JP2017125295A - 構造体 - Google Patents
構造体 Download PDFInfo
- Publication number
- JP2017125295A JP2017125295A JP2017057973A JP2017057973A JP2017125295A JP 2017125295 A JP2017125295 A JP 2017125295A JP 2017057973 A JP2017057973 A JP 2017057973A JP 2017057973 A JP2017057973 A JP 2017057973A JP 2017125295 A JP2017125295 A JP 2017125295A
- Authority
- JP
- Japan
- Prior art keywords
- core material
- fiber
- porous layer
- fibers
- laminate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
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Abstract
Description
(1)式において、V1は多孔質層の空孔を含む体積で、多孔質層の縦長さL1、多孔質層の横長さL2、及び多孔質層の厚みL3から下記(2)式により算出される。多孔質層の空孔を含む体積V1は、多孔質層に液体等の材料が充填されていない状態で行われる。多孔質層に液体等の材料が充填されている場合、多孔質層の洗浄等によって材料を除去した後に測定を行う。また、各寸法L1、L2及びL3は、基材又は芯材上に作製した多孔質層を基材及び芯材から剥離した後、多孔質層を平面上に置いた状態でスケールにより計測する。
また、V2は多孔質層の正味の体積で、多孔質層の重量を多孔質層の密度で割ったものである。
(3)式において、V3は積層体の空孔を含む体積で、積層体の縦長さL4、積層体の横長さL5、及び積層体の厚みL6から下記(4)式により算出される。積層体の空孔を含む体積V3は、積層体に液体等の材料が充填されていない状態で行われる。積層体に液体等の材料が充填されている場合、積層体の洗浄等によって材料を除去した後に測定を行う。また、各寸法L4、L5及びL6は、積層体を平面上に置いた状態でスケールにより計測する。
V3=L4×L5×L6 (4)
また、V4は積層体の正味の体積で、積層体の重量を積層体の密度で割ったものである。
(実施例1)
溶剤であるN.N−ジメチルホルムアミド(DMF)で50重量%希釈したエポキシ樹脂主剤に、LiBrを1重量%添加して溶解させて溶液を調製した。この溶液にエポキシ樹脂主剤に対して40重量%量の硬化剤を加えて70℃に加熱して仮硬化させ、原料溶液を得た。
(実施例2)
実施例1と同様な方法で作製した多孔質層と芯材を用意した。図3に示すように、芯材1の両方の最外層に多孔質層を積層し、積層体を得た。多孔質層の積層数は、芯材の片側当たり10層とした。積層体の空孔率は80%であった。
得られた積層体を、実施例1と同様な5層構造のラミネートフィルム製の袋状外装部材に収納した後、真空ポンプを用いて外装部材内を真空状態にし、外装部材をヒートシールにより封止して構造体を得た。
(実施例3)
芯材として、図4に示す構造を有し、縦長さ150mm、横長さ150mm、厚み5mm、空孔率が80%のアクリル樹脂製の多孔質板を用意した。
(実施例4)
実施例3と同様な方法で作製した多孔質層と芯材を用意した。図3に示すように、芯材1の両方の最外層に多孔質層を積層し、積層体を得た。多孔質層の積層数は、芯材の片側当たり10層とした。積層体の空孔率は92%であった。
(実施例5)
電解質としてLiBrの代わりに0.1重量%のLiClを用いること以外は、実施例1と同様にして多孔質層を形成した。
(実施例6)
電解質としてLiBrの代わりに0.1重量%のベンジルトリエチルアンモニウムクロライドを用いること以外は、実施例1と同様にして多孔質層を形成した。
(実施例7)
エレクトロスピニング工程において、溶剤であるN.N−ジメチルホルムアミド(DMF)で45重量%希釈したエポキシ樹脂主剤を用いることによりエポキシ樹脂含有繊維の平均直径を450nmにすること以外は、実施例1と同様にして多孔質層を形成した。エポキシ樹脂の密度と比誘電率、繊維の熱伝導率、多孔質層の縦長さ、横長さ、厚みは実施例1と同様であった。多孔質層の空孔率、積層体の空孔率を表1に示す。
(実施例8)
溶剤であるN,N−ジメチルホルムアミド(DMF)にポリスチレンを溶解して20wt%溶液を調製し、原料溶液とした。
(実施例9)
溶剤であるN,N−ジメチルアセトアミド(DMAc)にポリアミドイミド30%を溶解して30wt%溶液を調製し原料溶液とした。
(比較例)
ガラス繊維からなる多孔質シートを用意した。多孔質シートは、縦長さ150mm、横長さ150mm、厚さが1mmであった。ガラスの密度は2.5g/cm3であった。ガラスの熱伝導率を繊維の熱伝導率とみなすため、繊維の熱伝導率は1W/m・Kである。繊維の平均直径を、実施例1と同様な方法で測定したところ、5μmであった。多孔質層の空孔率を前述の方法で測定したところ、95%であった。
以下に、当初の特許請求の範囲に記載された発明を付記する。
