JP2017520560A5 - - Google Patents
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- Publication number
- JP2017520560A5 JP2017520560A5 JP2016575025A JP2016575025A JP2017520560A5 JP 2017520560 A5 JP2017520560 A5 JP 2017520560A5 JP 2016575025 A JP2016575025 A JP 2016575025A JP 2016575025 A JP2016575025 A JP 2016575025A JP 2017520560 A5 JP2017520560 A5 JP 2017520560A5
- Authority
- JP
- Japan
- Prior art keywords
- reactor
- aniline
- mass flow
- flow rate
- time
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims 27
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 claims 22
- 238000000034 method Methods 0.000 claims 9
- 239000002253 acid Substances 0.000 claims 8
- 229920000768 polyamine Polymers 0.000 claims 5
- 150000007854 aminals Chemical class 0.000 claims 4
- ZZTCPWRAHWXWCH-UHFFFAOYSA-N diphenylmethanediamine Chemical compound C=1C=CC=CC=1C(N)(N)C1=CC=CC=C1 ZZTCPWRAHWXWCH-UHFFFAOYSA-N 0.000 claims 3
- 238000004519 manufacturing process Methods 0.000 claims 3
- 239000011541 reaction mixture Substances 0.000 claims 3
- 150000004985 diamines Chemical class 0.000 claims 2
- 239000012074 organic phase Substances 0.000 claims 2
- 239000003377 acid catalyst Substances 0.000 claims 1
- 239000008346 aqueous phase Substances 0.000 claims 1
- 238000010924 continuous production Methods 0.000 claims 1
- CZZYITDELCSZES-UHFFFAOYSA-N diphenylmethane Chemical compound C=1C=CC=CC=1CC1=CC=CC=C1 CZZYITDELCSZES-UHFFFAOYSA-N 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- PAYRUJLWNCNPSJ-UHFFFAOYSA-O phenylazanium Chemical class [NH3+]C1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-O 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP14173581 | 2014-06-24 | ||
| EP14173581.1 | 2014-06-24 | ||
| PCT/EP2015/063922 WO2015197519A1 (de) | 2014-06-24 | 2015-06-22 | Verfahren zur herstellung von di- und polyaminen derdiphenylmethanreihe |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2017520560A JP2017520560A (ja) | 2017-07-27 |
| JP2017520560A5 true JP2017520560A5 (OSRAM) | 2018-08-02 |
| JP6655559B2 JP6655559B2 (ja) | 2020-02-26 |
Family
ID=50980957
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016575025A Expired - Fee Related JP6655559B2 (ja) | 2014-06-24 | 2015-06-22 | ジフェニルメタン系ジアミンおよびポリアミンの製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US10125090B2 (OSRAM) |
| EP (1) | EP3160935B1 (OSRAM) |
| JP (1) | JP6655559B2 (OSRAM) |
| KR (1) | KR20170026487A (OSRAM) |
| CN (1) | CN106458844B (OSRAM) |
| HU (1) | HUE057242T2 (OSRAM) |
| PT (1) | PT3160935T (OSRAM) |
| SA (1) | SA516380562B1 (OSRAM) |
| WO (1) | WO2015197519A1 (OSRAM) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106458845B (zh) * | 2014-06-24 | 2019-10-22 | 科思创德国股份有限公司 | 用于制备二苯基甲烷系列的二胺和多胺的方法 |
| CN110088078B (zh) * | 2016-12-22 | 2022-09-09 | 科思创德国股份有限公司 | 生产二苯基甲烷系列的二胺和多胺的方法 |
| CN110291063B (zh) * | 2016-12-22 | 2022-07-05 | 科思创德国股份有限公司 | 在不同的生产能力下制备二苯基甲烷系列的二胺和多胺的方法 |
| US10626078B2 (en) | 2016-12-22 | 2020-04-21 | Covestro Deutschland Ag | Method of producing diamines and polyamines of the diphenylmethane series at different production capacities |
| US10640453B2 (en) | 2016-12-22 | 2020-05-05 | Covestro Deutschland Ag | Method of producing diamines and polyamines of the diphenylmethane series |
