JP2018500308A5 - - Google Patents
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- Publication number
- JP2018500308A5 JP2018500308A5 JP2017531268A JP2017531268A JP2018500308A5 JP 2018500308 A5 JP2018500308 A5 JP 2018500308A5 JP 2017531268 A JP2017531268 A JP 2017531268A JP 2017531268 A JP2017531268 A JP 2017531268A JP 2018500308 A5 JP2018500308 A5 JP 2018500308A5
- Authority
- JP
- Japan
- Prior art keywords
- solvent
- water
- miscible organic
- organic solvent
- surface area
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 claims 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 9
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims 9
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 9
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims 9
- 239000003960 organic solvent Substances 0.000 claims 7
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 6
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims 6
- 239000003586 protic polar solvent Substances 0.000 claims 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 6
- 239000000010 aprotic solvent Substances 0.000 claims 5
- 229960002413 ferric citrate Drugs 0.000 claims 5
- NPFOYSMITVOQOS-UHFFFAOYSA-K iron(III) citrate Chemical compound [Fe+3].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NPFOYSMITVOQOS-UHFFFAOYSA-K 0.000 claims 5
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 claims 3
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims 3
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 claims 3
- 125000003158 alcohol group Chemical group 0.000 claims 3
- 150000001408 amides Chemical class 0.000 claims 3
- 150000001728 carbonyl compounds Chemical group 0.000 claims 3
- PJGSXYOJTGTZAV-UHFFFAOYSA-N pinacolone Chemical compound CC(=O)C(C)(C)C PJGSXYOJTGTZAV-UHFFFAOYSA-N 0.000 claims 3
- 239000002904 solvent Substances 0.000 claims 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical group [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims 2
- 229910000288 alkali metal carbonate Inorganic materials 0.000 claims 2
- 150000008041 alkali metal carbonates Chemical class 0.000 claims 2
- 239000007864 aqueous solution Substances 0.000 claims 2
- 229960004887 ferric hydroxide Drugs 0.000 claims 2
- IEECXTSVVFWGSE-UHFFFAOYSA-M iron(3+);oxygen(2-);hydroxide Chemical compound [OH-].[O-2].[Fe+3] IEECXTSVVFWGSE-UHFFFAOYSA-M 0.000 claims 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims 2
- YASYEJJMZJALEJ-UHFFFAOYSA-N Citric acid monohydrate Chemical compound O.OC(=O)CC(O)(C(O)=O)CC(O)=O YASYEJJMZJALEJ-UHFFFAOYSA-N 0.000 claims 1
- VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical compound [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 claims 1
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims 1
- 229910000019 calcium carbonate Inorganic materials 0.000 claims 1
- 229960002303 citric acid monohydrate Drugs 0.000 claims 1
- 238000000151 deposition Methods 0.000 claims 1
- 238000004090 dissolution Methods 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims 1
- 229910000027 potassium carbonate Inorganic materials 0.000 claims 1
- 229910000029 sodium carbonate Inorganic materials 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IN6352CH2014 | 2014-12-17 | ||
| IN6352/CHE/2014 | 2014-12-17 | ||
| PCT/IN2015/050208 WO2016098131A2 (en) | 2014-12-17 | 2015-12-17 | Improved method for the synthesis of ferric oraganic compounds |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2018500308A JP2018500308A (ja) | 2018-01-11 |