[1]繊維により構成されるコア材と、前記コア材を構成するものであって、前記コア材の変形を抑制する芯材と、を備える構造体。
[2]前記芯材は、前記コア材内に設けられ、前記繊維からなる繊維層の厚さを抑えることにより前記繊維の圧縮量を抑制する[1]に記載の構造体。
[3]前記芯材は、前記コア材内に設けられることにより、前記繊維の使用量を抑える[1]または[2]に記載の構造体。
[4]前記芯材は、多孔質である[1]から[3]の何れかに記載の構造体。
[5]前記コア材の少なくとも一部を覆う表面形成材を備える[1]から[4]何れかに記載の構造体。
[6][1]から[5]の何れかに記載の構造体に備えられるコア材。
[7]熱硬化性樹脂及び電解質を含む繊維を含む多孔質層を少なくとも一層含む、構造体。
[8]前記熱硬化性樹脂がエポキシ樹脂で、かつ前記電解質が臭化リチウムである、[7]に記載の構造体。
[9]前記繊維が30nm以上5μm以下の平均直径を有する、[7]または[8]に記載の構造体。
[10]前記熱硬化性樹脂の比誘電率の範囲は1以上1000以下である、[7]〜[9]いずれかに記載の構造体。
[11]密度が0.5g/cm 3 以上3g/cm 3 以下の樹脂を含有し、かつ30nm以上5μm未満の平均直径を有する繊維を含む空孔率が45%以上95%以下の多孔質層を複数含む積層体を含む、構造体。
[12]前記密度が1g/cm 3 以上2g/cm 3 以下である、[11]に記載の構造体。
[13]前記積層体の空孔率が45%以上95%以下である、[11]または[12]に記載の構造体。
[14]前記繊維の熱伝導率が0.01W/m・K以上5W/m・K以下である、[11]〜[13]のいずれかに記載の構造体。
[15]前記樹脂がエポキシ樹脂である、[11]〜[14]のいずれかに記載の構造体。
[16]繊維により構成されるコア材と、前記コア材を構成するものであって、前記コア材と接触している芯材と、を備える構造体。
Claims (16)
- 繊維により構成されるコア材と、
前記コア材を構成するものであって、前記コア材の変形を抑制する芯材と、を備える構造体。 - 前記芯材は、前記コア材内に設けられ、前記繊維からなる繊維層の厚さを抑えることにより前記繊維の圧縮量を抑制する請求項1に記載の構造体。
- 前記芯材は、前記コア材内に設けられることにより、前記繊維の使用量を抑える請求項1または2に記載の構造体。
- 前記芯材は、多孔質である請求項1から3の何れか1項に記載の構造体。
- 前記コア材の少なくとも一部を覆う表面形成材を備える請求項1から4の何れか1項に記載の構造体。
- 請求項1から5の何れか1項に記載の構造体に備えられるコア材。
- 熱硬化性樹脂及び電解質を含む繊維を含む多孔質層を少なくとも一層含む、構造体。
- 前記熱硬化性樹脂がエポキシ樹脂で、かつ前記電解質が臭化リチウムである、請求項7に記載の構造体。
- 前記繊維が30nm以上5μm以下の平均直径を有する、請求項7または請求項8に記載の構造体。
- 前記熱硬化性樹脂の比誘電率の範囲は1以上1000以下である、請求項7〜9いずれか1項に記載の構造体。
- 密度が0.5g/cm3以上3g/cm3以下の樹脂を含有し、かつ30nm以上5μm未満の平均直径を有する繊維を含む空孔率が45%以上95%以下の多孔質層を複数含む積層体を含む、構造体。
- 前記密度が1g/cm3以上2g/cm3以下である、請求項11に記載の構造体。
- 前記積層体の空孔率が45%以上95%以下である、請求項11または12に記載の構造体。
- 前記繊維の熱伝導率が0.01W/m・K以上5W/m・K以下である、請求項11〜13のいずれか1項に記載の構造体。
- 前記樹脂がエポキシ樹脂である、請求項11〜14のいずれか1項に記載の構造体。
- 繊維により構成されるコア材と、
前記コア材を構成するものであって、前記コア材と接触している芯材と、
を備える構造体。
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CN107415383B (zh) | 2021-01-12 |
EP3272517A1 (en) | 2018-01-24 |
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US10906266B2 (en) | 2021-02-02 |
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CN106163793A (zh) | 2016-11-23 |
CN107323014A (zh) | 2017-11-07 |
JP6725713B2 (ja) | 2020-07-22 |
JPWO2016148259A1 (ja) | 2017-04-27 |
EP3272517B1 (en) | 2022-04-20 |
US10099447B2 (en) | 2018-10-16 |
CN109895482A (zh) | 2019-06-18 |
JP2017087737A (ja) | 2017-05-25 |
JP6139805B2 (ja) | 2017-05-31 |
US20170100913A1 (en) | 2017-04-13 |
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