JP2017522341A5 - - Google Patents
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- Publication number
- JP2017522341A5 JP2017522341A5 JP2017504822A JP2017504822A JP2017522341A5 JP 2017522341 A5 JP2017522341 A5 JP 2017522341A5 JP 2017504822 A JP2017504822 A JP 2017504822A JP 2017504822 A JP2017504822 A JP 2017504822A JP 2017522341 A5 JP2017522341 A5 JP 2017522341A5
- Authority
- JP
- Japan
- Prior art keywords
- stream
- alcohol
- process according
- acid
- heavy
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 8
- YIWUKEYIRIRTPP-UHFFFAOYSA-N 2-ethylhexan-1-ol Chemical compound CCCCC(CC)CO YIWUKEYIRIRTPP-UHFFFAOYSA-N 0.000 claims 6
- 239000002253 acid Substances 0.000 claims 6
- SJWFXCIHNDVPSH-UHFFFAOYSA-N octan-2-ol Chemical compound CCCCCCC(C)O SJWFXCIHNDVPSH-UHFFFAOYSA-N 0.000 claims 6
- 239000006227 byproduct Substances 0.000 claims 5
- 239000011541 reaction mixture Substances 0.000 claims 5
- 239000012535 impurity Substances 0.000 claims 4
- 238000000746 purification Methods 0.000 claims 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 4
- 150000002148 esters Chemical class 0.000 claims 3
- 239000011347 resin Substances 0.000 claims 3
- 229920005989 resin Polymers 0.000 claims 3
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims 2
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims 2
- 239000003054 catalyst Substances 0.000 claims 2
- 238000004821 distillation Methods 0.000 claims 2
- 230000032050 esterification Effects 0.000 claims 2
- 238000005886 esterification reaction Methods 0.000 claims 2
- 239000012074 organic phase Substances 0.000 claims 2
- 239000000376 reactant Substances 0.000 claims 2
- 238000005406 washing Methods 0.000 claims 2
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 claims 1
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims 1
- 150000007513 acids Chemical class 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 239000008346 aqueous phase Substances 0.000 claims 1
- 125000002091 cationic group Chemical group 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- MWKFXSUHUHTGQN-UHFFFAOYSA-N decan-1-ol Chemical compound CCCCCCCCCCO MWKFXSUHUHTGQN-UHFFFAOYSA-N 0.000 claims 1
- 238000010908 decantation Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- YLQLIQIAXYRMDL-UHFFFAOYSA-N propylheptyl alcohol Chemical compound CCCCCC(CO)CCC YLQLIQIAXYRMDL-UHFFFAOYSA-N 0.000 claims 1
- 239000010409 thin film Substances 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1457262 | 2014-07-28 | ||
| FR1457262A FR3024143B1 (fr) | 2014-07-28 | 2014-07-28 | Procede perfectionne de fabrication de (meth)acrylates d'alkyle |
| PCT/FR2015/051648 WO2016016528A1 (fr) | 2014-07-28 | 2015-06-22 | Procédé perfectionne de fabrication de (méth)acrylates d'alkyle |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2017522341A JP2017522341A (ja) | 2017-08-10 |
| JP2017522341A5 true JP2017522341A5 (enExample) | 2018-06-21 |
| JP6618524B2 JP6618524B2 (ja) | 2019-12-11 |
Family
ID=51726738
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017504822A Active JP6618524B2 (ja) | 2014-07-28 | 2015-06-22 | アルキル（メタ）アクリレートを製造するための改良された方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US9975842B2 (enExample) |
| EP (1) | EP3174844B1 (enExample) |
| JP (1) | JP6618524B2 (enExample) |
| KR (1) | KR102331106B1 (enExample) |
| CN (1) | CN106536473B (enExample) |
| BR (1) | BR112017001772B1 (enExample) |
| FR (1) | FR3024143B1 (enExample) |
| MX (1) | MX2016017052A (enExample) |
| SG (1) | SG11201700702SA (enExample) |