| CN110997637B (zh) | 2017-09-05 | 2022-09-27 | 保仕健生物科技(上海)有限公司 | 芳香类衍生物、其制备方法及其在医药上的应用 |
| WO2020177067A1 (en) | 2019-03-05 | 2020-09-10 | Bioardis Llc | Aromatic derivatives, preparation methods, and medical uses thereof |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE844896C (de) | 1944-04-04 | 1952-09-15 | Bayer Ag | Verfahren zur Herstellung von organischen Isocyanaten |
| GB1517585A (en) | 1974-11-13 | 1978-07-12 | Mobay Chemical Corp | Process for the production of a polyamino-polyphenyl-(poly)-methylene polyamine |
| US4792624A (en) | 1987-02-26 | 1988-12-20 | The Dow Chemical Company | Process for polymeric MDA, recycle of finished polymeric MDA |
| JP2825604B2 (ja) | 1990-04-11 | 1998-11-18 | 三井化学株式会社 | メチレン架橋されたポリアリールアミンの製造方法 |
| US5286760A (en) | 1992-10-09 | 1994-02-15 | Miles, Inc. | Process for reducing impurity levels in methylene diphenyamines |
| DE19804915A1 (de) | 1998-02-07 | 1999-08-12 | Basf Ag | Verfahren zur Herstellung von Methylendi(phenylamin) und Methylendi(phenylisocyanat) |
| DE19817691A1 (de) | 1998-04-21 | 1999-10-28 | Basf Ag | Verfahren zur Herstellung von Mischungen aus Diphenylmehandiisocyanaten und Polyphenylen-polymethylen-polyisocyanaten mit vermindertem Gehalt an chlorierten Nebenprodukten und verminderter Jodfarbzahl |
| DE10006452A1 (de) * | 2000-02-14 | 2001-08-16 | Bayer Ag | Verfahren zur Herstellung von Diaminodiphenylmethanen |
| DE102004032416A1 (de) * | 2004-07-05 | 2006-02-02 | Bayer Materialscience Ag | Verfahren zur Herstellung von Polyaminen der Diphenylmethanreihe bei niedriger Protonierung |
| DE102004052370A1 (de) | 2004-10-28 | 2006-05-04 | Bayer Materialscience Ag | Verfahren zur Herstellung von Di- und Polyaminen der Diphenylmethanreihe |
| DE102006004047A1 (de) | 2006-01-28 | 2007-08-02 | Bayer Materialscience Ag | Verfahren zur Herstellung von Di- und Polyaminen der Diphenylmethanreihe |
| DE102006004041A1 (de) | 2006-01-28 | 2007-08-02 | Bayer Materialscience Ag | Verfahren zur Herstellung von Di- und Polyaminen der Diphenylmethanreihe |
| EP2039676A1 (en) * | 2007-09-19 | 2009-03-25 | Huntsman International Llc | Process for the production of di-and polyamines of the diphenylmethane series |
| DE102008015123A1 (de) * | 2008-03-20 | 2009-09-24 | Bayer Materialscience Ag | Verfahren zur Herstellung von Di- und Polyaminen der Diphenylmethanreihe |
| JP5850345B2 (ja) * | 2010-12-29 | 2016-02-03 | ワンホア ケミカル グループ カンパニー リミテッド | 高速混合反応器およびその使用 |
| CN106458845B (zh) * | 2014-06-24 | 2019-10-22 | 科思创德国股份有限公司 | 用于制备二苯基甲烷系列的二胺和多胺的方法 |
-
2015
- 2015-06-22 CN CN201580034184.6A patent/CN106458844B/zh active Active
- 2015-06-22 US US15/317,301 patent/US10125090B2/en active Active
- 2015-06-22 JP JP2016575025A patent/JP6655559B2/ja not_active Expired - Fee Related
- 2015-06-22 PT PT157301789T patent/PT3160935T/pt unknown
- 2015-06-22 KR KR1020177001662A patent/KR20170026487A/ko not_active Withdrawn
- 2015-06-22 HU HUE15730178A patent/HUE057242T2/hu unknown
- 2015-06-22 WO PCT/EP2015/063922 patent/WO2015197519A1/de not_active Ceased
- 2015-06-22 EP EP15730178.9A patent/EP3160935B1/de active Active
-
2016
- 2016-12-21 SA SA516380562A patent/SA516380562B1/ar unknown
-
2018
- 2018-09-24 US US16/139,580 patent/US10689323B2/en not_active Expired - Fee Related
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