JP2017507876A5 - - Google Patents
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- Publication number
- JP2017507876A5 JP2017507876A5 JP2016541150A JP2016541150A JP2017507876A5 JP 2017507876 A5 JP2017507876 A5 JP 2017507876A5 JP 2016541150 A JP2016541150 A JP 2016541150A JP 2016541150 A JP2016541150 A JP 2016541150A JP 2017507876 A5 JP2017507876 A5 JP 2017507876A5
- Authority
- JP
- Japan
- Prior art keywords
- colloidal silica
- acid
- activator
- activated
- value
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000000034 method Methods 0.000 claims 19
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical class O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 17
- 239000008119 colloidal silica Substances 0.000 claims 9
- 239000012190 activator Substances 0.000 claims 7
- 239000000203 mixture Substances 0.000 claims 5
- 239000002994 raw material Substances 0.000 claims 4
- 235000002639 sodium chloride Nutrition 0.000 claims 4
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid group Chemical group S(O)(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 3
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims 3
- 239000000463 material Substances 0.000 claims 3
- 150000003839 salts Chemical class 0.000 claims 3
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 claims 2
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 claims 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims 2
- 230000004913 activation Effects 0.000 claims 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims 2
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims 2
- LWIHDJKSTIGBAC-UHFFFAOYSA-K potassium phosphate Substances [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 claims 2
- 239000011541 reaction mixture Substances 0.000 claims 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 claims 2
- 239000001488 sodium phosphate Substances 0.000 claims 2
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 claims 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims 2
- BZSXEZOLBIJVQK-UHFFFAOYSA-N 2-methylsulfonylbenzoic acid Chemical compound CS(=O)(=O)C1=CC=CC=C1C(O)=O BZSXEZOLBIJVQK-UHFFFAOYSA-N 0.000 claims 1
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims 1
- 239000005711 Benzoic acid Substances 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims 1
- 229910004298 SiO 2 Inorganic materials 0.000 claims 1
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims 1
- 235000011054 acetic acid Nutrition 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 claims 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 1
- 229960001716 benzalkonium Drugs 0.000 claims 1
- SRSXLGNVWSONIS-UHFFFAOYSA-N benzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-N 0.000 claims 1
- 229940092714 benzenesulfonic acid Drugs 0.000 claims 1
- CYDRXTMLKJDRQH-UHFFFAOYSA-N benzododecinium Chemical compound CCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 CYDRXTMLKJDRQH-UHFFFAOYSA-N 0.000 claims 1
- 235000010233 benzoic acid Nutrition 0.000 claims 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 claims 1
- ZPWVASYFFYYZEW-UHFFFAOYSA-L dipotassium hydrogen phosphate Chemical compound [K+].[K+].OP([O-])([O-])=O ZPWVASYFFYYZEW-UHFFFAOYSA-L 0.000 claims 1
- 229910000396 dipotassium phosphate Inorganic materials 0.000 claims 1
- 235000019797 dipotassium phosphate Nutrition 0.000 claims 1
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims 1
- 229910000397 disodium phosphate Inorganic materials 0.000 claims 1
- 235000019800 disodium phosphate Nutrition 0.000 claims 1
- 239000000835 fiber Substances 0.000 claims 1
- 235000019253 formic acid Nutrition 0.000 claims 1
- 239000001530 fumaric acid Substances 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims 1
- 239000011976 maleic acid Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 150000007522 mineralic acids Chemical group 0.000 claims 1
- 229910000402 monopotassium phosphate Inorganic materials 0.000 claims 1
- 235000019796 monopotassium phosphate Nutrition 0.000 claims 1
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims 1
