルタウリンナトリウム 0.1
セルロースガム 0.09
キレート剤 適量
防腐剤 適量
水 残余
POE(20)ステアリン酸ソルビタン 1.0 質量%
ステアロイルメチルタウリンナトリウム 0.2
ベヘニルアルコール 1.0
セトステアリルアルコール 0.2
ステアリン酸グリセリル 0.5
シクロメチコン 10.0
メトキシケイヒ酸エチルヘキシル 7.0
t−ブチルメトキシベンゾイルメタン 1.0
イソステアリン酸 0.5
ジメチコンコポリオール 0.5
ブチレングリコール 7.0
ジプロピレングリコール 7.0
メントール 0.2
トラネキサム酸 2.0
N−メチルタウリンナトリウム 0.2
キレート剤 適量
防腐剤 適量
水 残余
グリセリン 5 質量%
ブチレングリコール 5
タウリン 0.2
ポリエチレングリコール1500 2
フェノキシエタノール 0.3
エデト酸3ナトリウム 0.02
クエン酸 0.03
N−メチルタウリンナトリウム 0.02
エタノール 5
POE・POP−デシルテトラデシルエーテル(24E.O.)(13P.O.)
0.4
PPG−20デシルテトラデセス−10 0.05
メントール 0.1
カンファー 0.1
水 残余
タルク 3 質量%
二酸化チタン 4
ベンガラ 0.5
黄酸化鉄 1.5
黒酸化鉄 0.1
ベントナイト 0.5
モノステアリン酸ポリオキシエチレンソルビタン 1
N−メチルタウリンナトリウム 0.8
ジプロピレングリコール 8
ジココイルエチルヒドロキシエチルモニウムメトサルフェート
0.6
イオン交換水 残余
ベヘニン酸 0.5
ステアリルアルコール 0.4
イソヘキサデシルアルコール 6
モノステアリン酸グリセリン 2
液状ラノリン 2
流動パラフィン 6
パラベン 0.1
3−L−メントキシプロパン−1,2−ジオール 0.3
香料 0.05
Claims (9)
- (a)成分および(b)成分を含むことを特徴とする化粧料および洗浄料。
(a)清涼化剤
(b)分子内にアミド結合および炭素数10以上のアルキル鎖を有さない1級アミンおよび/または2級アミン 0.1〜1.2質量% - 請求項1に記載の化粧料および洗浄料において、(b)1級アミンが下記式(I)で示されることを特徴とする化粧料および洗浄料。
(化1)
NH2−C(R1)2−CH2−R2 (I)
式(I)中、R1は水素原子またはメチル基、R2はOH、SO2H、SO2SH、SO3Hから選択される官能基である。 - 請求項1または2に記載の化粧料および洗浄料において、(b)2級アミンが下記式(II)で示されることを特徴とする化粧料および洗浄料。
(化2)
NHR3−CH2−CH2−R4 (II)
式(II)中、R3は炭素数1〜9のアルキル基、R2はOH、SO2H、SO2SH、SO3Hから選択されるいずれかである。 - 請求項1〜3のいずれかに記載の化粧料および洗浄料において、(a)成分の配合量が0.2〜1.2質量%であることを特徴とする化粧料および洗浄料。
- 請求項1〜4のいずれかに記載の化粧料および洗浄料において、pHが6.5以下であることを特徴とする化粧料および洗浄料。
- 請求項1〜5のいずれかに記載の化粧料および洗浄料において、(b)成分と(a)成分の配合比である(b)/(a)=0.01〜20であることを特徴とする化粧料および洗浄料。
- 請求項1〜6のいずれかに記載の化粧料および洗浄料において、(a)清涼化剤が、メントール、ハッカ油、l−メンチルグリセリルエーテル、乳酸メンチル、カンファー、イソプレゴール、ボルネオロール、シネオールメントン、スペアミント、ペパーミント、マロン酸メンチル、グリコシル−モノ−メンチル−O−アセテート、3−L−メントキシプロパン−1,2−ジオール、1−メンチル−3−ヒドロキシブチレートからなる群から選択される1種または2種以上のTRP M8活性化物質であることを特徴とする化粧料および洗浄料。
- 請求項1〜7のいずれかに記載の化粧料および洗浄料において、カチオン性多糖類 0.1〜1.0質量%を含むことを特徴とする化粧料および洗浄料。
- 請求項1〜8のいずれかに記載の化粧料および洗浄料において、アニオン性界面活性剤を含むことを特徴とする化粧料および洗浄料。
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CN201980056391.XA CN112638355A (zh) | 2018-08-29 | 2019-08-02 | 化妆品和清洁品 |
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