| JP2018500308A5 true JP2018500308A5 (enExample) | 2019-01-31 |
Family
ID=56127792
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017531268A Pending JP2018500308A (ja) | 2014-12-17 | 2015-12-17 | 有機鉄化合物を合成するための改良された方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US10882813B2 (enExample) |
| EP (1) | EP3233783A4 (enExample) |
| JP (1) | JP2018500308A (enExample) |
| KR (1) | KR20170094388A (enExample) |
| CN (1) | CN107108443A (enExample) |
| WO (1) | WO2016098131A2 (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108125193A (zh) * | 2017-12-29 | 2018-06-08 | 南通市飞宇精细化学品有限公司 | 一种食品添加剂柠檬酸铁的制备方法 |
| JP2019167305A (ja) * | 2018-03-23 | 2019-10-03 | 株式会社トクヤマ | クエン酸第二鉄の製造方法 |
| JP7335268B2 (ja) * | 2018-11-14 | 2023-08-29 | 株式会社トクヤマ | クエン酸第二鉄水和物の製造方法 |
| JP7335269B2 (ja) * | 2018-11-14 | 2023-08-29 | 株式会社トクヤマ | クエン酸第二鉄水和物の製造方法 |
| WO2020165781A1 (en) * | 2019-02-12 | 2020-08-20 | Biophore India Pharmaceuticals Pvt. Ltd | "improved process for the preparation of sucroferric oxyhydroxide" |
| JP7175235B2 (ja) * | 2019-04-19 | 2022-11-18 | 株式会社トクヤマ | クエン酸第二鉄水和物の製造方法 |
| CN110105194A (zh) * | 2019-05-10 | 2019-08-09 | 上海万巷制药有限公司 | 一种药用级柠檬酸铁的制备方法 |
| US11560339B2 (en) | 2019-05-30 | 2023-01-24 | Koch Agronomie Services, LLC | Micronutrient foliar solutions |
| WO2021089766A1 (en) | 2019-11-08 | 2021-05-14 | Química Sintética, S.A. | Process for the preparation of ferric organic compounds |
| CN115247232B (zh) * | 2022-03-02 | 2024-04-09 | 广州大鱼创福科技有限公司 | 一种铁矾渣钙化产物沉降分离方法 |
| WO2023047424A1 (en) * | 2022-04-29 | 2023-03-30 | West Bengal Chemical Industries Limited | Pharmaceutical acceptable iron (iii) coordination complex having high phosphate binding capacity and preparation thereof |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AT279048B (de) * | 1967-07-04 | 1970-02-25 | Pharmazeutische Fabrik Montavit Gmbh | Verfahren zur Herstellung neuer, löslicher und stabiler organischer Eisen(III)-Komplexverbindungen und Injektionslösungen davon |
| PL69800B1 (enExample) | 1970-06-01 | 1973-10-31 | ||
| JPS606619A (ja) * | 1983-06-27 | 1985-01-14 | Kyowa Chem Ind Co Ltd | 鉄分欠乏症処置剤及びその製法 |
| IT1222654B (it) * | 1987-09-14 | 1990-09-12 | Schering Ag | Complesso micellare di ferro-citrato |
| CN1202067C (zh) * | 2002-09-09 | 2005-05-18 | 苏荣仁 | 药用级枸橼酸铁的制备方法 |
| US8093423B2 (en) * | 2003-02-19 | 2012-01-10 | Globoasia, Llc | Pharmaceutical-grade ferric organic compounds, uses thereof and method of making same |
| TWI335218B (en) * | 2003-02-19 | 2011-01-01 | Panion & Bf Biotech Inc | Ferric organic compounds, uses thereof and methods of making same |
| US6903235B2 (en) | 2003-10-08 | 2005-06-07 | Panion & Bf Biotech Inc. | Pharmaceutical-grade ferric citrate |
| US7179939B2 (en) * | 2004-03-16 | 2007-02-20 | Navinta Llc | Sodium ferric gluconate complexes and method of manufacture thereof |
| JP5667343B2 (ja) * | 2005-08-18 | 2015-02-12 | パニオン アンド ビーエフ バイオテック インコーポレーテッド | 医薬グレードの第二鉄有機化合物、その使用およびその製造方法 |
-
2015
- 2015-12-17 KR KR1020177019244A patent/KR20170094388A/ko not_active Withdrawn
- 2015-12-17 JP JP2017531268A patent/JP2018500308A/ja active Pending
- 2015-12-17 US US15/536,807 patent/US10882813B2/en active Active
- 2015-12-17 WO PCT/IN2015/050208 patent/WO2016098131A2/en not_active Ceased
- 2015-12-17 EP EP15869481.0A patent/EP3233783A4/en not_active Withdrawn
- 2015-12-17 CN CN201580069351.0A patent/CN107108443A/zh active Pending
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