- 235000019799 monosodium phosphate Nutrition 0.000 claims 1
- 229910017604 nitric acid Inorganic materials 0.000 claims 1
- 150000007524 organic acids Chemical class 0.000 claims 1
- 235000005985 organic acids Nutrition 0.000 claims 1
- 235000006408 oxalic acid Nutrition 0.000 claims 1
- 239000011736 potassium bicarbonate Substances 0.000 claims 1
- 235000015497 potassium bicarbonate Nutrition 0.000 claims 1
- 229910000028 potassium bicarbonate Inorganic materials 0.000 claims 1
- VKJKEPKFPUWCAS-UHFFFAOYSA-M potassium chlorate Chemical compound [K+].[O-]Cl(=O)=O VKJKEPKFPUWCAS-UHFFFAOYSA-M 0.000 claims 1
- 239000001103 potassium chloride Substances 0.000 claims 1
- 235000011164 potassium chloride Nutrition 0.000 claims 1
- GNSKLFRGEWLPPA-UHFFFAOYSA-M potassium dihydrogen phosphate Chemical compound [K+].OP(O)([O-])=O GNSKLFRGEWLPPA-UHFFFAOYSA-M 0.000 claims 1
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 claims 1
- 239000004323 potassium nitrate Substances 0.000 claims 1
- 235000010333 potassium nitrate Nutrition 0.000 claims 1
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims 1
- 229910052939 potassium sulfate Inorganic materials 0.000 claims 1
- 235000011151 potassium sulphates Nutrition 0.000 claims 1
- 235000019260 propionic acid Nutrition 0.000 claims 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 235000015424 sodium Nutrition 0.000 claims 1
- 239000011780 sodium chloride Substances 0.000 claims 1
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims 1
- 239000004317 sodium nitrate Substances 0.000 claims 1
- 235000010344 sodium nitrate Nutrition 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310697915.8 | 2013-12-18 | ||
| CN201310697915 | 2013-12-18 | ||
| CN201410748835.5A CN104947499B (zh) | 2013-12-18 | 2014-12-10 | 硅溶胶、制备其的设备和方法和其在造纸中的应用 |
| CN201410748835.5 | 2014-12-10 | ||
| PCT/US2014/070927 WO2015095377A1 (en) | 2013-12-18 | 2014-12-17 | Silica sols, method and apparatus for producing the same and use thereof in papermaking |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2017507876A JP2017507876A (ja) | 2017-03-23 |
| JP2017507876A5 true JP2017507876A5 (OSRAM) | 2018-02-22 |
| JP6595482B2 JP6595482B2 (ja) | 2019-10-23 |
Family
ID=53403647
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016541150A Active JP6595482B2 (ja) | 2013-12-18 | 2014-12-17 | シリカゾル、その製造のための方法および装置ならびに製紙でのそれらの使用 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US9975781B2 (OSRAM) |
| EP (1) | EP3083499B1 (OSRAM) |
| JP (1) | JP6595482B2 (OSRAM) |
| KR (1) | KR102379044B1 (OSRAM) |
| CN (2) | CN104947499B (OSRAM) |
| BR (1) | BR112016014038B1 (OSRAM) |
| CA (1) | CA2934323C (OSRAM) |
| WO (1) | WO2015095377A1 (OSRAM) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017054198A1 (en) | 2015-09-30 | 2017-04-06 | Ecolab Usa Inc. | Compositions and methods for treating filler in papermaking |
| US20210130176A1 (en) * | 2017-10-11 | 2021-05-06 | Applied Material Solutions, Inc. | Multimodal Particles for Retention and Drainage for Paper-Making Machines |
| CN108083283B (zh) * | 2017-12-07 | 2021-08-20 | 临汾博利士纳米材料有限公司 | 铝改性酸性硅溶胶及其制备方法 |
| CN108277639B (zh) * | 2018-02-11 | 2020-08-25 | 宜州市壮之都丝绸家纺有限公司 | 一种四元硅溶胶掺杂真丝丝绸的工艺 |
| CN108277640B (zh) * | 2018-02-11 | 2020-08-21 | 宜州市壮之都丝绸家纺有限公司 | 一种三元硅溶胶掺杂真丝丝绸的工艺 |
| US10876258B2 (en) * | 2018-11-27 | 2020-12-29 | Solenis Technologies, L.P. | Method for improving filler and fiber retention in paper making processes |
| EP3980500A1 (en) * | 2019-06-07 | 2022-04-13 | Ecolab Usa Inc. | Hydrophilic cationic dispersion polymers for improved print quality and water fastness |
| CN111302347B (zh) * | 2020-04-02 | 2020-10-16 | 临沂市科翰硅制品有限公司 | 一种高纯大粒径硅溶胶的制备方法 |
| CN119173476A (zh) * | 2022-05-13 | 2024-12-20 | 多摩化学工业株式会社 | 胶体二氧化硅及其制造方法 |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2244355A (en) | 1940-04-12 | 1941-06-03 | Lester C Britner | Clothes display hanger |
| US2769785A (en) * | 1950-09-02 | 1956-11-06 | B I F Ind Inc | Continuous silica sol apparatus |
| US3582502A (en) | 1968-12-06 | 1971-06-01 | Nalco Chemical Co | Method of reinforcing latex foam |