| WO (1) | WO2016016528A1 (enExample) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3060001B1 (fr) * | 2016-12-08 | 2020-05-01 | Arkema France | Procede de fabrication d'esters (meth)acryliques |
| FR3096368B1 (fr) | 2019-05-23 | 2021-04-23 | Arkema France | Procede perfectionne de fabrication d’acrylates d’alkyle de purete elevee |
| EP3798202A1 (de) * | 2019-09-25 | 2021-03-31 | Röhm GmbH | Verfahren zur aufreinigung von methylmethacrylat von leichtsiedenden komponenten |
| US10807063B1 (en) | 2019-12-31 | 2020-10-20 | Industrial Technology Research Institute | Device and method for continuously manufacturing acrylate compound |
| FR3119845B1 (fr) | 2021-02-15 | 2023-01-06 | Arkema France | Procede perfectionne de fabrication d’acrylates d’alkyle de purete elevee |
| CN117185921A (zh) * | 2022-06-01 | 2023-12-08 | 中国石油化工股份有限公司 | （甲基）丙烯酸酯的制备方法 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4748268A (en) * | 1986-07-31 | 1988-05-31 | Amoco Corporation | Continuous process for production of methacrylic acid ester of C1 to C4 aliphatic alcohol |
| JPH0764787B2 (ja) * | 1987-04-16 | 1995-07-12 | 株式会社日本触媒 | 高純度メタクリル酸エステルの製造方法 |
| JPS649956A (en) * | 1987-07-01 | 1989-01-13 | Nippon Catalytic Chem Ind | Production of unsaturated carboxylic acid ester |
| JP2679954B2 (ja) * | 1994-11-25 | 1997-11-19 | ラッキー リミテッド | 不飽和カルボン酸エステル類の製造方法及び製造装置 |
| DE19536178A1 (de) * | 1995-09-28 | 1997-04-03 | Basf Ag | Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Alkylestern der (Meth)acrylsäure |
| FR2739850B1 (fr) * | 1995-10-17 | 1997-12-05 | Atochem Elf Sa | Procede de fabrication d'esters acryliques et methacryliques d'alcools polyalkoxyles a chaine hydrophobe |
| JP3942713B2 (ja) * | 1996-12-16 | 2007-07-11 | 株式会社日本触媒 | カルボン酸エステル類の製造方法および樹脂分離槽 |
| FR2818639B1 (fr) * | 2000-12-26 | 2003-02-07 | Atofina | Procede perfectionne de fabrication d'esters carboxyliques insatures |
| FR2822825B1 (fr) * | 2001-04-02 | 2003-05-16 | Atofina | Procede de fabrication d'acrylate de 2-ethylhexyle comportant le lavage a l'eau du brut |
| DE10144490A1 (de) * | 2001-09-10 | 2003-03-27 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
| AU2002355041A1 (en) * | 2001-11-28 | 2003-06-10 | Mitsubishi Chemical Corporation | Process for producing (meth)acrylic acid compound |
| JP4160087B2 (ja) * | 2006-07-11 | 2008-10-01 | 株式会社日本触媒 | アクリル酸エステルの製造方法 |
| US7943094B2 (en) * | 2006-12-07 | 2011-05-17 | Grupo Petrotemex, S.A. De C.V. | Polyester production system employing horizontally elongated esterification vessel |
| JP5191170B2 (ja) * | 2007-06-19 | 2013-04-24 | 株式会社日本触媒 | （メタ）アクリル酸エステルの製造方法 |
| FR2982258B1 (fr) * | 2011-11-04 | 2013-11-15 | Arkema France | Procede de production d'acrylate de 2-octyle par esterification directe |
-
2014
- 2014-07-28 FR FR1457262A patent/FR3024143B1/fr not_active Expired - Fee Related
-
2015
- 2015-06-22 CN CN201580040689.3A patent/CN106536473B/zh active Active
- 2015-06-22 JP JP2017504822A patent/JP6618524B2/ja active Active
- 2015-06-22 KR KR1020177004631A patent/KR102331106B1/ko active Active
- 2015-06-22 WO PCT/FR2015/051648 patent/WO2016016528A1/fr not_active Ceased
- 2015-06-22 EP EP15735994.4A patent/EP3174844B1/fr active Active
- 2015-06-22 US US15/329,910 patent/US9975842B2/en active Active
- 2015-06-22 BR BR112017001772-5A patent/BR112017001772B1/pt active IP Right Grant
- 2015-06-22 MX MX2016017052A patent/MX2016017052A/es unknown
- 2015-06-22 SG SG11201700702SA patent/SG11201700702SA/en unknown
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