| AU546999B2 (en) | 1980-05-28 | 1985-10-03 | Eka A.B. | Adding binder to paper making stock |
| US4385961A (en) | 1981-02-26 | 1983-05-31 | Eka Aktiebolag | Papermaking |
| SE8403062L (sv) | 1984-06-07 | 1985-12-08 | Eka Ab | Forfarande vid papperstillverkning |
| SE451739B (sv) | 1985-04-03 | 1987-10-26 | Eka Nobel Ab | Papperstillverkningsforfarande och pappersprodukt varvid som avvattnings- och retentionsforbettrande kemikalie anvends katjonisk polyakrylamid och en speciell oorganisk kolloid |
| GB8602121D0 (en) | 1986-01-29 | 1986-03-05 | Allied Colloids Ltd | Paper & paper board |
| US4795531A (en) | 1987-09-22 | 1989-01-03 | Nalco Chemical Company | Method for dewatering paper |
| EP0359552B1 (en) * | 1988-09-16 | 1993-05-19 | E.I. Du Pont De Nemours And Company | Polysilicate microgels as retention/drainage aids in papermaking |
| SE500387C2 (sv) | 1989-11-09 | 1994-06-13 | Eka Nobel Ab | Silikasoler, förfarande för framställning av silikasoler samt användning av solerna i pappersframställning |
| US5503820A (en) | 1992-05-26 | 1996-04-02 | E. I. Du Pont De Nemours And Company | Method for preparing low-concentration polysilicate microgels |
| US5279807A (en) * | 1992-05-26 | 1994-01-18 | E. I. Du Pont De Nemours And Company | Method for preparing low-concentration polysilicate microgels |
| CN1066617C (zh) * | 1992-07-10 | 2001-06-06 | 诺瓦特克有限公司 | 含有胶态二氧化硅的增香组合物及其制造和使用方法 |
| AU4672293A (en) * | 1992-07-10 | 1994-01-31 | Novatech, Inc. | Flavor enhancing composition containing colloidal silica and method for its preparation and use |
| SE501214C2 (sv) * | 1992-08-31 | 1994-12-12 | Eka Nobel Ab | Silikasol samt förfarande för framställning av papper under användande av solen |
| FR2732368B1 (fr) | 1995-03-31 | 1997-06-06 | Roquette Freres | Nouveau procede de fabrication de papier |
| US5573674A (en) * | 1995-10-27 | 1996-11-12 | General Chemical Corporation | Activated silica sol |
| FR2740482B1 (fr) | 1995-10-30 | 1997-11-21 | Snf Sa | Procede pour ameliorer la retention dans un procede de fabrication du papier, carton et analogue |
| KR100573343B1 (ko) | 1997-06-13 | 2006-04-24 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 저-농도 폴리알루미노실리케이트 마이크로겔의 개선된제조 방법 |
| CO5070714A1 (es) * | 1998-03-06 | 2001-08-28 | Nalco Chemical Co | Proceso para la preparacion de silice coloidal estable |
| CA2375399C (en) * | 1999-06-02 | 2007-04-24 | Nalco Chemical Company | Stable silica sols of high surface area and improved activity |
| JP3496072B2 (ja) | 1999-06-29 | 2004-02-09 | 沖電気工業株式会社 | 送受信回路 |
| ES2641564T3 (es) * | 2003-11-21 | 2017-11-10 | Akzo Nobel N.V. | Composición |
| US8491753B2 (en) * | 2004-10-15 | 2013-07-23 | Nalco Company | Composition and method for improving retention and drainage in papermaking processes by activating microparticles with a promoter-flocculant system |
| AR072689A1 (es) * | 2008-07-14 | 2010-09-15 | Akzo Nobel Nv | Soles basados en silice metodo para producirlos uso y metodo para producir papel que los utiliza |
| EP2338949B1 (en) * | 2009-12-17 | 2012-08-15 | Services Pétroliers Schlumberger | Pumpable geopolymers comprising a mixing aid and dispersing agent |
| PL2522626T3 (pl) * | 2011-05-12 | 2017-04-28 | Kemira Oyj | Sposób wytwarzania zolu na bazie krzemionki, zol na bazie krzemionki i jego zastosowanie |
| JP2012077307A (ja) * | 2011-11-18 | 2012-04-19 | Nippon Chem Ind Co Ltd | 地盤注入用グラウト材及び地盤注入工法 |
-
2014
- 2014-12-10 CN CN201410748835.5A patent/CN104947499B/zh active Active
- 2014-12-10 CN CN201711414284.9A patent/CN108130801B/zh active Active
- 2014-12-17 BR BR112016014038-9A patent/BR112016014038B1/pt active IP Right Grant
- 2014-12-17 JP JP2016541150A patent/JP6595482B2/ja active Active
- 2014-12-17 US US15/105,801 patent/US9975781B2/en active Active
- 2014-12-17 WO PCT/US2014/070927 patent/WO2015095377A1/en not_active Ceased
- 2014-12-17 KR KR1020167019330A patent/KR102379044B1/ko active Active
- 2014-12-17 CA CA2934323A patent/CA2934323C/en active Active
- 2014-12-17 EP EP14871356.3A patent/EP3083499B1/en active Active
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